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ASTM D5517-07

(Test Method)

Standard Test Method for Determining Extractability of Metals from Art Materials

Standard Test Method for Determining Extractability of Metals from Art Materials

SIGNIFICANCE AND USE
This acid extraction method is intended to indicate the solubility of metals from art materials in a weak acid medium. This test method may be useful as one indicator of the amount of metal that is readily available for absorption. It is not meant as a replacement for in vivo tests of absorption of a metal.5  
Maximum levels of metal extraction are seen with this test method when results are 250 ppm or less. If results are greater than 250 ppm, the extractant volume should be increased to 100 mL or greater to keep metal levels in the eluate at a level of 5 ppm or less.6
SCOPE
1.1 This test method covers the extraction of metals from art materials using an extractant that simulates the acid potential of gastric juice. This test method is similar to the extraction method in Specification F 963, except that it requires conducting extraction steps at body temperature instead of at room temperature. The extraction procedure specified in this test method is more rigorous than that noted in Specification F 963 because the procedure causes the extraction of a larger quantity of metal.
1.2 This test method is adapted from the European Toy Safety Standard, EN 71-3:1994 but differs from it in that a solvent extraction step is not required for processing waxes or oil-based products and no specific acceptable metal levels are specified.
1.3 The rational for this test method is discussed in .
1.4 This test method should be used on the art material as a whole and not an art material ingredient. Testing the art material as whole would be expected to give a more accurate estimate of soluble metal than from an extrapolation from testing ingredients.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2007
ICS
97.195 - Items of art and handicrafts. Cultural property and heritage
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.57 - Artist Paints and Related Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D5517-03 - Standard Test Method for Determining Extractability of Metals from Art Materials
Effective Date
01-Jun-2007

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ASTM D5517-07 - Standard Test Method for Determining Extractability of Metals from Art Materials
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5517 − 07
StandardTest Method for
1
Determining Extractability of Metals from Art Materials
This standard is issued under the fixed designation D5517; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 Thistestmethodcoverstheextractionofmetalsfromart
D4236 Practice for Labeling Art Materials for Chronic
materialsusinganextractantthatsimulatestheacidpotentialof
Health Hazards
gastric juice. This test method is similar to the extraction
E180 Practice for Determining the Precision of ASTM
method in Specification F963, except that it requires conduct-
Methods for Analysis and Testing of Industrial and Spe-
ing extraction steps at body temperature instead of at room
3
cialty Chemicals (Withdrawn 2009)
temperature. The extraction procedure specified in this test
E456 Terminology Relating to Quality and Statistics
method is more rigorous than that noted in Specification F963
F963 Consumer Safety Specification for Toy Safety
becausetheprocedurecausestheextractionofalargerquantity
4
2.2 International Standards:
of metal.
EN 71-3:1994 Safety of Toys
1.2 This test method is adapted from the European Toy
ISO 3696 Water for Laboratory Use—Specifications
Safety Standard, EN 71-3:1994 but differs from it in that a
ISO 3856 Paints and Varnishes—Determination of
solvent extraction step is not required for processing waxes or
“Soluble” Metal Content
oil-based products and no specific acceptable metal levels are Part 1: Determination of lead content—Flame atomic ab-
specified. sorption spectrometric method and dithiazone spectropho-
tometric method
1.3 The rational for this test method is discussed in Appen-
Part 2: Determination of antimony content—Flame atomic
dix X1.
absorption spectrophotometric method and Rhodamine B
spectrophotometric method
1.4 This test method should be used on the art material as a
Part 3: Determination of barium content—Flame atomic
whole and not an art material ingredient. Testing the art
emission spectrometric method
material as whole would be expected to give a more accurate
Part 4: Determination of cadmium content—Flame atomic
estimate of soluble metal than from an extrapolation from
absorption spectrometric method and polarographic
testing ingredients.
method
1.5 The values stated in SI units are to be regarded as
Part5: Determinationofhexavalentchromiumcontentofthe
standard. No other units of measurement are included in this
pigment portion of the liquid paint or the paint in powder
standard.
form—Diphenylcarbazide spectrophotometric method
Part6: Determinationoftotalchromiumcontentoftheliquid
1.6 This standard does not purport to address all of the
portion of paint—Flame atomic absorption spectrometric
safety concerns, if any, associated with its use. It is the
method
responsibility of the user of this standard to establish appro-
5
2.3 USEPA Standards:
priate safety and health practices and determine the applica-
USEPA Test Method SW-846
bility of regulatory limitations prior to use.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3
The last approved version of this historical standard is referenced on
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint www.astm.org.
4
and Related Coatings, Materials, andApplications and is the direct responsibility of Available from European Committee for Standardization (CEN), 36 rue de
Subcommittee D01.57 on Artist Paints and Related Materials. Stassart, B-1050, Brussels, Belgium, http://www.cenorm.be.
5
CurrenteditionapprovedJune1,2007.PublishedJuly2007.Originallyapproved Available from United States Environmental Protection Association (EPA),
in 1994. Last previous edition approved in 2003 as D5517 – 03. DOI: 10.1520/ Ariel Rios Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460, http://
D5517-07. www.epa.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5517 − 07
6010 Test Method for antimony, arsenic, barium, beryllium, 4. Summary of Test Method
cadmium, chromium, cobalt, copper, lead, manganese,
4.1 Apowdered, liquid, comminuted or ground art material
molybdenum, nickel, selenium, silver, thallium, vana-
is mixed with a 0.07 N hydrochloric acid solution and, after
dium, and zinc
adjusting the pH to 1.5, is shaken for 1 h and th
...

