iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM D3618-05

(Test Method)

Standard Test Method for Detection of Lead in Paint and Dried Paint Films

Standard Test Method for Detection of Lead in Paint and Dried Paint Films

SIGNIFICANCE AND USE
The permissible level of heavy metals in certain coatings is specified by governmental regulatory agencies. This test method provides a fully documented procedure for determining low concentrations of lead present in both water and solvent-reducible coatings to determine compliance.
SCOPE
1.1 This test method is intended as a screening test to determine if the solids in a paint contain more than 0.5 % lead. The test described barely detects the presence of 0.4 % but gives a definite positive result at the 0.5 % level. Note 1This test method may be used to detect the presence of lead at concentrations higher or lower than 0.5 % by making appropriate changes in the specimen size and reagent quantities specified.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 Paints giving an unexpected positive or questionable result should be analyzed quantitatively for lead, using Test Method D 3335.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section .

General Information

Status
Historical
Publication Date
31-Dec-2004
ICS
87.040 - Paints and varnishes
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.21 - Chemical Analysis of Paints and Paint Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D3618-85a(1999) - Standard Test Method for Detection of Lead in Paint and Dried Paint Films
Effective Date
01-Jan-2005
Replaced By
ASTM D3618-05(2010) - Standard Test Method for Detection of Lead in Paint and Dried Paint Films
Effective Date
01-Dec-2010
Referred By
ASTM D4834-03(2021) - Standard Test Method for Detection of Lead in Paint by Direct Aspiration Atomic Absorption Spectroscopy
Effective Date
01-Jan-2005

Buy Standard

ASTM D3618-05 - Standard Test Method for Detection of Lead in Paint and Dried Paint FilmsASTM D3618-05 - Standard Test Method for Detection of Lead in Paint and Dried Paint Films
PreviousNext
Standard
ASTM D3618-05 - Standard Test Method for Detection of Lead in Paint and Dried Paint Films
English language
3 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D3618–05
Standard Test Method for
1
Detection of Lead in Paint and Dried Paint Films
This standard is issued under the fixed designation D3618; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope extract is transferred to filter paper. Lead present is oxidized to
leadperoxidewithbrominewater,thentreatedwith“tetrabase”
1.1 This test method is intended as a screening test to
to produce a blue quinoidal salt. Known amounts of lead are
determine if the solids in a paint contain more than 0.5 % lead.
added to standard paints that are concurrently tested to provide
The test described barely detects the presence of 0.4 % but
a base for comparison.
gives a definite positive result at the 0.5 % level.
NOTE 1—This test method may be used to detect the presence of lead 4. Significance and Use
at concentrations higher or lower than 0.5 % by making appropriate
4.1 The permissible level of heavy metals in certain coat-
changes in the specimen size and reagent quantities specified.
ingsisspecifiedbygovernmentalregulatoryagencies.Thistest
1.2 The values stated in SI units are to be regarded as the
methodprovidesafullydocumentedprocedurefordetermining
standard. The values given in parentheses are for information
low concentrations of lead present in both water and solvent-
only.
reducible coatings to determine compliance.
1.3 Paints giving an unexpected positive or questionable
5. Apparatus
result should be analyzed quantitatively for lead, using Test
Method D3335.
5.1 Burner, Meker-type.
1.4 This standard does not purport to address all of the
5.2 Crucibles, porcelain, high-form, 15-mL, with covers.
safety concerns, if any, associated with its use. It is the
5.3 Filter Paper, ashless, medium texture.
responsibility of the user of this standard to establish appro-
5.4 Hot Plate, with variable surface temperature control
priate safety and health practices and determine the applica-
over the range from 70 to 200°C.
bility of regulatory limitations prior to use. Specific hazard
5.5 Muffle Furnace, maintained at 475 6 25°C.
statements are given in Section 7.
5.6 Syringe, glass, 2-mL.
5.7 Volumetric Flasks, 50, 100, 1000-mL.
2. Referenced Documents
5.8 Paint Shaker.
2
2.1 ASTM Standards:
5.9 Paint Draw-Down Bar.
D1193 Specification for Reagent Water
6. Reagents
D2832 Guide for Determining Volatile and Nonvolatile
Content of Paint and Related Coatings
6.1 Purity of Reagents—Reagent grade chemicals shall be
D3335 Test Method for Low Concentrations of Lead, Cad-
used in all tests unless otherwise specified. Unless otherwise
mium, and Cobalt in Paint by Atomic Absorption Spec-
indicated, it is intended that all reagents shall conform to the
troscopy
specifications of the Committee on Analytical Reagents of the
American Chemical Society, where such specifications are
3. Summary of Test Method
3
available. Other grades may be used, provided it is first
3.1 The sample of liquid paint or dried film is prepared by
ascertained that the reagent is of sufficiently high purity to
dry ashing a weighed specimen at 475 to 500°C. The ash is
permit its use without lessening the accuracy of the determi-
extracted with hot sodium hydroxide solution and a drop of the
nation.
6.2 Purity of Water—Unless otherwise indicated, references
to water shall be understood to mean reagent grade water
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint conforming to Type II of Specification D1193.
and Related Coatings, Materials, andApplications and is the direct responsibility of
Subcommittee D01.21 on Chemical Analysis of Paints and Paint Materials.
Current edition approved Jan. 1, 2005. Published February 2005. Originally
3
approved in 1977. Last previous edition approved in 1999 as D3618 – 85a (1999). Reagent Chemicals, American Chemical Society Specifications , American
DOI: 10.1520/D3618-05. Chemical Society, Washington, DC. For suggestions on the testing of reagents not
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or listed by the American Chemical Society, see Analar Standards for Laboratory
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
Standards volume information, refer to the standard’s Document Summary page on and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville,
the ASTM website. MD.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D3
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM D7190-10(2023)(Practice)
Standard Practice to Evaluate Leaching of Water-Soluble Materials from Latex Paint Films

