SIST EN 13632:2010
(Main)Bitumen and bituminous binders - Visualisation of polymer dispersion in polymer modified bitumen
Bitumen and bituminous binders - Visualisation of polymer dispersion in polymer modified bitumen
This European Standard specifies a method for visualisation of the polymer distribution in polymer modified bitumen by fluorescent microscopy. The method is applicable for most of the commercially used polymers, but before the method is used it should be examined whether the test is applicable for the actual polymer. The method should only be used for identification purposes, i.e. in connection with production control.
Bitumen und bitumenhaltige Bindemittel - Visualisierung der Polymerverteilung in polymermodifiziertem Bitumen
Dieses Dokument legt ein Verfahren zur Visualisierung der Polymerverteilung in polymermodifiziertem Bitumen mit einem Fluoreszenz-Mikroskop fest. Das Verfahren ist auf die meisten handelsüblichen Polymere anwendbar, vor seiner Anwendung sollte jedoch geprüft werden, ob die Prüfung auch für das im gegebenen Fall vorliegende Polymer geeignet ist. Das Verfahren sollte nur für die Zwecke der Identifizierung, d. h. im Zusammenhang mit der Produktionskontrolle, angewendet werden. ANMERKUNG Probenvorbereitung und -behandlung haben erheblichen Einfluss auf die Prüfergebnisse, und es ist daher wichtig, das beschriebene Verfahren strikt zu befolgen, um vergleichbare Ergebnisse zu erhalten. WARNUNG — Die Anwendung dieser Europäischen Norm kann den Umgang mit gefährlichen Substanzen und Ausrüstungsteilen und die Ausführung gefährlicher Arbeitsgänge einschließen. Diese Europäische Norm erhebt nicht den Anspruch, alle mit ihrer Anwendung verbundenen Sicherheitsprobleme
anzusprechen.
Verhaltensregeln zur Sicherheit und Gesundheit festzulegen und vor der Anwendung zu klären,
ob einschränkende Vorschriften zu berücksichtigen sind.
Bitumes et liants bitumineux - Visualisation de la dispersion des polymères dans les bitumes modifiés par des polymères
La présente norme européenne spécifie une méthode de visualisation de la distribution des polymères dans les
bitumes modifiés par des polymères, par microscopie de fluorescence.
La méthode est applicable à la plupart des polymères utilisés commercialement, mais il est recommandé de vérifier
que l’essai s’applique au polymère en présence avant d’utiliser la méthode.
Il convient d’utiliser la méthode seulement à des fins d’identification, c’est à dire en rapport avec des contrôles de
production.
NOTE La préparation de l'échantillon et son traitement ont une influence importante sur les résultats de l'essai, aussi est-il
essentiel de suivre strictement la méthode décrite en vue d'obtenir des résultats comparables.
AVERTISSEMENT — L'utilisation de la présente Norme européenne implique l'intervention de produits,
d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n'est pas censée
aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur
de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des
restrictions réglementaires avant utilisation.
Bitumen in bitumenska veziva - Vizualni pregled razporeditve polimerov v bitumnih, modificiranih s polimeri
Ta evropski standard določa metodo vizualnega pregleda razporedite polimerov v bitumnih, modificiranih s polimeri, s fluorescentno mikroskopijo. Metoda velja za večino komercialno uporabljenih polimerov, vendar je potrebno uporabo metode presoditi, ali preskus velja za aktualni polimer. Metoda naj se uporablja samo za namen identifikacije, t.j. v povezavi s kontrolo proizvodnje.
General Information
Relations
Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen in bitumenska veziva - Vizualni pregled razporeditve polimerov v bitumnih, modificiranih s polimeriBitumen und bitumenhaltige Bindemittel - Visualisierung der Polymerverteilung in polymermodifiziertem BitumenBitumes et liants bitumineux - Visualisation de la dispersion des polymères dans les bitumes modifiés par des polymèresBitumen and bituminous binders - Visualisation of polymer dispersion in polymer modified bitumen91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13632:2010SIST EN 13632:2010en,fr,de01-oktober-2010SIST EN 13632:2010SLOVENSKI
STANDARDSIST EN 13632:20041DGRPHãþD
SIST EN 13632:2010
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 13632
May 2010 ICS 75.140; 91.100.50 Supersedes EN 13632:2003English Version
Bitumen and bituminous binders - Visualisation of polymer dispersion in polymer modified bitumen
Bitumes et liants bitumineux -Visualisation de la dispersion des polymères dans les bitumes modifiés par des polymères
Bitumen und bitumenhaltige Bindemittel - Visualisierung der Polymerverteilung in polymermodifiziertem Bitumen This European Standard was approved by CEN on 23 April 2010.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 13632:2010: ESIST EN 13632:2010
EN 13632:2010 (E) 2 Contents page Foreword . 31 Scope . 42 Normative references . 43 Principle . 44 Apparatus . 45 Preparation of test samples . 56 Procedure . 57 Expression of results . 58 Test report . 5Annex A (informative)
Bitumen modified by polymers . 7 SIST EN 13632:2010
EN 13632:2010 (E) 3 Foreword This document (EN 13632:2010) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR/BNPé. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by November 2010, and conflicting national standards shall be withdrawn at the latest by November 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 13632:2003. Annex A is informative. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. SIST EN 13632:2010
