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ASTM D5396-04

(Specification)

Standard Specification for Reclaimed Perchloroethylene

Standard Specification for Reclaimed Perchloroethylene

ABSTRACT
This specification establishes the requirements for reclaimed perchloroethylene typically needed in various industries for noncritical applications such as in metal cleaning formulations. This is not recommended for dry cleaning applications, but may be used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs. Covered here are the following types: Type I, generally recognized for use in precision applications; Type II, used for less demanding precision applications; and Type III, general purpose technical grade. Specimens shall be tested and each type should conform individually to the following properties: specific gravity; maximum compositions for chlorides, nonvolatile residue, water, and 1,1,1-trichloroethane; assay weight; color (Pt-Co scale); appearance; acid acceptance (as NaOH); and acidity (as HCl).
SCOPE
1.1 This specification covers the grade of perchloroethylene typically needed in various industries for noncritical applications, such as in metal cleaning formulations. It is not recommended for dry cleaning applications (see Specification D 4081). It may be used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs.

General Information

Status
Historical
Publication Date
31-Dec-2003
ICS
71.080.20 - Halogenated hydrocarbons
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.02 - Vapor Degreasing
Current Stage
Ref Project

Relations

Replaces
ASTM D5396-00 - Standard Specification for Reclaimed Perchloroethylene
Effective Date
01-Jan-2004
Replaced By
ASTM D5396-04(2010) - Standard Specification for Reclaimed Perchloroethylene
Effective Date
01-Feb-2010

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ASTM D5396-04 - Standard Specification for Reclaimed PerchloroethyleneASTM D5396-04 - Standard Specification for Reclaimed Perchloroethylene
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ASTM D5396-04 - Standard Specification for Reclaimed Perchloroethylene
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D5396 – 04
Standard Specification for
,
1 2
Reclaimed Perchloroethylene
This standard is issued under the fixed designation D5396; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D6806 Practice for Analysis of Halogenated Organic Sol-
vents and Their Admixtures by Gas Chromatography
1.1 This specification covers the grade of perchloroethylene
E1064 Test Method for Water in Organic Liquids by Cou-
typically needed in various industries for noncritical applica-
lometric Karl Fischer Titration
tions, such as in metal cleaning formulations. It is not recom-
2.2 Other Documents:
mended for dry cleaning applications (see Specification
29 CFR 1910.1200 Department of Labor, OSHA Regula-
D4081). It may be used as a reference document by purchasers
4
tions, Hazard Communication
orbypersonsestablishingin-houseperchloroethylenerecovery
49 CFR 100 to 199 Department of Transportation Hazard-
programs.
4
ous Materials Regulations
2. Referenced Documents
3. Classification
3
2.1 ASTM Standards:
3.1 Type I—Generally recognized for use in precision ap-
D2108 Test Method for Color of Halogenated Organic
plications.
Solvents and Their Admixtures (Platinum-Cobalt Scale)
3.2 Type II—Use for less demanding precision applications.
D2109 Test Methods for Nonvolatile Matter in Halogenated
3.3 Type III—General-purpose technical grade.
Organic Solvents and Their Admixtures
D2111 Test Methods for Specific Gravity and Density of
4. Properties
Halogenated Organic Solvents and Their Admixtures
4.1 Reclaimed perchloroethylene, Type I, shall meet the
D2942 Test Method for Total Acid Acceptance of Haloge-
requirements of Table 1.
nated Organic Solvents (Nonreflux Methods)
4.2 Reclaimed perchloroethylene, Type II, shall meet the
D2988 Test Methods for Water-Soluble Halide Ion in Ha-
requirements of Table 1.
logenated Organic Solvents and Their Admixtures
4.3 Reclaimed perchloroethylene, Type III, shall meet the
D2989 Test Method for Acidity-Alkalinity of Halogenated
requirements of Table 1.
Organic Solvents and Their Admixtures
D3401 Test Methods for Water in Halogenated Organic
5. Packaging and Package Marking
Solvents and Their Admixtures
5.1 Industrial or commercial quantities shall be packaged
D3741 Test Methods for Appearance of Admixtures Con-
and labeled in accordance with DOTregulations as found in 49
taining Halogenated Organic Solvents
CFR100to199,inaccordancewithstateandlocalregulations,
D4081 Specification for Drycleaning-Grade Perchloroeth-
and in accordance with OSHA regulations found in 29 CFR
ylene
1919.1200.
1
6. Keywords
This specification is under the jurisdiction of ASTM Committee D26 on
H
...

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