ASTM D421-85(2007)
(Practice)Standard Practice for Dry Preparation of Soil Samples for Particle-Size Analysis and Determination of Soil Constants (Withdrawn 2016)
Standard Practice for Dry Preparation of Soil Samples for Particle-Size Analysis and Determination of Soil Constants (Withdrawn 2016)
SIGNIFICANCE AND USE
This practice can be used to prepare samples for particle-size and plasticity tests where it is desired to determine test values on air-dried samples, or where it is known that air drying does not have an effect on test results relative to samples prepared in accordance with Practice D 2217.
SCOPE
1.1 This practice covers the dry preparation of soil samples as received from the field for particle-size analysis and the determination of the soil constants.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This practice covers the dry preparation of soil samples as received from the field for particle-size analysis and the determination of the soil constants.
Formerly under the jurisdiction of Committee D18 on Soil and Rock, this practice was withdrawn in January 2016 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D421 − 85 (Reapproved2007)
Standard Practice for
Dry Preparation of Soil Samples for Particle-Size Analysis
and Determination of Soil Constants
This standard is issued under the fixed designation D421; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 4.3 Sieves—A series of sieves, of square mesh woven wire
cloth, conforming to Specification E11.The sieves required are
1.1 This practice covers the dry preparation of soil samples
as follows:
as received from the field for particle-size analysis and the
No. 4 (4.75-mm)
determination of the soil constants.
No. 10 (2.00-mm)
1.2 This standard does not purport to address all of the
No. 40 (425-µm)
safety concerns, if any, associated with its use. It is the
4.4 Sampler—A riffle sampler or sample splitter, for quar-
responsibility of the user of this standard to establish appro-
tering the samples.
priate safety and health practices and determine the applica-
5. Sampling
bility of regulatory limitations prior to use.
5.1 Expose the soil sample as received from the field to the
2. Referenced Documents
air at room temperature until dried thoroughly. Break up the
aggregations thoroughly in the mortar with a rubber-covered
2.1 ASTM Standards:
pestle. Select a representative sample of the amount required to
D2217 Practice for Wet Preparation of Soil Samples for
perform the desired tests by the method of quartering or by the
Particle-Size Analysis and Determination of Soil Con-
use of a sampler. The amounts of material required to perform
stants
the individual tests are as follows:
E11 Specification for Woven Wire Test Sieve Cloth and Test
5.1.1 Particle-Size Analysis—For the particle-size analysis,
Sieves
material passing a No. 10 (2.00-mm) sieve is required in
amounts equal to 115 g of sandy soils and 65 g of either silt or
3. Significance and Use
clay soils.
3.1 This practice can be used to prepare samples for
5.1.2 Tests for Soil Constants—For the tests for soil
particle-size and plasticity tests where it is desired to determine
constants, material passing the No. 40 (425-µm) sieve is
test values on air-dried samples, or where it is known that air
required in total amount of 220 g, allocated as follows:
dryingdoesnothaveaneffectontestresultsrelativetosamples
Test Grams
prepared in accordance with Practice D2217.
Liquid limit 100
Plastic limit 15
4. Apparatus
Centrifuge moisture equivalent 10
Volumetric shrinkage 30
4.1 Balance, sensitive to 0.1 g.
Check tests 65
4.2 Mortar and Rubber-Covered Pestle , suitable for break-
6. Preparation of Test Sample
ing up the aggregations of soil particles.
6.1 Select that portion of the air-dried sample selected for
purposeoftestsandrecordthemassasthemassofthetotaltest
sample uncorrected for hygroscopic moisture. Separate the test
This practice is under the jurisdiction of ASTM Committee D18 on Soil and
sample by sieving with a No. 10 (2.00-mm) sieve. Grind that
Rock and is the direct res
...
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1.1 This test method covers the determination of specific gravity and absorption of rock for erosion control. The specific gravity may be expressed as bulk specific gravity or apparent specific gravity. Bulk specific gravity and absorption are based on a 24 ± 4-h soaking time for the rock specimens tested. This test is appropriate for breakwater stone, armor stone, riprap, and gabion sized rock materials, or similar.
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5.1 The meaning of the test is related to the manufacturing and end use of the material, to determine characteristics of products.