EN 13632:2010 (E) 4 1 Scope This European Standard specifies a method for visualisation of the polymer distribution in polymer modified bitumen by fluorescent microscopy. The method is applicable for most of the commercially used polymers, but before the method is used it should be examined whether the test is applicable for the actual polymer. The method should only be used for identification purposes, i.e. in connection with production control. NOTE Sample preparation and treatment have an important influence on the test results and it is essential to follow strictly the method described to achieve comparable results. WARNING — The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders — Sampling bituminous binders EN 12594, Bitumen and bituminous binders — Preparation of test samples 3 Principle A sample of polymer modified bitumen is homogenised by gentle stirring and poured into a preheated mould. After a controlled cooling procedure to ambient temperature the sample is cooled below – 20 °C for a minimum period of time. The bitumen layer is broken into small pieces and the freshly broken surface is viewed through a microscope with a magnification of 25 times to 500 times. The views can be stored photographically or electronically. 4 Apparatus 4.1 Epifluorescence microscope, (incident light excitation) with an appropriate light source and filter systems. NOTE Examples of light source and filter system are given in Annex A. 4.2 Freezer or solid carbon dioxide. 4.3 Sharp tool. Scissors shall not be used. 4.4 Aluminium basin, disposable, approximate height 35 mm, approximate diameter 70 mm. 4.5 Porcelain evaporating basin, diameter 150 mm, height 63 mm (approximate volume: 600 ml). SIST EN 13632:2010
EN 13
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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen in bitumenska veziva - Vizualni pregled razporeditve polimerov v bitumnih, modificiranih s polimeriBitumen und bitumenhaltige Bindemittel - Visualisierung der Polymerverteilung in polymermodifiziertem BitumenBitumes et liants bitumineux - Visualisation de la dispersion des polymères dans les bitumes modifiés par des polymèresBitumen and bituminous binders - Visualisation of polymer dispersion in polymer modified bitumen91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:FprEN 13632kSIST FprEN 13632:2010en,de01-januar-2010kSIST FprEN 13632:2010SLOVENSKI
STANDARD
kSIST FprEN 13632:2010
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
FINAL DRAFT
FprEN 13632
October 2009 ICS 75.140; 91.100.50 Will supersede EN 13632:2003English Version
Bitumen and bituminous binders - Visualisation of polymer dispersion in polymer modified bitumen
Bitumes et liants bitumineux -Visualisation de la dispersion des polymères dans les bitumes modifiés par des polymères
Bitumen und bitumenhaltige Bindemittel - Visualisierung der Polymerverteilung in polymermodifiziertem Bitumen This draft European Standard is submitted to CEN members for unique acceptance procedure. It has been drawn up by the Technical Committee CEN/TC 336.
If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2009 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. FprEN 13632:2009: EkSIST FprEN 13632:2010
FprEN 13632:2009 (E) 2 Contents page Foreword . 31 Scope . 42 Normative references . 43 Principle . 44 Apparatus . 45 Preparation of test samples . 56 Procedure . 57 Expression of results . 58 Test report . 5Annex A (informative)
Bitumen modified by polymers . 7 kSIST FprEN 13632:2010
FprEN 13632:2009 (E) 3 Foreword This document (FprEN 13632:2009) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This document is currently submitted to the Unique Acceptance Procedure. This document will supersede EN 13632:2003. Annex A is informative. kSIST FprEN 13632:2010
FprEN 13632:2009 (E) 4 1 Scope This document specifies a method for visualisation of the polymer distribution in polymer modified bitumen by fluorescent microscopy. The method is applicable for most of the commercially used polymers, but before the method is used it should be examined whether the test is applicable for the actual polymer. The method should only be used for identification purposes, i.e. in connection with production control. NOTE Sample preparation and treatment have an important influence on the test results and it is essential to follow strictly the method described to achieve comparable results. WARNING — The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders — Sampling bituminous binders EN 12594, Bitumen and bituminous binders — Preparation of test samples 3 Principle A sample of polymer modified bitumen is homogenised by gentle stirring and poured into a preheated mould. After a controlled cooling procedure to ambient temperature the sample is cooled below – 20 °C for a minimum period of time. The bitumen layer is broken into small pieces and the freshly broken surface is viewed through a microscope with a magnification of 25 times to 500 times. The views can be stored photographically or electronically. 4 Apparatus 4.1 Epifluorescence microscope, (incident light excitation) with an appropriate light source and filter systems. NOTE Examples of light source and filter system are given in Annex A. 4.2 Freezer or solid carbon dioxide 4.3 Sharp tool Scissors shall not be used. 4.4 Aluminium basin, disposable, approximate height 35 mm, approximate diameter 70 mm 4.5 Porcelain evaporating basin, diameter 150 mm, height 63 mm (approximate volume: 600 ml) 4.6 Fine aggregate (sand) kSIST FprEN 13632:2010
FprEN 13632:2009 (E) 5 4.7 Temperature regulated sand bath 5 Preparation of test samples Take the sample in accordance with EN 58. Prepare it in accordance with EN 12594. Homogenise the sample by gentle hand stirring for at least 1 min and not more than 5 min. Pour the material into the aluminium basin placed in a sand bat
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