SIST EN 12594:2007
(Main)Bitumen and bituminous binders - Preparation of test samples
Bitumen and bituminous binders - Preparation of test samples
This European Standard specifies a method for preparing samples of bituminous binders in order to test their properties.
WARNING - Use of this European standard can involve hazardous materials, operations and equipment. This European standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Bitumen und bitumenhaltige Bindemittel - Vorbereitung von Untersuchungsproben
Bitumes et liants bitumineux - Préparation des échantillons d'essai
La présente Norme européenne prescrit une méthode de préparation des échantillons de liants bitumineux afin de tester leurs propriétés.
AVERTISSEMENT - L'utilisation de la présente Norme européenne peut impliquer l'intervention de produits, d'opérations et d'équipements a caractere dangereux. La présente Norme européenne n'est pas censée aborder tous les problemes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de cette norme d'établir des regles de sécurité et d'hygiene appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.
Bitumen in bitumenska veziva - Priprava preskusnih vzorcev
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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen and bituminous binders - Preparation of test samplesBitumen in bitumenska veziva - Priprava preskusnih vzorcevBitumes et liants bitumineux - Préparation des échantillons d'essaiBitumen und bitumenhaltige Bindemittel - Vorbereitung von UntersuchungsprobenTa slovenski standard je istoveten z:EN 12594:2007SIST EN 12594:2007en91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:SIST EN 12594:20001DGRPHãþDSLOVENSKI
STANDARDSIST EN 12594:200701-julij-2007
EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 12594March 2007ICS 75.140; 91.100.50Supersedes EN 12594:1999
English VersionBitumen and bituminous binders - Preparation of test samplesBitumes et liants bitumineux - Préparation des échantillonsd'essaiBitumen und bitumenhaltige Bindemittel - Vorbereitung vonUntersuchungsprobenThis European Standard was approved by CEN on 3 February 2007.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2007 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 12594:2007: E
EN 12594:2007 (E) 2 Contents Page Foreword.3 1 Scope.4 2 Normative references.4 3 Terms and definitions.5 4 Principle.5 5 Reagents and materials.5 6 Apparatus.6 7 Procedure for sample preparation.6 8 Test report.9
EN 12594:2007 (E) 3 Foreword This document (EN 12594:2007) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2007, and conflicting national standards shall be withdrawn at the latest by September 2007. This document supersedes EN 12594:1999. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EN 12594:2007 (E) 4 1 Scope This European Standard specifies a method for preparing samples of bituminous binders in order to test their properties. WARNING — Use of this European standard can involve hazardous materials, operations and equipment. This European standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced standard (including any amendments) applies. EN 58, Bitumen and bituminous binders - Sampling bituminous binders EN 1425, Bitumen and bituminous binders - Characterization of perceptible properties EN 1427, Bitumen and bituminous binders - Determination of the softening point - Ring and Ball method EN 1429, Bitumen and bituminous binders - Determination of residue on sieving of bitumen emulsions, and determination of storage stability by sieving EN 1431, Bitumen and bituminous binders - Determination of recovered binder and oil distillate from bitumen emulsions by distillation EN 12607-1, Bitumen and bituminous binders - Determination of the resistance to hardening under the influence of heat and air - Part 1: RTFOT method EN 12607-2, Bitumen and bituminous binders - Determination of the resistance to hardening under the influence of heat and air - Part 2: TFOT method EN 12607-3, Bitumen and bituminous binders - Determination of the resistance to hardening under the influence of heat and air - Part 3: RFT method EN 12697-1, Bituminous mixtures - Test methods for hot mix asphalt - Part 1: Soluble binder content EN 12697-2, Bituminous mixtures - Test method for hot mix asphalt - Part 2: Determination of particle size distribution EN 12697-4, Bituminous mixtures - Test methods for hot mix asphalt - Part 4: Bitumen recovery: Fractionating column EN 12847, Bitumen and bituminous binders - Determination of settling tendency of bitumen emulsions EN 13074, Bitumen and bituminous binders - Recovery of binder from bitumen emulsions by evaporation EN 14769, Bitumen and bituminous binders - Accelerated long-term ageing conditioning by a Pressure Ageing Vessel (PAV) EN 14895, Bitumen and bituminous binders - Stabilisation of binder from bituminous emulsions or from cut-back and fluxed bituminous binders
EN 12594:2007 (E) 5 EN ISO 3696:1995, Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) ISO 5280, Xylene for industrial use – Specification 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 58 and the following apply. 3.1 laboratory sample sample of bituminous binder intended for laboratory tests. It may be a spot sample, a composite sample or a part thereof (a divided sample) 3.2 test sample sample of bituminous binder produced by treatment or subdivision of a laboratory sample for individual testing 4 Principle In order to produce the laboratory sample the test material shall have been sampled in accordance with EN 58. Perceptible properties of the test material shall be checked in accordance with EN 1425, prior to performing the present standard. Homogenize the laboratory sample before the test samples are taken. For certain tests (7.3.2) transfer the laboratory sample directly to the test sample containers and for other tests (7.3.3) sieve the laboratory sample prior to testing. Store the laboratory sample from which the test samples are taken under controlled conditions. Stir gently to render it uniform and warm the sample, if necessary. Prepare all test samples that are required for one property at the same time. 5 Reagents and materials 5.1 General Use only reagents of standard analytical grade and water conforming to grade 3 of EN ISO 3696:1995. 5.2 Solution Sa Aqueous solution with a nominal 0,01 mol/L of sodium hydroxide (NaOH) containing a nominal 1 % mass fraction sodium oleate. This solution may be used for preparing anionic emulsion samples. The actual soap solution may be used if available on site, in case of routine tests or for simplicity. NOTE Sa stands for "anionic solution" as this solution is used for preparing anionic emulsion samples. 5.3 Solution Sc Aqueous solution of nominal 0,01 mol/l of hydrochloric acid (HCl) containing a nominal 1 % mass fraction cetyltrimethylammonium bromide. This solution may be used for preparing cationic emulsion samples. The actual aqueous phase may be used if available on site, in case
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