Oil and gas industries including lower carbon energy - Wet thermal insulation systems for pipelines and subsea equipment - Part 1: Validation of materials and insulation systems (ISO/FDIS 12736-1:2023)

Erdöl- und Erdgasindustrie - Wärmedämmschicht für Rohrleitungen und Unterwasseranlagen - Teil 1: Validierung von Materialien und Isoliersystemen (ISO/FDIS 12736-1:2023)

Industries du pétrole et du gaz, y compris les énergies à faible teneur en carbone - Systèmes d'isolation thermique en milieu humide pour conduites et équipements sous-marins - Partie 1: Validation des matériaux et des systèmes d'isolation (ISO/FDIS 12736-1:2023)

Naftna in plinska industrija, vključno z nizkoogljično energijo - Mokre toplotne izolacijske prevleke za naftovode in podvodno opremo - 1. del: Validacija materialov in izolacijskih sistemov (ISO/FDIS 12736-1:2023)

General Information

Status
Not Published
Public Enquiry End Date
10-Mar-2022
Technical Committee
Current Stage
5020 - Formal vote (FV) (Adopted Project)
Start Date
14-Jul-2023
Due Date
01-Sep-2023
Completion Date
14-Jul-2023

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SLOVENSKI STANDARD
oSIST prEN ISO 12736-1:2022
01-marec-2022
Industrija za predelavo nafte in zemeljskega plina - Mokre toplotne izolacijske
prevleke za naftovode in podvodno opremo - 1. del: Validacija materialov in
izolacijskih sistemov (ISO/DIS 12736-1:2021)
Petroleum and natural gas industries - Wet thermal insulation systems for pipelines and
subsea equipment - Part 1: Validation of materials and insulation systems (ISO/DIS
12736-1:2021)
Erdöl- und Erdgasindustrie - Wärmedämmschicht für Rohrleitungen und
Unterwasseranlagen - Teil 1: Validierung von Materialien und Isoliersystemen (ISO/DIS
12736-1:2021)
Industries du pétrole et du gaz naturel - Revêtements pour isolation thermique humide
de canalisations, lignes d'écoulement et structures sous-marines - Partie 1: Validation
des matériaux et des systèmes d'isolation (ISO/DIS 12736-1:2021)
Ta slovenski standard je istoveten z: prEN ISO 12736-1
ICS:
25.220.20 Površinska obdelava Surface treatment
75.180.10 Oprema za raziskovanje, Exploratory, drilling and
vrtanje in odkopavanje extraction equipment
oSIST prEN ISO 12736-1:2022 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN ISO 12736-1:2022

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oSIST prEN ISO 12736-1:2022
DRAFT INTERNATIONAL STANDARD
ISO/DIS 12736-1
ISO/TC 67/SC 2 Secretariat: UNI
Voting begins on: Voting terminates on:
2021-12-17 2022-03-11
Petroleum and natural gas industries — Wet thermal
insulation systems for pipelines and subsea equipment —
Part 1:
Validation of materials and insulation systems
ICS: 25.220.20; 75.180.10
This document is circulated as received from the committee secretariat.
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
ISO/CEN PARALLEL PROCESSING
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 12736-1:2021(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2021

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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2021
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 2
4 Symbols and abbreviated terms.6
4.1 Symbols . 6
4.2 Abbreviated terms . 7
5 Conformance . 8
5.1 Rounding . 8
5.2 C onformity to requirement . 8
6 Material classes . 9
7 Materials and system validation testing . 9
7.1 General . 9
7.2 Material validation testing . 9
7.2.1 General . 9
7.2.2 Small scale exposure testing for materials . 10
7.3 System validation testing.13
7.3.1 General .13
7.3.2 System test requirements . 14
7.3.3 Full scale test program for systems . 14
7.3.4 Small scale full-system exposure test . 17
7.4 System repairs . 17
7.5 Validation of long-term performance . 17
7.6 Technical validation dossier . 18
7.6.1 General . 18
7.6.2 Content of the validation dossier . 18
7.7 Anti-corrosion coating documentation . 20
Annex A (informative) Guidelines for using this document.21
Annex B (normative) Thermal conductivity testing .26
Annex C (normative) Hydrostatic compressive behaviour/Tri-axial test procedures .38
Annex D (normative) Simulated bend test .46
Annex E (normative) System shear resistance test .49
Annex F (normative) Impact test .51
Annex G (normative) Simulated service test for pipelines .54
Annex H (normative) Simulated service test for subsea equipment .56
Annex I (normative) Small scale full-system exposure test .58
Bibliography .60
iii
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore
structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 2, Pipeline
transportation systems.
This second edition partly cancels and replaces the first edition (ISO 12736:2014), which has been
technically revised and split into three parts.
The main changes compared to the previous edition are as follows:
— clearer delineation between validation and projects;
— introduction of material classes;
— modification of material property testing requirements, including detailed thermal conductivity
testing requirements;
— introduction of additional long-term testing requirements;
— introduction of additional system testing requirements, including system interfaces;
— removal of project specific testing requirements;
— addition of requirement for risk-based analysis of the system long-term performance;
— modifications of the format and content requirements of the final validation dossier;
— addition of informative annex with guidelines for using this document.
A list of all parts in the ISO 12736 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
Introduction
Users of this document are advised that further or differing requirements can be required for individual
applications. This document is not intended to inhibit a vendor from offering, or the purchaser from
accepting, alternative equipment or engineering solutions for the individual application. This can be
particularly applicable where there is innovative or developing technology. Where an alternative is
offered, it is the responsibility of the vendor to identify any variations from this document and provide
details. Annex A further clarifies the intended use of this document.
v
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oSIST prEN ISO 12736-1:2022

