SIST EN 12606-1:2015
(Main)Bitumen and bituminous binders - Determination of the paraffin wax content - Part 1: Method by distillation
Bitumen and bituminous binders - Determination of the paraffin wax content - Part 1: Method by distillation
This European Standard specifies a procedure for determining the paraffin wax content of bitumen and bituminous binder by the DIN method.
Aqueous bituminous binders, fluxed or cut-back anhydrous binders, and modified binders, whatever their consistency, are not within the scope of the present test method.
WARNING - Use of this European standard can involve hazardous materials, operations and equipment. This European standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Paraffingehaltes - Teil 1: Destillationsverfahren
Diese Europäische Norm legt ein Verfahren zur Bestimmung des Paraffingehaltes von Bitumen und bitumenhaltigen Bindemitteln nach dem DIN-Verfahren fest.
Dieses Prüfverfahren gilt nicht für wässrige bitumenhaltige Bindemittel, gefluxte oder verschnittene nicht wässrige Bindemittel und modifizierte Bindemittel, egal von welcher Konsistenz.
WARNUNG — Die Anwendung dieser Europäischen Norm kann den Umgang mit gefährlichen Substanzen und Ausrüstungsteilen und die Ausführung gefährlicher Arbeitsgänge einschließen. Diese Europäische Norm erhebt nicht den Anspruch, alle mit ihrer Anwendung verbundenen Sicherheitsprobleme anzusprechen. Es liegt in der Verantwortung des Anwenders dieser Europäischen Norm, geeignete Verhaltensregeln für den Arbeits- und Gesundheitsschutz festzulegen und vor der Anwendung zu klären, ob einschränkende Vorschriften zu berücksichtigen sind.
Bitumes et liants bitumineux - Détermination de la teneur en paraffines - Partie 1 : Méthode par distillation
La présente Norme européenne a pour objet la détermination de la teneur en paraffines des bitumes et liants bitumineux par la méthode DIN.
Les liants bitumineux aqueux, les liants anhydres fluxés ou fluidifiés et les liants modifiés, quelle que soit leur consistance, ne font pas partie du domaine d’application de la présente méthode d’essai.
AVERTISSEMENT — L’utilisation de la présente Norme européenne peut impliquer le recours à des produits, des opérations et des équipements à caractères dangereux. La présente Norme européenne n’est pas censée aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l’utilisateur de consulter et d’établir des règles de sécurité et d’hygiène appropriées et de déterminer l’applicabilité des restrictions réglementaires avant utilisation.
Bitumen in bitumenska veziva - Določevanje parafina - 1. del: Metoda destilacije
Ta evropski standard določa postopek za določevanje parafina bitumna in bitumenskega veziva z metodo DIN.
Vodna bitumenska veziva, rezana ali razredčena brezvodna veziva in spremenjena veziva, ne glede na njihovo gostoto, niso zajeta v tej preskusni metodi.
OPOZORILO: Pri uporabi tega evropskega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta evropski standard ne obravnava vseh varnostnih težav, ki se nanašajo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega evropskega standarda.
