Bitumen and bituminous binders - Dynamic viscosity of bituminous emulsions, cut-back and fluxed bituminous binders - Rotating spindle viscometer method

This European Standard specifies a method for the determination of the dynamic viscosity of bituminous emulsions, cut-back and fluxed bituminous binders, by means of a coaxial viscometer. There are standard application temperatures quoted, although the dynamic viscosity can be measured at other temperatures if required. Similarly, viscosity is quoted at standard rates of shear, although additional measurements can be taken at varying shear rates if required.
NOTE   Some bituminous materials may exhibit non-Newtonian behaviour under the conditions of this method. Since non-Newtonian viscosity values are not unique material properties, but reflect the behaviour of the fluid and the measurement system, it should be recognised that measurements made by this method may not always predict performance under the conditions of use. Comparisons between non-Newtonian viscosities should be made only for measurements under similar conditions of shear stress and shear rate.
WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Dynamische Viskosität von Bitumenemulsionen, verschnittenen und gefluxten bitumenhaltigen Bindemitteln - Viskosimeter-Verfahren mit rotierender Spindel

Diese Europäische Norm legt ein Verfahren zur Bestimmung der dynamischen Viskosität von Bitumenemulsionen
sowie verschnittenen und gefluxten bitumenhaltigen Bindemitteln mittels eines Koaxialviskosimeters
fest. Es sind Standard-Anwendungstemperaturen angegeben, obgleich die dynamische Viskosität, falls
erforderlich, auch bei anderen Temperaturen gemessen werden kann. In entsprechender Weise ist die Viskosität
bei Standard-Schergeschwindigkeiten angegeben, obgleich bei veränderlichen Schergeschwindigkeiten,
falls erforderlich, zusätzliche Maßnahmen ergriffen werden dürfen.
ANMERKUNG Einige bitumenhaltige Materialien können unter den Bedingungen dieses Verfahrens nicht-newtonsches
Verhalten aufweisen. Da nicht-newtonsche Viskositätswerte keine eindeutigen Materialeigenschaften sind, sondern das
Verhalten der Flüssigkeit und des Messsystems widerspiegeln, sollte beachtet werden, dass sich aus den nach diesem
Verfahren erhaltenen Messwerten möglicherweise nicht immer die Leistung unter den Einsatzbedingungen vorhersagen
lässt. Vergleiche zwischen nicht-newtonschen Viskositäten sollten nur für Messungen angestellt werden, die unter ähnlichen
Bedingungen hinsichtlich der Schubspannung und der Schergeschwindigkeit stattfinden.
WARNUNG - Die Anwendung dieser Norm kann den Umgang mit gefährlichen Substanzen und Ausrüstungsteilen
und die Ausführung gefährlicher Arbeitsgänge einschließen. Diese Norm erhebt nicht
den Anspruch, alle mit ihrer Anwendung verbundenen Sicherheitsprobleme anzusprechen. Es liegt in
der Verantwortung des Anwenders dieser Norm, geeignete Verhaltensregeln zur Sicherheit und Gesundheit
festzulegen und die Anwendbarkeit einschränkender Vorschriften vor der Anwendung zu
bestimmen.

Bitumes et liants bitumineux - Détermination de la viscosité dynamique des émulsions bitumineuses, des liants bitumineux fluidifiés et fluxés - Méthode du viscosimetre a mobile tournant

La présente Norme européenne prescrit une méthode de détermination de la viscosité dynamique des
émulsions bitumineuses, des liants bitumineux fluidifiés et fluxés au moyen d’un viscosimetre coaxial. Des
températures de référence sont citées dans la norme, cependant la viscosité dynamique peut etre mesurée a
d’autres températures si cela est exigé. De maniere analogue, la viscosité est évaluée pour des taux de
cisaillement précisés, cependant d’autres mesures peuvent etre réalisées avec des taux de cisaillement
variables si exigé.
NOTE Il arrive que certaines émulsions présentent un comportement non-newtonien dans les conditions de la
présente méthode. Les valeurs de viscosité non newtoniennes ne sont pas des propriétés intrinseques du matériau mais
sont l'image du comportement du fluide et des conditions de mesure. Il convient donc d’avoir a l’esprit que les mesures
effectuées par la présente méthode ne donnent pas toujours une bonne prévision des performances dans les conditions
d’utilisation. Il est conseillé de n’effectuer des comparaisons entre des viscosités non-newtoniennes que pour des
mesures effectuées sous des contraintes de cisaillement et des taux de cisaillement comparables.
AVERTISSEMENT - La mise en oeuvre de la présente norme peut impliquer l’utilisation de produits, des
manipulations et des appareillages a caractere dangereux. La présente norme européenne n'est pas censée
aborder tous les problemes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de
consulter et d'établir des regles de sécurité et d'hygiene appropriées et de déterminer l'applicabilité des
restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določevanje dinamične viskoznosti bitumenskih emulzij ter rezanih in fluksiranih bitumenskih veziv - Metoda z rotacijskim vretenom