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oSIST prEN ISO 12736-1:2022
DRAFT INTERNATIONAL STANDARD ISO/DIS 12736-1:2021(E)
Petroleum and natural gas industries — Wet thermal
insulation systems for pipelines and subsea equipment —
Part 1:
Validation of materials and insulation systems
1 Scope
This document defines the minimum requirements for validation of wet thermal insulation systems
applied to pipelines and subsea equipment in the petroleum and natural gas industries.
This document is applicable to wet thermal insulation systems submerged in seawater.
This document is not applicable to:
— maintenance works on existing installed wet thermal insulation systems;
— qualification for anti-corrosion coating;
— thermal insulation in the annulus of a steel pipe-in-pipe system.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 34 (all parts), Rubber, vulcanized or thermoplastic — Determination of tear strength
ISO 37, Rubber, vulcanized or thermoplastic — Determination of tensile stress-strain properties
ISO 179-1, Plastics — Determination of Charpy impact properties — Part 1: Non-instrumented impact test
ISO 527 (all parts), Plastics — Determination of tensile properties
ISO 604, Plastics — Determination of compressive properties
ISO 844, Rigid cellular plastics — Determination of compression properties
ISO 868, Plastics and ebonite — Determination of indentation hardness by means of a durometer (Shore
hardness)
ISO 1183 (all parts), Plastics — Methods for determining the density of non-cellular plastics
ISO 6721-1, Plastics — Determination of dynamic mechanical properties — Part 1: General principles
ISO 8301, Thermal insulation — Determination of steady-state thermal resistance and related properties
— Heat flow meter apparatus
ISO 8302, Thermal insulation — Determination of steady-state thermal resistance and related properties
— Guarded hot plate apparatus
ISO 11357-1, Plastics — Differential scanning calorimetry (DSC) — Part 1: General principles
ISO 11357-4, Plastics — Differential scanning calorimetry (DSC) — Part 4: Determination of specific heat
capacity
1
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
ISO 11359-2, Plastics — Thermomechanical analysis (TMA) — Part 2: Determination of coefficient of linear
thermal expansion and glass transition temperature
ISO 12736-2, Petroleum and natural gas industries — Wet thermal insulation systems for pipelines and
subsea equipment — Part 2: Qualification processes for production and application procedures
ISO 12736-3, Petroleum and natural gas industries — Wet thermal insulation systems for pipelines and
subsea equipment — Part 3: Interfaces between systems, field joint systems, field repairs, and pre-fabricated
insulation
ISO 15711, Paints and varnishes — Determination of resistance to cathodic disbonding of coatings exposed
to sea water
ISO 80000-1, Quantities and units — Part 1: General
ASTM D575, Standard Test Methods for Rubber Properties in Compression
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
3.1
application procedure specification
quality specification document, or group of specifications, describing procedures, method, equipment,
tools, etc. used for system (3.34) application
3.2
batch
quantity of material (3.17) produced in a continuous manufacturing operation using raw materials of
the same source or grade
3.3
blown foam
insulation material (3.17) formed by incorporating a gas phase into a polymer matrix
3.4
certificate of analysis
document provided by the manufacturer which indicates results of specific tests or analysis, including
test methodology, performed on a defined lot of the manufacturer’s product and corresponding
conformity ranges
3.5
construction joint
interface (3.12) where both systems (3.34) are identical
3.6
cutback
length of item left uncoated at each end for joining purposes
Note 1 to entry: Joining purposes are welding, for example.
3.7
field joint
uncoated area that results when two pipe sections, or a pipe section and a fitting (3.8), with cutbacks
(3.6) are assembled by welding or other methods
2
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
3.8
fitting
receptacle on a piece of subsea equipment (3.32), which interfaces to a pipeline (3.21)
3.9
high molecular weight precursor thermoset
material (3.17), which is a polymeric compound that remains malleable until application of sufficient
heat to cause network formation and then does not flow upon reheating
EXAMPLE Butyl rubber.
3.10
inorganic syntactic foam
insulation material (3.17) formed by dispersing inorganic hollow particles within a polymer matrix
3.11
inspection and test plan
document providing an overview of the sequence of inspections and tests, including appropriate
