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ASTM D5248-04(2010)

(Specification)

Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane

Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane

ABSTRACT
This specification covers the three grades of 1,1,2- trichloro 1,2,2 trifluoroethane typically needed in various industries. This may be a reference for 1,1,2-trichloro 1,2,2- trifluoroethane recovery programs. The three classifications are as follows: Type I - generally recognized for use in precision applications; Type II - used for less demanding precision applications; and Type III - general-purpose technical grade. Materials shall be tested and the individual grades shall conform to specified values of specific gravity, chloride content, acid number, non-volatile residue content, water content, 1,1,2-trichloro 1,2,2- trifluoroethane content, 1,1,1- trichloroethane content, color, and appearance.
SCOPE
1.1 This specification covers the three grades of 1,1,2-trichloro 1,2,2-trifluoroethane typically needed in various industries. It may be used as a reference document by purchasers or by persons establishing in-house, 1,1,2-trichloro 1,2,2-trifluoroethane recovery programs.

General Information

Status
Historical
Publication Date
31-Jan-2010
ICS
71.080.10 - Aliphatic hydrocarbons
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.02 - Vapor Degreasing
Current Stage
Ref Project

Relations

Replaces
ASTM D5248-04 - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
Effective Date
01-Feb-2010
Replaced By
ASTM D5248-04(2015) - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
Effective Date
01-Jun-2015

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ASTM D5248-04(2010) - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-TrifluoroethaneASTM D5248-04(2010) - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
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Technical specification
ASTM D5248-04(2010) - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5248 −04(Reapproved 2010)
Standard Specification for
1
Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
This standard is issued under the fixed designation D5248; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D3401 Test Methods for Water in Halogenated Organic
Solvents and Their Admixtures
1.1 This specification covers the three grades of 1,1,2-
2 D3443 Test Method for Chloride in Trichlorotrifluoroethane
trichloro 1,2,2-trifluoroethane typically needed in various
D3444 Test Method for Total Acid Number of Trichlorotri-
industries. It may be used as a reference document by purchas-
fluoroethane
ers or by persons establishing in-house, 1,1,2-trichloro 1,2,2-
D3741 Test Methods for Appearance of Admixtures Con-
trifluoroethane recovery programs.
taining Halogenated Organic Solvents
D6806 Practice for Analysis of Halogenated Organic Sol-
2. Referenced Documents
vents and Their Admixtures by Gas Chromatography
3
2.1 ASTM Standards:
D1064 Test Methods for Iron in Rosin Tall Oil Fatty Acids
3. Classification
4
and Other Related Products (Withdrawn 2002)
3.1 Type I—Generally recognized for use in precision ap-
D2108 Test Method for Color of Halogenated Organic
plications.
Solvents and Their Admixtures (Platinum-Cobalt Scale)
3.2 Type II—Use for less demanding precision applications.
D2109 Test Methods for Nonvolatile Matter in Halogenated
Organic Solvents and Their Admixtures
3.3 Type III—General-purpose technical grade.
D2111 Test Methods for Specific Gravity and Density of
Halogenated Organic Solvents and Their Admixtures 4. Properties
4.1 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type I
shall meet the requirements prescribed in Table 1.
1
This specification is under the jurisdiction of ASTM Committee D26 on
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
4.2 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type II
responsibility of Subcommittee D26.02 on Vapor Degreasing.
shall meet the requirements prescribed in Table 2.
Current edition approved Feb. 1, 2010. Published March 2010. Originally
approved in 1992. Last previous edition approved in 2004 as D5248 – 04. DOI:
4.3 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type III
10.1520/D5248-04R10.
shall meet the requirements prescribed in Table 3.
2
1,1,2-trichloro 1,2,2-trifluoroethane: CAS No. 76-13-1.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
5. Keywords
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
5.1 1,1,2-trichloro 1,2,2-trifluoroethane ; CFC 113; Type I;
the ASTM website.
4 Type II; Type II
...

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ABSTRACT
This specification covers the three grades of 1,1,2- trichloro 1,2,2 trifluoroethane typically needed in various industries. This may be a reference for 1,1,2-trichloro 1,2,2- trifluoroethane recovery programs. The three classifications are as follows: Type I - generally recognized for use in precision applications; Type II - used for less demanding precision applications; and Type III - general-purpose technical grade. Materials shall be tested and the individual grades shall conform to specified values of specific gravity, chloride content, acid number, non-volatile residue content, water content, 1,1,2-trichloro 1,2,2- trifluoroethane content, 1,1,1- trichloroethane content, color, and appearance.
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ASTM D7266-23(Test Method)
Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (External Standard)

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5.1 This test method is suitable for setting specifications on the materials referenced in Table 1 and for use as an internal quality control tool where cyclohexane is produced or is used in a manufacturing process. It may also be used in development or research work involving cyclohexane.  
5.2 This test method is useful in determining the purity of cyclohexane with normal impurities present. If extremely high boiling or unusual impurities are present in the cyclohexane, this test method would not necessarily detect them and the purity calculation would be erroneous.
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1.1 This test method covers the determination of the purity of cyclohexane by gas chromatography.  
1.2 This test method is applicable to the measurement of impurities in Table 1. This test method is applicable to samples with concentrations to 400 mg/kg, but may be applicable to a wider range. The limit of detection (LOD) is 1 mg/kg and the limit of quantitation (LOQ) is 3 mg/kg for benzene.
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1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Analysis of Cyclohexane by Gas Chromatography (Effective Carbon Number)

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5.1 This test method is suitable for setting specifications on the materials referenced in Table 1 and for use as an internal quality control tool where cyclohexane is produced or is used in a manufacturing process. It may also be used in development or research work involving cyclohexane.  
5.2 This test method is useful in determining the purity of cyclohexane with normal impurities present. If extremely high boiling or unusual impurities are present in the cyclohexane, this test method would not necessarily detect them and the purity calculation would be erroneous.
SCOPE
1.1 This test method covers the determination of the purity of cyclohexane by gas chromatography.  
1.2 This test method has been found applicable to the measurement of impurities such as those found in Table 1, which are impurities that may be found in cyclohexane. The impurities can be analyzed over a range with an upper limit of 400 mg/kg by this method, but may be applicable to a wider range. The limit of detection (LOD) is 0.7 mg/kg and the limit of quantitation (LOQ) is 2.3 mg/kg.
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5.1 High-purity propylene is required as a feedstock for various manufacturing processes, and the presence of trace amounts of certain hydrocarbon impurities may have adverse effects on yield or catalyst life. This test method is suitable for use as a benchmark in setting commercial specifications, for use as an internal quality control tool, and for use in development or research work.
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SCOPE
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