ASTM D4283-98(2015)

Standard Test Method for Viscosity of Silicone Fluids

SIGNIFICANCE AND USE
3.1 The viscosity of silicone fluids is typically measured by kinematic viscosity. Test Method D445 describes the basics and background for this measurement. The purpose of this test method is to set forth specific conditions and recommend apparatus for measuring viscosity of silicone fluids.
SCOPE
1.1 This test method covers the measurement of the kinematic viscosity of silicone fluids for polish applications.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

• Status: Historical
• Publication Date: 30-Sep-2015
• ICS: 75.100 - Lubricants, industrial oils and related products
• Technical Committee: D21 - Polishes
• Drafting Committee: D21.02 - Raw Materials

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D4283 − 98 (Reapproved 2015)
Standard Test Method for
1
Viscosity of Silicone Fluids
This standard is issued under the fixed designation D4283; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4.1.2 Ubbelohde Viscometer—up to 100 000 cSt.
4.1.3 Cannon Fenski—up to 5000 cSt.
1.1 This test method covers the measurement of the kine-
matic viscosity of silicone fluids for polish applications. 4.2 Constant Temperature Bath, of 25 6 0.2 °C.
1.2 The values stated in SI units are to be regarded as 4.3 Cleaning Solution for Viscometers, such as toluene,
standard. No other units of measurement are included in this alcoholic KOH.
standard.
4.4 Fluid Standards, for calibrating viscometers.
1.3 This standard does not purport to address all of the
4.5 Stopwatch.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to consult and
5. Preparation of Sample
establish appropriate safety and health practices and deter-
5.1 After charging the fluid to the selected viscometer and
mine the applicability of regulatory limitations prior to use.
placing it in the constant temperature bath, keep in bath for a
2. Referenced Documents
minimum of 15 min to reach the proper temperature level.
2
2.1 ASTM Standards:
6. Calibration and Standardization
D445 Test Method for Kinematic Viscosity of Transparent
6.1 Viscometer Constant (F)—Consult the manufacturer’s
and Opaque Liquids (and Calculation of Dynamic Viscos-
instructions for calibrating individual viscometers.
ity)
3. Significance and Use
7. Procedure
3.1 The viscosity of silicone fluids is typically measured by
7.1 Follow manufacturer’s directions for using their vis-
kinematic viscosity. Test Method D445 describes the basics cometers.
and background for this measurement. The purpose of this test
8. Calculation
method is to set forth specific conditions and recommend
apparatus for measuring viscosity of silicone fluids.
8.1 Calculate the viscosity of silicone fluids as follows:
4. Apparatus
Efflux Time ~s! 3Viscometer Constant ~F! 5 Viscosity ~cSt!
4.1 Viscometer Recommendations:
9. Precision and Bias
4.1.1 Ostwald Viscometer—up to 5000 cSt.
9.1 Precision—Duplicate results by the same operator shall
1
not be cons
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D4283 − 98 (Reapproved 2010) D4283 − 98 (Reapproved 2015)
Standard Test Method for
1
Viscosity of Silicone Fluids
This standard is issued under the fixed designation D4283; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the measurement of the kinematic viscosity of silicone fluids for polish applications.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
3. Significance and Use
3.1 The viscosity of silicone fluids is typically measured by kinematic viscosity. Test Method D445 describes the basics and
background for this measurement. The purpose of this test method is to set forth specific conditions and recommend apparatus for
measuring viscosity of silicone fluids.
4. Apparatus
4.1 Viscometer Recommendations:
4.1.1 Ostwald Viscometer—up to 5000 cSt.
4.1.2 Ubbelohde Viscometer—up to 100 000 cSt.
4.1.3 Cannon Fenski—up to 5000 cSt.
4.2 Constant Temperature Bath, of 25 6 0.2 °C.
4.3 Cleaning Solution for Viscometers, such as toluene, alcoholic KOH.
4.4 Fluid Standards, for calibrating viscometers.
4.5 Stopwatch.
5. Preparation of Sample
5.1 After charging the fluid to the selected viscometer and placing it in the constant temperature bath, keep in bath for a
minimum of 15 min to reach the proper temperature level.
6. Calibration and Standardization
6.1 Viscometer Constant (F)—Consult the manufacturer’s instructions for calibrating individual viscometers.
7. Procedure
7.1 Follow manufacturer’s directions for using their viscometers.
1
This test method is under the jurisdiction of ASTM Committee D21 on Polishes and is the direct responsibilit
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