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen und bitumenhaltige Bindemittel - Bestimmung des Paraffingehaltes - Teil 1: DestillationsverfahrenBitumes et liants bitumineux - Détermination de la teneur en paraffines - Partie 1 : Méthode par distillationBitumen and bituminous binders - Determination of the paraffin wax content - Part 1: Method by distillation91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 12606-1:2015SIST EN 12606-1:2015en,fr,de01-oktober-2015SIST EN 12606-1:2015SLOVENSKI
STANDARDSIST EN 12606-1:20071DGRPHãþD
SIST EN 12606-1:2015
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 12606-1
July 2015 ICS 75.140; 91.100.50 Supersedes EN 12606-1:2007English Version
Bitumen and bituminous binders - Determination of the paraffin wax content - Part 1: Method by distillation
Bitumes et liants bitumineux - Détermination de la teneur en paraffines - Partie 1 : Méthode par distillation
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Paraffingehaltes - Teil 1: Destillationsverfahren This European Standard was approved by CEN on 27 May 2015.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2015 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 12606-1:2015 ESIST EN 12606-1:2015
EN 12606-1:2015 (E) 2 Contents Page Foreword .3 1 Scope .4 2 Normative references .4 3 Terms and definitions .4 4 Principle .4 5 Reagents and materials .5 6 Apparatus .5 7 Sampling .6 8 Procedure .6 9 Calculation .8 10 Expression of results .8 11 Precision .9 11.1 Repeatability .9 11.2 Reproducibility .9 12 Test report .9 13 Figures . 10
SIST EN 12606-1:2015
EN 12606-1:2015 (E) 3 Foreword This document (EN 12606-1:2015) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This document supersedes EN 12606-1:2007. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2016, and conflicting national standards shall be withdrawn at the latest by January 2016. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. The standard has been revised due to a normative reference to mercury thermometers. The changes involve mainly the text in 6.2. The terms “sample thermometer” and “bath thermometer” have been changed, as a consequence, to “sample temperature transducer” and “bath temperature transducer” respectively in some subparagraphs of Clause 8. This draft European standard EN 12606 consists of the following parts under the general title Bitumen and bituminous binders – Determination of the paraffin wax content — Part 1: Method by distillation; — Part 2: Method by extraction. The changes introduced mainly involve the revision of the text in 6.2 relating to the mentioning of mercury thermometers as reference thermometers. According to the CEN/CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 12606-1:2015
EN 12606-1:2015 (E) 4 1 Scope This European Standard specifies a procedure for determining the paraffin wax content of bitumen and bituminous binder by the DIN method. Aqueous bituminous binders, fluxed or cut-back anhydrous binders, and modified binders, whatever their consistency, are not within the scope of the present test method. WARNING — Use of this European standard can involve hazardous materials, operations and equipment. This European standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders - Sampling bituminous binders EN 1425, Bitumen and bituminous binders - Characterization of perceptible properties EN 12594, Bitumen and bituminous binders - Preparation of test samples EN ISO 3696:1995, Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) ISO 383, Laboratory glassware — Interchangeable conical ground joints 3 Terms and definitions For the purposes of this document, the following term and definition applies. 3.1 paraffin wax mixture of hydrocarbons crystallising in a 50 % volume fraction mixture of ether/ethanol at temperatures down to - 20 °C, obtained by a specified process and having a melting range of above 25 °C 4 Principle Paraffin wax present in bitumen is determined in the distillate obtained from a specified distillation process. SIST EN 12606-1:2015
EN 12606-1:2015 (E) 5 5 Reagents and materials 5.1 General Use only reagents of recognized analytical grade and water conforming to grade 3 of EN ISO 3696:1995 unless otherwise specified. 5.2 Ethoxyethane (Diethylether), anhydrous, referred to in this standard as ether. 5.3 Ethanol, absolute. 5.4 Ethanol, technical grade. 5.5 Petroleum spirit, with density of approximately 645 kg/m³ at 15 °C, and a distillation range of approximately 30 °C to 75 °C. 5.6 Acetone, reagent grade. 5.7 Carbon dioxide, solid, finely ground. NOTE A cryostat with a cooling effect equivalent to that of solid carbon dioxide can be used. 5.8 Ice, finely ground. 5.9 Washing liquid, a 50 % volume fraction mixture of ether/ethanol. 6 Apparatus Usual laboratory apparatus and glassware, together with the following: (Dimensions in this clause are approximate unless tolerances are stated). 6.1 Oven, capable of maintaining (125 ± 5) °C. 6.2 Temperature measuring devices, (combining reading device and transducers) referred to in this standard as: 6.2.1 Sample temperature transducer: a sensor which together with a reading device shall have a measuring range of –38 °C to 50 °C, be readable to the nearest 1,0 °C with an accuracy of 0,5 °C. The sensor shall be embedded in a glass rod with total length (360 ± 5) mm and outside diameter (10,0 ± 0,5) mm. 6.2.2 Bath temperature transducer: a sensor which together with a reading device shall have a measuring range of –30 °C to 50 °C, be readable to the nearest 0,5 °C with an accuracy of 0,5 °C. The sensor shall be embedded in a glass rod with total length (220 ± 5) mm and outside diameter (8,0 ± 0,5) mm. The temperature measuring devices employed shall be calibrated regularly. 6.3 Distillation flask as shown in Figure 1, fitted with cork stopper. 6.4 Sheet metal guard ring with an approximate 18 mm inside diameter and a 65 mm outside diameter. 6.5 Test tubes, fitted with a spout and bored cork stopper; dimensions are given in Figure 2. 6.6 Test
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