5.2 A manufacturer of raw psyllium will base the grade of psyllium produced on multiple properties of which swell volume is one.
5.3 Erosion control contractors and those writing erosion control specifications will use this test method to evaluate the grade of psyllium being used as a hydraulically applied erosion control product. The swell volume will help determine the application rate of psyllium needed to meet the erosion control performance criteria.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 The purpose of this quantitative test method is to provide a means of determining the swell volume plantago insularis (Ovata, Psyllium).
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1.3 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
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5.1 Hydraulically operated stationary piston samplers are used to gather soil samples for laboratory or field testing and analysis for geologic investigations, soil chemical composition studies, and water quality investigations. The sampler is sometimes used when attempts to recover unstable soils with thin-walled tubes, Practice D1587/D1587M, are unsuccessful. Examples of a few types of investigations in which hydraulic stationary piston samplers may be used include building site foundation studies containing soft sediments, highway and dam foundation investigations where softer soil formation need evaluation, wetland crossings utilizing floating structures, and hazardous waste site investigations. Hydraulically operated stationary piston samplers provide specimens necessary to determine the physical and chemical composition of soils and, in certain circumstances, contained pore fluids (see Guide D6169/D6169M).
5.2 Hydraulically operated stationary piston samplers can provide relatively intact soil samples of soft or loose formation materials for testing to determine accurate information on the physical characteristics of that soil. Samples of soft formation materials can be tested to determine numerous soil characteristics such as; soil stratigraphy, particle size, water content, permeability, shear strength, compressibility, and so forth. The chemical composition of soft formation soils can also be determined from the sample if provisions are made to ensure that clean, decontaminated tools are used in the sample gathering procedure. Field-extruded samples can be field-screened or laboratory-analyzed to determine the chemical composition of soil and contained pore fluids. Using sealed or protected sampling tools, cased boreholes, and proper advancement techniques can help in the acquisition of good representative samples. A general knowledge of subsurface conditions at the site is beneficial.
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1.1 This practice covers a procedure for sampling of cohesive, organic, or fine-grained soils, or combination thereof, using a thin-walled metal tube that is inserted into the soil formation by means of a hydraulically operated piston. It is used to collect relatively intact soil samples suitable for laboratory tests to determine structural and chemical properties for geotechnical and environmental site characterizations.
1.1.1 Guidance on preservation and transport of samples in accordance with Practice D4220/D4220M may apply. Samples for classification may be preserved using procedures similar to Class A. In most cases, a thin-walled tube sample can be considered as Class B, C, or D. Refer to Guide D6169/D6169M for use of the hydraulically operated stationary piston soil sampler for environmental site characterization. This sampling method is often used in conjunction with rotary drilling methods such as fluid rotary; Guide D5783; and hollow stem augers, Practice D6151/D6151M. Sampling data shall be reported in the field log in accordance with Guide D5434.
1.2 The hydraulically operated stationary piston sampler is limited to soils and unconsolidated materials that can be penetrated with the available hydraulic pressure that can be applied without exceeding the structural strength of the thin-walled tube. This standard addresses typical hydraulic piston samplers used on land or shallow water in drill holes. The standard does not address specialized offshore samplers for deep marine applications that may or may not be hydraulically operated. This standard does not address operation of other types of mechanically advanced piston samplers. For information on other soil samplers, refer to Guide D6169/D6169M.
1.3 Units—The values stated in either inch-pound units or SI units [presented in brackets] are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, e...
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SIGNIFICANCE AND USE
5.1 This test method utilizes large-scale testing equipment and procedures established at a variety of testing laboratories over the last 30 years.
5.2 This method is useful in evaluating ECPs and their installation to reduce soil loss and sediment concentrations when exposed to defined rainfall conditions and improving water quality exiting the area disturbed by earthwork activity by reducing suspended solids and turbidity.
5.3 This test method is a performance test, but can also be used for acceptance testing to determine product conformance to project specifications. For project-specific conformance, unique project-specific conditions should be considered. Caution is advised since information regarding laboratory specific precision is incomplete at this time, and differences in soil and other environmental and geotechnical conditions may affect ECP performance.
