Analysis of natural gas - Biomethane - Determination of ammonia content by Tuneable Diode Laser Absorption Spectroscopy (ISO/FDIS 2612:2023)

This document specifies a Tuneable Diode Laser Absorption Spectroscopy method for the determination of ammonia content of biogas, natural gas or biomethane
This document describes the suitable handling and sampling of pressurised mixtures of ammonia in
methane that are applied to several different ammonia measurement systems. The measurement systems comprise of readily available commercial spectroscopic analysers that are specific to ammonia.
The method is applicable to the determination of ammonia concentrations from 1 mg/m3 (1,3 ppm volume fraction) to 100 mg/m3 (132 ppm volume fraction).
The method has a lower limit of detection of about 0,4 mg/m3 (0,5 ppm volume fraction) NH3 in air with
the tested analyser in Annex B.

Analyse von Erdgas - Biomethan - Bestimmung von Ammoniakanteil durch Absorptionsspektroskopie mittels durchstimmbarer Laserdioden (ISO/FDIS 2612:2023)

Dieses Dokument beschreibt mehrere Prüfverfahren zum Messen des Ammoniakmengenanteils in Erdgas und Biomethan im Spurenbereich (μmol mol-1). Die geeignete Handhabung und Probenahme von druckbeaufschlagten Gemischen von Ammoniak in Methan, die auf mehrere verschiedene Ammoniakmesseinrichtungen angewendet werden, sind beschrieben. Die Messeinrichtungen bestehen aus fertig im Handel erhältlichen spektroskopischen Analysatoren, die spezifisch für Ammoniak sind. Diese NH3-Analysatoren gelten als eine Black Box bezüglich ihres Betriebs, der von den Anweisungen des Herstellers abhängig ist. Das Dokument beschreibt geeignete Kalibrier- und Messstrategien zum Quantifizieren von Ammoniak in (Bio)Methan um und über einem Niveau von 10 mg m−3 (14 μmol mol−1) und gilt für eine Analyse innerhalb von Absolutdruckbereichen von 1 bar bis 2 bar, bei Temperaturen von 0 °C bis 40 °C und bei einer relativen Feuchtigkeit von <90 %.
Es sind ebenfalls Verweisungen auf zusätzliche Normen enthalten, die auf die Erdgasanalyse oder auf Luftqualitätsmessungen angewendet werden. In diesem Dokument ist das Matrixgas immer Methan oder Biomethan und die Messgröße ist der Stoffmengenanteil NH3.
ANMERKUNG 1 bar = 0,1 MPa = 105 Pa; 1 MPa = 1 N/mm2

Analyse du gaz naturel - Biométhane - Détermination de la teneur en ammoniac par spectroscopie d'absorption laser à diode accordable (ISO/FDIS 2612:2023)

Le présent document décrit plusieurs méthodes d'essai permettant de mesurer la fraction molaire d'ammoniac dans le gaz naturel et le biométhane à l'état de traces (µmol mol−1). Il décrit la manipulation et l'échantillonnage appropriés de mélanges sous pression d'ammoniac dans le méthane appliqués à plusieurs systèmes de mesure de l'ammoniac différents. Les systèmes de mesure comprennent des analyseurs par spectroscopie commerciaux facilement disponibles qui sont spécifiques à l'ammoniac. Ces analyseurs de NH3 sont considérés comme une boîte noire en ce qui concerne leur fonctionnement, qui dépend des instructions du fabricant. Le présent document décrit les stratégies d'étalonnage et de mesurage appropriées pour la quantification de l'ammoniac dans le (bio)méthane aux environs et au-dessus du niveau de 10 mg m−3 (14 µmol mol−1) et s'applique à l'analyse dans des plages de pression absolue de 1 bar à 2 bar, des températures de 0 °C à 40 °C et une humidité relative < 90 %.
Des références sont également faites à des normes supplémentaires qui s'appliquent soit à l'analyse du gaz naturel, soit aux mesures de la qualité de l'air. Dans le présent document, le gaz de la matrice est toujours le méthane ou le biométhane et le mesurande est la fraction molaire de NH3.
NOTE            1 bar = 0,1 Mpa = 105 Pa; 1 Mpa = 1 N/mm2.

Analiza zemeljskega plina - Biometan - Določanje amoniaka z absorpcijsko spektroskopijo z nastavljivimi laserskimi diodami (ISO/FDIS 2612:2023)

General Information

Status
Not Published
Public Enquiry End Date
02-May-2023
Technical Committee
Current Stage
5020 - Formal vote (FV) (Adopted Project)
Start Date
25-Sep-2023
Due Date
13-Nov-2023
Completion Date
10-Nov-2023

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Standards Content (Sample)

SLOVENSKI STANDARD
oSIST prEN ISO 2612:2023
01-april-2023
[Not translated]
Analysis of natural gas - Biomethane - Determination of ammonia content by Tuneable
Diode Laser Absorption Spectroscopy (ISO/DIS 2612:2023)
Analyse von Erdgas - Biomethan - Bestimmung von Ammoniakanteil durch
Absorptionsspektroskopie mittels durchstimmbarer Laserdioden (ISO/DIS 2612:2023)
Analyse du gaz naturel - Biométhane - Détermination de la teneur en ammoniac par
spectroscopie d'absorption laser à diode accordable (ISO/DIS 2612:2023)
Ta slovenski standard je istoveten z: prEN ISO 2612
ICS:
75.060 Zemeljski plin Natural gas
oSIST prEN ISO 2612:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN ISO 2612:2023

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oSIST prEN ISO 2612:2023
DRAFT INTERNATIONAL STANDARD
ISO/DIS 2612
ISO/TC 193/SC 1 Secretariat: NEN
Voting begins on: Voting terminates on:
2023-02-13 2023-05-08
Analysis of natural gas — Biomethane — Determination
of ammonia content by Tuneable Diode Laser Absorption
Spectroscopy
ICS: 75.060
This document is circulated as received from the committee secretariat.
THIS DOCUMENT IS A DRAFT CIRCULATED
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PROVIDE SUPPORTING DOCUMENTATION. © ISO 2023

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oSIST prEN ISO 2612:2023
ISO/DIS 2612:2023(E)
DRAFT INTERNATIONAL STANDARD
ISO/DIS 2612
ISO/TC 193/SC 1 Secretariat: NEN
Voting begins on: Voting terminates on:

Analysis of natural gas — Biomethane — Determination
of ammonia content by Tuneable Diode Laser Absorption
Spectroscopy
ICS: 75.060
This document is circulated as received from the committee secretariat.
COPYRIGHT PROTECTED DOCUMENT
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© ISO 2023
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be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on STANDARD UNTIL PUBLISHED AS SUCH.
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NATIONAL REGULATIONS.
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ii
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PROVIDE SUPPORTING DOCUMENTATION. © ISO 2022

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oSIST prEN ISO 2612:2023
ISO/DIS 2612:2022(E)
Contents Page
Foreword .v
Introduction . vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions .
...

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