resources and procedures
3.12
interface
location where two systems (3.34) meet and affect each other.
Note 1 to entry: A field joint system has two interfaces.
Note 2 to entry: In the case of multilayer systems, interfaces can be made up of multiple sub-interfaces.
3.13
jumper
short section of pipeline (3.21) that transfers fluid between two pieces of subsea equipment (3.32)
3.14
liquid precursor elastomeric thermoset
material (3.17), which is a polymeric compound with its glass transition below ambient temperature,
that is produced via combination of one or more components that can be pumped and flow as liquids
and which react to create a crosslinked polymer that does not flow upon reheating
EXAMPLE Liquid precursor silicone rubber.
3.15
liquid precursor non-elastomeric thermoset
material (3.17), which is a polymeric compound with its glass transition above ambient temperature,
that is produced via combination of one or more components that can be pumped and flow as liquids
and which react to create a crosslinked polymer that does not flow upon reheating
EXAMPLE Liquid epoxy,.
3.16
mainline
portion of a pipeline (3.21) which is not a field joint (3.7)
3.17
material
polymeric compound applied to the surface to be protected/insulated in units of discrete thickness
(layers) to build up a system (3.34)
3.18
material manufacturer
legal entity responsible for the manufacture of one or more materials (3.17) utilized in a system (3.34)
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
3.19
material maximum and minimum rated temperature
maximum and minimum temperature to which a particular material (3.17) can be continuously
exposed, as per system provider (3.36) recommendation, during storage or in service as part of a system
(3.34)
Note 1 to entry: For multi-layer systems, the material maximum rated temperature can be less than the system
maximum rated temperature (3.35).
3.20
maximum rated pressure
maximum hydrostatic pressure to which the system (3.34) can be exposed, according to the system
provider (3.36)
3.21
pipeline
flowline
tubular piping used to convey fluids
Note 1 to entry: Pipeline includes jumpers (3.13), risers (3.27) and field joints (3.7).
3.22
pre-fabricated insulation
section of stand-alone insulative material (3.17), which is factory manufactured into its final form and
then installed in the field by mechanically fastening or bonding to a corrosion protected structure
3.23
pre-production trial
series of tests performed immediately before the start of production, designed to demonstrate that the
requirements of the validated system (3.34) and/or procedure qualification trial (3.24) are achieved, as
outlined in this document and as agreed
3.24
procedure qualification trial
series of tests designed to demonstrate that the materials (3.17), system provider (3.36), equipment and
procedures can produce the system (3.34) in accordance with the validation dossier (3.43) and meet the
specific project requirements as outlined in this document and as agreed
3.25
project
scope of work agreed upon contractually between system purchaser (3.37) and system provider (3.36)
3.26
R-lay
reel-lay
method of pipeline (3.21) installation in which long stalks (3.31) of pre-insulated pipes are pre-
assembled by welding and application of field joint (3.7) system onshore before being spooled onto large
reels onboard the installation vessel, which then lays the pipes by unspooling the reel offshore
3.27
riser
vertical portion of a pipeline (3.21), including the bottom bend, arriving on or departing from an
offshore surface installation
4
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
3.28
safety data sheet
DEPRACATED: material safety data sheet
form intended to provide workers and emergency personnel with procedures for handling and working
with a material (3.17) utilized in the manufacture of the system (3.34) in a safe manner including
physical data
Note 1 to entry: Physical data can include flash point, toxicity and first aid.
3.29
service life
specified period of use for a system (3.34) in service
3.30
solid/solid filled
insulation material (3.17) which systematically does not contain voids, bubbles, or hollow particles
3.31
stalk
continuous string of welded and field joint (3.7) coated pipe, which is prepared in readiness for pipe
spooling onto a reel-lay (3.26) barge
Note 1 to entry: Note1 to entry: A number of stalks will normally be required to make up a pipeline (3.21).
3.32
subsea equipment
components from a subsea production system, including subsea processing items and structures, meant
to control hydrocarbons, not including pipelines (3.21)