5.4 This standard can also be used as a comparative tool for evaluating the erosion control characteristics of different ECPs and can also be used to gain agency approvals.
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SCOPE
1.1 This test method is used to evaluate the ability of erosion control products (ECP) to protect slopes from rainfall-induced erosion using an adjustable tilting bed slope. The standard slopes range from 2.5:1 to 4:1 (H:V) having target rainfall intensities between 4.0 and 5.0 in./h [100 and 125 mm/h].
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4.2 The basic criteria provided by this practice is intended to be supplemented by more specific criteria serving the requirements of the certification organization.
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1.1 This practice provides a guide for evaluation and certification procedures for personnel engaged in testing soil and rock in accordance with ASTM test methods and is intended for use by independent organizations providing certification services.
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5.3 The change in mass of RECPs submerged in water may vary considerably depending on the composition of the materials used in the product or due to inconsistency within the product. This test method enables the characterization and control of product consistency.
5.4 This test method may be used to determine the effect of different component materials and makeup of RECPs on the change in mass when submerged in water.
5.5 This test method may be used for acceptance testing of commercial shipments of RECPs. Comparative tests as directed in 5.6 may be advisable.
5.6 In case of a dispute arising from differences in reported test results when using this test method for acceptance testing of commercial shipments, the purchaser and the supplier shall conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the evaluation of bias. As a minimum, the two parties shall take a group of test specimens that are as homogeneous as possible and that are formed from a lot of material of the type in question. The test specimens shall be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories shall be compared using Student’s t-test for unpaired date and an acceptable probability level ch...
SCOPE
1.1 This test method measures the change in mass of a rolled erosion control product when specimens are submerged in water for a prescribed period of time. The change in mass is reported as a percentage of the original dry mass of the specimen.
1.2 Units—The values stated in either SI units or inch-pound units [given in brackets] are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
1.2.1 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This practice implicitly combines two separate systems of units; that is, the absolute system and the gravitational system. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit of mass. However, the use of balances and scales recording pounds of mass (lbf) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.
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1.3.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for t...
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SIGNIFICANCE AND USE
5.1 Test methods A and B are used to estimate the permanganate natural oxidant demand exerted by the soil or aquifer solids by determining the quantity of potassium permanganate that is consumed by naturally occurring species as a function of time. Test Method C is used to estimate the permanganate total oxidant demand exerted by soil, aquifer solids, chemical contaminants or any other reduced species by determining the quantity of potassium permanganate that is consumed by all components of the bulk aquifer as a function of time. Typically, the measurement of oxidant demand is used to screen potential sites for in situ chemical oxidation (ISCO) with permanganate (Test Methods A and C) and provide information to aid in the design of remediation systems (Test Methods B and C).
5.2 While some oxidizable species react relatively quickly (that is, days to weeks), others react more slower (weeks to months). Consequently, the PNODt is expected to be some fraction of the PNODmax.
5.3 For ISCO injection applications, the PNOD may overestimate the demand exerted due to mass transport related issues. For soil blending applications, the PNOD is a more accurate measure of the demand exerted due to better mass to oxidant contact.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/and so forth.
SCOPE
1.1 These test methods cover the estimation of the permanganate natural oxidant demand (PNOD) through the determination of the quantity of potassium permanganate (KMnO4) that organic matter and other naturally occurring oxidizable species present in soil or aquifer solids will consume under specified conditions as a function of time. Oxidizable species may include organic constituents and oxidizable inorganic ions, such as ferrous iron and sulfides. The following test methods are included:
Test Method A—48-hour Permanganate Natural Oxidant Demand
Test Method B—Permanganate Natural Oxidant Demand Kinetics
Test Method C—Permanganate Total Oxidant Demand
1.2 These test methods are limited by the reagents employed to a permanganate natural oxidant demand (PNOD) of 40 g KMnO4 per kg soil or aquifer solids after a period of 48 hours (Methods A and C) or two weeks (Method B).
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to interpret the results of the data. It is the responsibility of the user of this standard to interpret the results obtained and to determine the applicability of these results prior to use.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
- Standard6 pagesEnglish languagesale 15% off
- Standard6 pagesEnglish languagesale 15% off
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