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ASTM D6352-03

(Test Method)

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography

SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum distillate fractions. The test method is applicable to petroleum distillate fractions having an initial boiling point greater than 174°C (345°F) and a final boiling point of less than 700°C (1292°F) (C10 to C90) at atmospheric pressure as measured by this test method.
1.2 The test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight components (for example naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example alcohols, ethers, acids, or esters) or residue are not to be analyzed by this test method. See Test Methods D 3710, D 2887, or D 5307 for possible applicability to analysis of these types of materials.
1.3 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are for information only and may be included as parenthetical values.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Oct-2003
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0H - Chromatographic Distribution Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D6352-02 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700&#176C by Gas Chromatography
Effective Date
01-Nov-2003
Replaced By
ASTM D6352-04 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
Effective Date
01-Jun-2004
Referred By
ASTM D7500-15(2019) - Standard Test Method for Determination of Boiling Range Distribution of Distillates and Lubricating Base Oils—in Boiling Range from 100 °C to 735 °C by Gas Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM D7213-15(2019) - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 °C to 615 °C by Gas Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM D7798-20 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates with Final Boiling Points up to 538 °C by Ultra Fast Gas Chromatography (UF GC)
Effective Date
01-Nov-2003
Referred By
ASTM D6417-15(2019) - Standard Test Method for Estimation of Engine Oil Volatility by Capillary Gas Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM F3337-19 - Standard Guide for Taking Property and Behavior Measurements on Weathered Fractions of Oil
Effective Date
01-Nov-2003
Referred By
ASTM D7807-20 - Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection
Effective Date
01-Nov-2003
Referred By
ASTM D7398-21 - Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM D7169-23 - Standard Test Method for Boiling Point Distribution of Samples with Residues Such as Crude Oils and Atmospheric and Vacuum Residues by High Temperature Gas Chromatography
Effective Date
01-Nov-2003

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ASTM D6352-03 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas ChromatographyASTM D6352-03 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
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ASTM D6352-03 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 6352 – 03
Standard Test Method for
Boiling Range Distribution of Petroleum Distillates in
1
Boiling Range from 174 to 700°C by Gas Chromatography
This standard is issued under the fixed designation D 6352; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope* D 2887 Test Method for Boiling Range Distribution of
Petroleum Fractions by Gas Chromatography
1.1 This test method covers the determination of the boiling
D 2892 Test Method for Distillation of Crude Petroleum
range distribution of petroleum distillate fractions. The test
(15-Theoretical Plate Column)
method is applicable to petroleum distillate fractions having an
D 3710 Test Method for Boiling Range Distribution of
initial boiling point greater than 174°C (345°F) and a final
Gasoline and Gasoline Fractions by Gas Chromatography
boiling point of less than 700°C (1292°F) (C10 to C90) at
D 4626 Practice for Calculation of Gas Chromatographic
atmospheric pressure as measured by this test method.
Response Factors
1.2 The test method is not applicable for the analysis of
D 5307 Test Method for Determination of Boiling Range
petroleum or petroleum products containing low molecular
Distributions of Crude Petroleum by Gas Chromatography
weight components (for example naphthas, reformates, gaso-
E 355 Practice for Gas Chromatography Terms and Rela-
lines, crude oils). Materials containing heterogeneous compo-
tionships
nents (for example alcohols, ethers, acids, or esters) or residue
E 594 Practice for Testing Flame Ionization Detectors Used
are not to be analyzed by this test method. See Test Methods
in Gas or Supercritical Fluid Chromatography
D 3710, D 2887, or D 5307 for possible applicability to analy-
E 1510 Practice for Installing Fused Silica Open Tubular
sis of these types of materials.
Capillary Columns in Gas Chromatographs
1.3 The values stated in SI units are to be regarded as
standard. The values stated in inch-pound units are for infor-
3. Terminology
mation only and may be included as parenthetical values.
3.1 Definitions—This test method makes reference to many
1.4 This standard does not purport to address all of the
common gas chromatographic procedures, terms, and relation-
safety concerns, if any, associated with its use. It is the
ships. For definitions of these terms used in this test method,
responsibility of the user of this standard to establish appro-
refer to Practices E 355, E 594, and E 1510.
priate safety and health practices and determine the applica-
3.2 Definitions of Terms Specific to This Standard:
bility of regulatory limitations prior to use.
3.2.1 area slice—the area resulting from the integration of
2. Referenced Documents the chromatographic detector signal within a specified reten-
2 tion time interval. In area slice mode (see 6.4.2), peak detection
2.1 ASTM Standards:
parameters are bypassed and the detector signal integral is
D 86 Test Method for Distillation of Petroleum Products at
recorded as area slices of consecutive, fixed duration time
Atmospheric Pressure
intervals.
D 1160 Test Method for Distillation of Petroleum Products
3.2.2 corrected area slice—an area slice corrected for base-
at Reduced Pressure
line offset by subtraction of the exactly corresponding area
slice in a previously recorded blank (non-sample) analysis.
3.2.3 cumulative corrected area—the accumulated sum of
1
This test method is under the jurisdiction of ASTM Committee D02 on
corrected area slices from the beginning of the analysis through
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
a given retention time, ignoring any non-sample area (for
D02.04 on Hydrocarbon Analysis.
example solvent).
Current edition approved Nov. 1, 2003. Published November 2003. Originally
approved in 1998. Last previous edition approved in 2002 as D 6352–02.
3.2.4 final boiling point (FBP)—the temperature (corre-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
sponding to the retention time) at which a cumulative corrected
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
area count equal to 99.5 % of the total sample area under the
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. chromatogram is obtained.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D6352–03
3.2.5 initial boiling point (
...