General Information

Status
Withdrawn
Publication Date
30-Nov-2006
Withdrawal Date
02-May-2010
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
03-May-2010
Due Date
26-May-2010
Completion Date
03-May-2010

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen and bituminous binders - Dynamic viscosity of bituminous emulsions, cut-back and fluxed bituminous binders - Rotating spindle viscometer methodELWXPHQVNLKRWDFLMVNLPYUHWHQRPBitumes et liants bitumineux - Détermination de la viscosité dynamique des émulsions bitumineuses, des liants bitumineux fluidifiés et fluxés - Méthode du viscosimetre a mobile tournantBitumen und bitumenhaltige Bindemittel - Dynamische Viskosität von Bitumenemulsionen, verschnittenen und gefluxten bitumenhaltigen Bindemitteln - Viskosimeter-Verfahren mit rotierender SpindelTa slovenski standard je istoveten z:EN 14896:2006SIST EN 14896:2006en91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:SLOVENSKI
STANDARDSIST EN 14896:200601-december-2006







EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14896September 2006ICS 75.140; 91.100.50 English VersionBitumen and bituminous binders - Dynamic viscosity ofbituminous emulsions, cut-back and fluxed bituminous binders -Rotating spindle viscometer methodBitumes et liants bitumineux - Détermination de la viscositédynamique des émulsions bitumineuses, des liantsbitumineux fluidifiés et fluxés - Méthode du viscosimètre àmobile tournantBitumen und bitumenhaltige Bindemittel - DynamischeViskosität von Bitumenemulsionen, verschnittenen undgefluxten bitumenhaltigen Bindemitteln - Viskosimeter-Verfahren mit rotierender SpindelThis European Standard was approved by CEN on 3 August 2006.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2006 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14896:2006: E



EN 14896:2006 (E) 2 Contents Page Foreword.3 1 Scope.4 2 Normative references.4 3 Terms and definitions.4 4 Principle.5 5 Apparatus.5 6 Sampling.5 7 Procedure.6 8 Expression of results.8 9 Precision.8 10 Test report.8



EN 14896:2006 (E) 3 Foreword This document (EN 14896:2006) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by March 2007, and conflicting national standards shall be withdrawn at the latest by March 2007. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association, and supports essential requirements of EU Construction Products Directive (89/106/EEC). According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.



EN 14896:2006 (E) 4 1 Scope This European Standard specifies a method for the determination of the dynamic viscosity of bituminous emulsions, cut-back and fluxed bituminous binders, by means of a rotating spindle viscometer. There are standard application temperatures quoted, although the dynamic viscosity can be measured at other temperatures if required. Similarly, viscosity is quoted at standard rates of shear, although additional measurements can be taken at varying shear rates if required. NOTE Some bituminous materials may exhibit non-Newtonian behaviour under the conditions of this method. Since non-Newtonian viscosity values are not unique material properties, but reflect the behaviour of the fluid and the measurement system, it should be recognised that measurements made by this method may not always predict performance under the conditions of use. Comparisons between non-Newtonian viscosities should be made only for measurements under similar conditions of shear stress and shear rate. WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders – Sampling bituminous binders EN 12594, Bitumen and bituminous binders – Preparation of test samples 3 Terms and definitions For the purposes of this European Standard, the following terms and definitions apply. 3.1 shear rate velocity gradient in a flowing fluid perpendicular to the stress, measured in units of s-1 NOTE The shear rate calculation depends upon the viscosimeter geometry. This should be mentioned by the viscosimeter manufacturer. 3.2 shear stress force acting tangentially to a surface divided by the area of the surface, measured in units of
N. m-2, kg. m-1. s-2 or Pa 3.3 dynamic viscosity ratio between the applied shear stress and the shear rate NOTE Dynamic viscosity is the measurement of the resistance to flow of the liquid. The SI unit of dynamic viscosity is the Pascal.second (Pa.s), the milliPascal.second (mPa.s) is a frequently used sub-unit. 3.4 Newtonian fluid fluid having a viscosity that is independent of the rate of shear



EN 14896:2006 (E) 5 NOTE The ratio of the shear stress to the shear rate is the viscosity of the fluid. If this ratio is not constant the liquid is non-Newtonian. Many fluids exhibit both Newtonian and non-Newtonian behaviour depending on the temperature and the shear rate. 3.5 form factor specific factor or factors applied for individual equipment in order to obtain the actual viscosity from the readings, mainly due to t
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