SIGNIFICANCE AND USE
4.1 Surfactant staining is a common problem with exterior house paints, particularly when subjected to humid environments (such as morning dew) shortly after application.  
4.2 Interior paints used in humid areas such as kitchens and bathrooms may also experience surfactant staining.  
4.3 Leaching of water-soluble materials may be dependent on colorant dispersions that are mixed into tint base paints. Other paint components may also affect the leaching of water-soluble materials.
SCOPE
1.1 This practice covers the ability of a latex paint film to resist staining caused by the leaching of water-soluble materials when contacted with water shortly after application.  
1.2 Water staining is attributed to the leaching of surfactants or other water-soluble materials from a paint film.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D4287-00(2023)(Test Method)
Standard Test Method for High-Shear Viscosity Using a Cone/Plate Viscometer

SIGNIFICANCE AND USE
4.1 The viscosity value obtained by this test method gives information about the flow properties of the material under high-shear conditions similar to those encountered during application: brushing (see Test Method D4958), spraying, electrostatic disk, or roll coating.  
4.2 This test method is suitable for all paints and varnishes whether they are Newtonian in behavior or not. However, due to the narrow gap between the stationary and rotary parts of high-shear viscometers, this test method is more reproducible for paints having finer pigment dispersions as determined by Test Method D1210.
SCOPE
1.1 This test method covers the determination of the viscosity of paints, varnishes, and related products at a rate of shear of 12 000 s−1.  
1.2 Paints and varnishes that dry very rapidly may not give reproducible results with this test method. Measurements made at elevated temperatures may also give poor precision due to loss of volatiles and to drying.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
ASTM
ASTM D4214-23(Test Method)
Standard Test Methods for Evaluating the Degree of Chalking of Exterior Paint Films

SIGNIFICANCE AND USE
4.1 The procedures provide a broad range of techniques and photographic references to evaluate chalking of exterior paints.
SCOPE
1.1 These test methods cover the evaluation of the degree of chalking on white or tinted exterior paint films. These test methods describe the procedures recommended for transferring the chalk to a fabric or fingertip, which is then compared to photographic reference standards, or in the case of adhesive tapes, compared to a reflectance table or photographic reference standards, to determine the degree of chalking.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D4147-18(2023)(Practice)
Standard Practice for Applying Coil Coatings Using Wire-Wound Drawdown Bars

SIGNIFICANCE AND USE
3.1 This practice is useful in the laboratory to simulate roll-coated films.
SCOPE
1.1 This practice covers a procedure for applying a coil coating film of uniform thickness on a flat metal panel using wire-wound drawdown bars.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D16-23(Terminology)
Standard Terminology for Paint, Related Coatings, Materials, and Applications

