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ASTM D2887-02

(Test Method)

Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538°C (1000°F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55°C (100°F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D 3710.
1.3 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Nov-2002
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0H - Chromatographic Distribution Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D2887-01a - Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
Effective Date
10-Nov-2002
Replaced By
ASTM D2887-03 - Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM D7215-22 - Standard Test Method for Calculated Flash Point from Simulated Distillation Analysis of Distillate Fuels
Effective Date
10-Nov-2002
Referred By
ASTM D7223-21 - Standard Specification for Aviation Certification Turbine Fuel
Effective Date
10-Nov-2002
Referred By
ASTM D2549-23 - Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
Effective Date
10-Nov-2002
Referred By
ASTM D8144-22 - Standard Test Method for Separation and Determination of Aromatics, Nonaromatics, and FAME Fractions in Middle Distillates by Solid-Phase Extraction and Gas Chromatography
Effective Date
10-Nov-2002
Referred By
ASTM D7398-21 - Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography
Effective Date
10-Nov-2002
Referred By
ASTM D4737-21 - Standard Test Method for Calculated Cetane Index by Four Variable Equation
Effective Date
10-Nov-2002
Referred By
ASTM D7169-23 - Standard Test Method for Boiling Point Distribution of Samples with Residues Such as Crude Oils and Atmospheric and Vacuum Residues by High Temperature Gas Chromatography
Effective Date
10-Nov-2002
Referred By
ASTM D7665-22 - Standard Guide for Evaluation of Biodegradable Heat Transfer Fluids
Effective Date
10-Nov-2002
Referred By
ASTM D8046-21 - Standard Guide for Pumpability of Heat Transfer Fluids
Effective Date
10-Nov-2002
Referred By
ASTM D396-21 - Standard Specification for Fuel Oils
Effective Date
10-Nov-2002
Referred By
ASTM D6074-15(2022) - Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
Effective Date
10-Nov-2002
Referred By
ASTM D5154/D5154M-18 - Standard Test Method for Determining Activity and Selectivity of Fluid Catalytic Cracking (FCC) Catalysts by Microactivity Test
Effective Date
10-Nov-2002
Referred By
ASTM D2880-23 - Standard Specification for Gas Turbine Fuel Oils
Effective Date
10-Nov-2002

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ASTM D2887-02 - Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas ChromatographyASTM D2887-02 - Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
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ASTM D2887-02 - Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 2887 – 02
Standard Test Method for
Boiling Range Distribution of Petroleum Fractions by Gas
1
Chromatography
This standard is issued under the fixed designation D 2887; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
4
1. Scope E 260 Practice for Packed Column Gas Chromatography
E 355 Practice for Gas Chromatography Terms and Rela-
1.1 This test method covers the determination of the boiling
4
tionships
range distribution of petroleum products. The test method is
E 516 Practice for Testing Thermal Conductivity Detectors
applicable to petroleum products and fractions having a final
4
Used in Gas Chromatography
boiling point of 538°C (1000°F) or lower at atmospheric
E 594 Practice for Testing Flame Ionization Detectors Used
pressure as measured by this test method. This test method is
4
in Gas or Supercritical Fluid Chromatography
limited to samples having a boiling range greater than 55°C
(100°F), and having a vapor pressure sufficiently low to permit
3. Terminology
sampling at ambient temperature.
3.1 Definitions:
1.2 This test method is not to be used for the analysis of
3.1.1 This test method makes reference to many common
gasoline samples or gasoline components. These types of
gas chromatographic procedures, terms, and relationships.
samples must be analyzed by Test Method D 3710.
Detailed definitions of these can be found in Practices E 260,
1.3 The values stated in SI units are to be regarded as
E 355, and E 594.
standard. The inch-pound units given in parentheses are for
3.2 Definitions of Terms Specific to This Standard:
information only.
3.2.1 area slice—the area, resulting from the integration of
1.4 This standard does not purport to address all of the
the chromatographic detector signal, within a specified reten-
safety concerns, if any, associated with its use. It is the
tion time interval. In area slice mode (see 6.3.2), peak detection
responsibility of the user of this standard to establish appro-
parameters are bypassed and the detector signal integral is
priate safety and health practices and determine the applica-
recorded as area slices of consecutive, fixed duration time
bility of regulatory limitations prior to use.
intervals.
2. Referenced Documents 3.2.2 corrected area slice—an area slice corrected for base-
line offset, by subtraction of the exactly corresponding area
2.1 ASTM Standards:
slice in a previously recorded blank (non-sample) analysis.
D 86 Test Method for Distillation of Petroleum Products at
2
3.2.3 cumulative corrected area—the accumulated sum of
Atmospheric Pressure
corrected area slices from the beginning of the analysis through
D 1160 Test Method for Distillation of Petroleum Products
2
a given retention time, ignoring any non-sample area (for
at Reduced Pressure
example, solvent).
D 2892 Test Method for Distillation of Crude Petroleum
2
3.2.4 initial boiling point (IBP)—the temperature (corre-
(15-Theoretical Plate Column)
sponding to the retention time) at which a cumulative corrected
D 3710 Test Method for Boiling Range Distribution of
3
area count equal to 0.5 % of the total sample area under the
Gasoline and Gasoline Fractions by Gas Chromatography
chromatogram is obtained.
D 4057 Practice for Manual Sampling of Petroleum and
3
3.2.5 final boiling point (FBP)—the temperature (corre-
Petroleum Products
sponding to the retention time) at which a cumulative corrected
D 4626 Practice for Calculation of Gas Chromatographic
3
area count equal to 99.5 % of the total sample area under the
Response Factors
chromatogram is obtained.
3.2.6 slice rate—the time interval used to integrate the
1
This test method is under the jurisdiction of ASTM Committee D02 on
continuous (analog) chromatographic detector response during
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
an analysis. The slice rate is expressed in hertz (for example,
D02.04.0H on Chromatographic Distribution Methods.
Current edition approved Nov. 10, 2002. Published November 2002. Originally integrations or slices per second).
published as D 2887–73. Last previous edition D 2887–01a.
2
Annual Book of ASTM Standards, Vol 05.01.
3 4
Annual Book of ASTM Standards, Vol 05.02. Annual Book of ASTM Standards, Vol 14.02.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D2887–02
NOTE 1—It is not desirable to operate a thermal conductivit
...