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SIGNIFICANCE AND USE
5.1 This acid extraction method is intended to indicate the solubility of metals from art materials in a weak acid medium. This test method may be useful as one indicator of the amount of metal that is readily available for absorption. It is not meant as a replacement for in vivo tests of absorption of a metal.6 Other relevant information, when available, should be included in the overall toxicological assessment of metal-containing art materials, such as physico-chemical properties, toxicokinetics (absorption, distribution, metabolism and excretion), and mechanisms of toxicity of the metal(s) of interest.  
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1.2 This specification includes requirements for identification and lightfastness.  
1.3 Pastel specimens are exposed to both natural daylight through window glass and window glass-filtered simulated daylight radiation to determine the lightfastness category for each pastel.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Practice for Labeling Ceramic Art Materials for Chronic Adverse Health Hazards

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This practice describes a procedure for developing precautionary labels for ceramic art materials and provides hazard and precautionary statements concerning chronic adverse health hazards known to be associated with a product or product component(s), when the component(s) is present in a physical form, volume, or concentration that in the opinion of a toxicologist has the potential to produce a chronic adverse health effect(s). Precautionary labels covered by this practice are intended for adult usage and does not assure completely the safe use of an art product. This practice does not specify test methods for determining whether a substance or product presents chronic adverse health hazards and does not apply to products appropriately labeled for known chronic adverse health hazards according to chemical substances labeling standards and practices, such as another national consensus standard, existing labeling statutes, regulations, or guidelines. Requirements for the conformance to this practice are given. Determination of labeling and labeling practices such as, signal word, list of potential chronic hazards, name of chronic hazard components, safe handling, instructions, list of sensitizing components, combined statements, information sources, and supplement information are detailed.
SCOPE
1.1 This practice describes a procedure for developing precautionary labels for ceramic art materials and provides hazard and precautionary statements based upon knowledge that exists in the scientific and medical communities. This practice concerns those chronic adverse health hazards known to be associated with a product or product component(s), when the component(s) is present in a physical form, volume, or concentration that in the opinion of a toxicologist has the potential to produce a chronic adverse health effect(s).  
1.2 This practice is intended to apply exclusively to ceramic art materials which are packaged in sizes intended for use by artists or crafts people, either individually, or in a small group or class.  
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1.5 This practice does not apply to products appropriately labeled for known chronic adverse health hazards according to chemical substances labeling standards and practices, such as another national consensus standard, existing labeling statutes, regulations, or guidelines.  
1.6 Since knowledge about chronic adverse health hazards is incomplete and warning cannot cover all uses of any product, it is not possible for precautionary labeling to assure completely safe use of an art product.  
1.7 Manufacturers or repackagers may wish to determine individually or collectively precautionary labeling for ceramic art materials in accordance with this practice. Compliance may be certified by a certifying organization. Guidelines for a certifying organization are given in Appendix X1.  
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.9 This international standard was developed in accordance with international...

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ASTM D6801-07(2021)(Test Method)
Standard Test Method for Measuring Maximum Spontaneous Heating Temperature of Art and Other Materials

SIGNIFICANCE AND USE
5.1 This test method provides a means of accelerating the tendency of a material toward spontaneous heating that may eventually lead to a fire. It is applicable to liquids and pastes.  
5.2 The spontaneous heating behavior of an oil-based material is affected by such factors as the availability of oxygen, the amount of driers present, the degree of polymerization of oils, the surface area of the cellulose material, measures to prevent heat dissipation, and the amount of oil in contact with cellulose material. The degree of spontaneous heating bears little relationship to the type of cellulose material to which an oil-based material comes in contact or whether or not oil soaked materials are first air dried. Small amounts of contaminants, such as oil paint, quartz dust, dirt or drier (for example, materials that might be found on a dirty, oil-soaked rag), can act as catalysts for this reaction.4
SCOPE
1.1 This test method covers a small-scale laboratory procedure to determine the self heating tendency of oil-based materials by exposure to elevated temperatures in air in a controlled semi-adiabatic system.  
1.2 This test method has been developed to address an urgent need to identify oil-based materials that may require labeling for spontaneous heating tendency. Studies based on this test method may allow the development of a practice to identify such oil-based materials.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For safety concerns specific to disposal of solvent-soaked rags, see Appendix X1.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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