EXAMPLE Valve, connector, manifold, christmas tree, flowline end termination.
3.33
substrate
surface to which a material (3.17) is applied or is to be applied
3.34
system
all of the various materials (3.17) and the combination thereof, which can include layers of anti-
corrosion, insulation, adhesive, and protective materials, as defined by cross-section to the underlying
substrate (3.33) at a single point, which function together to act as a wet thermal insulation (3.44)
3.35
system maximum and minimum rated temperature
maximum and minimum temperature to which a particular system (3.34) can be continuously exposed,
as per system provider (3.36) recommendation, during storage or in service
3.36
system provider
legal entity which is selling/marketing the applied system (3.34)
3.37
system purchaser
legal entity which is purchasing the applied system (3.34)
3.38
thermal conductivity
k-value
conductivity
heat flow through a unit length of material (3.17) under the influence of a thermal gradient
-1 -1
Note 1 to entry: Thermal conductivity is expressed in W·m ·K
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
3.39
thermoplastic
material (3.17), which is a polymeric compound that solidifies upon cooling and can flow and be
reformed upon reheating
EXAMPLE Polypropylene.
3.40
tie-in field joint
connection of a pipeline (3.21) to a facility or subsea equipment (3.32), to other pipeline systems, or the
connecting together of different sections of a single pipeline
3.41
U-value
overall heat transfer coefficient
rate of heat transfer from a reference surface under the influence of a thermal gradient
-2 -1
Note 1 to entry: Note1 to entry: U-value is expressed in W·m ·K .
3.42
validation
demonstration of material (3.17) and system (3.34) performance during storage, handling and operation,
within a defined envelope of use, as determined by the system provider (3.36)
3.43
validation dossier
collection of documentation and test reports, which provides detailed information on the proposed
system (3.34), method of application, the materials (3.17) which form said system, and demonstration of
system performance, prepared in accordance with this document
3.44
wet thermal insulation
system (3.34) that provides external corrosion protection and thermal insulation, and that is in direct
contact with surrounding fluid
4 Symbols and abbreviated terms
4.1 Symbols
E impact energy (kinetic energy), expressed in Joules
kin
g standard gravity, equivalent to 9,81 metres per seconds squared
H pendulum height, expressed in metres
m mass of hammer, expressed in kilograms
h
Q average value of heat flux transducers signals for sample i, where i = 1, 2, or 3, expressed
ave,i
in microVolts
Q lower plate heat flux transducer signal, expressed in microVolts
lower
Q average lower plate heat flux transducer signal, expressed in microVolts
Lower,Average
Q average value of heat flux transducers signals for reference material sample, expressed
Ref Mat ave
in Watts per microVolts
Q average value of heat flux transducers signals for reference material sample 1 (typically
Ref Mat ave,1
the thinner sample), expressed in Watts per microVolts
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oSIST prEN ISO 12736-1:2022
ISO/DIS 12736-1:2021(E)
Q average value of heat flux transducers signals for reference material sample 2 (typically
Ref Mat ave,2
the thicker sample), expressed in Watts per microVolts
Q upper plate heat flow, expressed in microVolts
upper
Q average upper plate heat flow, expressed in microVolts
Upper,Average
S calibration factor, expressed in watts per microVolts
Cal
S single-thickness calibration factor, proportional factor between the electrical signal and
Cal1
heat flow, expressed in Watts per microVolts
S two-thickness calibration factor, proportional factor between the electrical signal and
Cal2
heat flow, expressed in Watts per microVolts
S lower plate calibration factor, expressed in Watts per microVolts
Cal,Lower
S upper plate calibration factor, expressed in Watts per microVolts
Cal,Upper
R̄ total average measured thermal resistance across all samples, expressed in metres
ave
square degrees Kelvin per Watt
R average measured thermal resistance of sample i, where i = 1, 2, or 3, expressed in metres
ave,i
square degrees Kelvin per Watt
R calibration contact resistance, expressed in metres square degrees Kelvin per Watt
cal
2R lower plate calibration contact resistance, expressed in metres square degrees Kelvin
Cal,Lower
per Watt
2R , upper plate calibration contact resistance, expressed in metres square degrees Kelvin
Cal Upper
per Watt
2R contact resistance
...

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