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5.1 The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining process, This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
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SCOPE
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1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
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SCOPE
1.1 This test method covers the determination of solvent extractables in petroleum waxes.  
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1.1 This test method covers the determination of the color of refined oils such as undyed motor and aviation gasoline, jet propulsion fuels, naphthas and kerosine, and, in addition, petroleum waxes and pharmaceutical white oils.  
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1.2 This test method reports results specific to this test method and recorded as, “Saybolt Color units.”  
1.3 The values stated in inch-pound units or in SI units and which are not in parentheses are to be regarded as the standard. The values given in parentheses are for information only.  
Note 2: Oil tubes and apparatus used in this test method have traditionally been marked in inches, (the tube is required to be etched with 1/8 in. divisions.) The Saybolt Color Numbers are aligned with inch, 1/2 in., 1/4 in., and 1/8 in. changes in the depth of oil. These fractional inch changes do not readily correspond to SI equivalents and in view of the preponderance of apparatus already in use and marked in inches, the inch/pound unit is regarded as the standard. However the test method does use SI units of length when the length is not directly related to divisions on the oil tube and Saybolt Color Numbers. The test method uses SI units for temperature.  
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ASTM D7152-23(Practice)
Standard Practice for Calculating Viscosity of a Blend of Petroleum Products

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5.1 Predicting the viscosity of a blend of components is a common problem. Both the Wright Blending Method and the ASTM Blending Method, described in this practice, may be used to solve this problem.  
5.2 The inverse problem, predicating the required blend fractions of components to meet a specified viscosity at a given temperature may also be solved using either the Inverse Wright Blending Method or the Inverse ASTM Blending Method.  
5.3 The Wright Blending Methods are generally preferred since they have a firmer basis in theory, and are more accurate. The Wright Blending Methods require component viscosities to be known at two temperatures. The ASTM Blending Methods are mathematically simpler and may be used when viscosities are known at a single temperature.  
5.4 Although this practice was developed using kinematic viscosity and volume fraction of each component, the dynamic viscosity or mass fraction, or both, may be used instead with minimal error if the densities of the components do not differ greatly. For fuel blends, it was found that viscosity blending using mass fractions gave more accurate results. For base stock blends, there was no significant difference between mass fraction and volume fraction calculations.  
5.5 The calculations described in this practice have been computerized as a spreadsheet and are available as an adjunct.3
SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
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ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For specific warning statements, see 7.3.  
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ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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  • Standard
    35 pages
    English language
    sale 15% off