SCOPE
1.1 This standard consists of technical terms used in standards under the jurisdiction of ASTM Committee D01 (on Paint and Related Coatings, Materials, and Applications), and of definitions suitable for use in these standards.
Note 1: When any definition in this standards is quoted or published out of the context of this standard, editorially insert the following delimiting statement “for paints and related coatings, materials, and applications” after the dash following the term (in the absence of an existing delimiting statement). This will limit the filed of application of the term and definition to that approved by this committee.  
1.2 In this terminology standard, definitions used in other ASTM standards are indicated by following the definition with the designation of that standard. In some cases, a relevant D01 subcommittee is also listed. Definitions influenced by those used by other organizations are indicated by the acronym of the organization. Primary terms are given in bold, while narrower and unapproved terms are given in italics.  
1.3 There are several specialized terminology standards under the jurisdiction of Committee D01, as follows: D804, D1695, D6440, D6488, and D7188. Few definitions from those standards are included in Terminology D16. Therefore, in searches for definitions of paints and coatings terms, these standards should be included where appropriate.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    10 pages
    English language
    sale 15% off
  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM D3732-23(Practice)
Standard Practice for Reporting Cure Times of Ultraviolet-Cured Coatings

SIGNIFICANCE AND USE
4.1 This practice provides a guide whereby all pertinent variables relating to the ultraviolet cure of a coating are described.
SCOPE
1.1 This practice applies to all coatings cured by ultraviolet energy.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D1644-01(2023)(Test Method)
Standard Test Methods for Nonvolatile Content of Varnishes

SIGNIFICANCE AND USE
2.1 These test methods are applicable to varnish and are useful to producers and users in determining nonvolatile content and are sometimes an appropriate measure of the film-forming matter in varnish.
SCOPE
1.1 These test methods determine the fraction of a varnish that is nonvolatile at the temperature of the test while volatile solvents are driven off. It is sometimes an approximate measure of the film-forming matter in a varnish.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific statement, see Section 3.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D6486-23(Practice)
Standard Practice for Short Term Vehicle Service Exposure of Automotive Coatings

SIGNIFICANCE AND USE
4.1 Since the exposure of automotive coatings to the various mechanical and chemical stresses encountered in actual operations, is very opportunistic, obtaining statistically significant data from which valid conclusions can be drawn, requires rigorous attention to the experimental designs and conditions of exposure.
SCOPE
1.1 This practice covers the protocol for vehicle service exposure testing of automotive coatings. Such exposure testing is valuable for the verification of the performance of automotive coatings and correlation with laboratory test data. Vehicle service exposure is intended to provide short term (2 to 20 weeks) exposure to the stress factors associated with vehicle operation. Factors included are scratch, mar, impact, stone chipping, insect impact, bird dropping, tree sap and staining, environmental fallout, etc.
Note 1: Vehicle service exposure is not intended to provide the conditions that are needed for characterizing the long term effects of weathering or corrosion exposure.  
1.2 The exposure conditions are produced by the placement of multiple test panels of automotive finishes on automotive test fleets that traverse a defined road course. Exposure to the operating environment can be 20 h/day, 7 days/week allowing for accumulation of over 100 000 miles in 10 weeks of exposure.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D2805-11(2023)(Test Method)
Standard Test Method for Hiding Power of Paints by Reflectometry

SIGNIFICANCE AND USE
5.1 This is a precise instrumental method giving results having an absolute physical significance without reference to a comparison paint. It should be used when maximum precision and minimum subjectivity are required, as in testing specification coatings or evaluating the hiding efficiency of pigments.  
5.2 Hiding power Test Method D344 is visual instead of instrumental, and gives results that are relative to a material standard instead of absolute. It is less precise than Test Method D2805 but more closely aligned with practical painting procedures.
SCOPE
1.1 This test method covers the determination, without reference to a material paint standard, of the hiding power of air dry coatings with Y tristimulus values greater than 15 %. With appropriate modification, it can also be used to test baking finishes.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM D6762-18(2023)(Test Method)
Standard Test Method for Determining the Hiding Power of Paint by Visual Evaluation of Spray Applied Coatings

SIGNIFICANCE AND USE
5.1 This test method determines hiding power of a test paint by visual evaluation of a spray applied coating.
Note 1: Test Method D2805 describes an instrumental method for determining hiding power. The paint film is applied at a uniform thickness (for example with a doctor blade), the film thickness is measured rigorously, and the opacity is determined photometrically. Hiding power is thereby determined with a high degree of precision.  
5.2 Test Method D6762 is less precise than Test Method D2805, but is commonly used since it is more closely related to the application characteristics of the paint and is simpler in concept and evaluation.
SCOPE
1.1 This test method provides for the quantitative visual determination of the film thickness required to achieve full hiding. This film thickness is considered to be the hiding power of a test paint.  
1.2 This method applies only to spray applied coatings but its concepts are valid for other methods of application as well.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off