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5.1 The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining process, This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
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5.1 The bromine number is useful as a measure of aliphatic unsaturation in petroleum samples. When used in conjunction with the calculation procedure described in Annex A2, it can be used to estimate the percentage of olefins in petroleum distillates boiling up to approximately 315 °C (600 °F).  
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1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
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SCOPE
1.1 This test method covers the determination of solvent extractables in petroleum waxes.  
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1.3 The values stated in inch-pound units or in SI units and which are not in parentheses are to be regarded as the standard. The values given in parentheses are for information only.  
Note 2: Oil tubes and apparatus used in this test method have traditionally been marked in inches, (the tube is required to be etched with 1/8 in. divisions.) The Saybolt Color Numbers are aligned with inch, 1/2 in., 1/4 in., and 1/8 in. changes in the depth of oil. These fractional inch changes do not readily correspond to SI equivalents and in view of the preponderance of apparatus already in use and marked in inches, the inch/pound unit is regarded as the standard. However the test method does use SI units of length when the length is not directly related to divisions on the oil tube and Saybolt Color Numbers. The test method uses SI units for temperature.  
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Standard Practice for Calculating Viscosity of a Blend of Petroleum Products

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5.1 Predicting the viscosity of a blend of components is a common problem. Both the Wright Blending Method and the ASTM Blending Method, described in this practice, may be used to solve this problem.  
5.2 The inverse problem, predicating the required blend fractions of components to meet a specified viscosity at a given temperature may also be solved using either the Inverse Wright Blending Method or the Inverse ASTM Blending Method.  
5.3 The Wright Blending Methods are generally preferred since they have a firmer basis in theory, and are more accurate. The Wright Blending Methods require component viscosities to be known at two temperatures. The ASTM Blending Methods are mathematically simpler and may be used when viscosities are known at a single temperature.  
5.4 Although this practice was developed using kinematic viscosity and volume fraction of each component, the dynamic viscosity or mass fraction, or both, may be used instead with minimal error if the densities of the components do not differ greatly. For fuel blends, it was found that viscosity blending using mass fractions gave more accurate results. For base stock blends, there was no significant difference between mass fraction and volume fraction calculations.  
5.5 The calculations described in this practice have been computerized as a spreadsheet and are available as an adjunct.3
SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
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ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For specific warning statements, see 7.3.  
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ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
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  • Standard
    35 pages
    English language
    sale 15% off