ASTM D5248-04(2015)

Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane

ABSTRACT
This specification covers the three grades of 1,1,2- trichloro 1,2,2 trifluoroethane typically needed in various industries. This may be a reference for 1,1,2-trichloro 1,2,2- trifluoroethane recovery programs. The three classifications are as follows: Type I - generally recognized for use in precision applications; Type II - used for less demanding precision applications; and Type III - general-purpose technical grade. Materials shall be tested and the individual grades shall conform to specified values of specific gravity, chloride content, acid number, non-volatile residue content, water content, 1,1,2-trichloro 1,2,2- trifluoroethane content, 1,1,1- trichloroethane content, color, and appearance.
SCOPE
1.1 This specification covers the three grades of 1,1,2-trichloro 1,2,2-trifluoroethane2 typically needed in various industries. It may be used as a reference document by purchasers or by persons establishing in-house, 1,1,2-trichloro 1,2,2-trifluoroethane recovery programs.

General Information

• Status: Historical
• Publication Date: 31-May-2015
• ICS: 71.080.10 - Aliphatic hydrocarbons
• Technical Committee: D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
• Drafting Committee: D26.02 - Vapor Degreasing

Relations

• Replaces: ASTM D5248-04(2010) - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
• Effective Date: 01-Jun-2015
• Replaced By: ASTM D5248-04(2020) - Standard Specification for Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
• Effective Date: 01-Apr-2020

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5248 −04 (Reapproved 2015)
Standard Specification for
1
Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
This standard is issued under the fixed designation D5248; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D3401 Test Methods for Water in Halogenated Organic
Solvents and Their Admixtures
1.1 This specification covers the three grades of 1,1,2-
2 D3443 Test Method for Chloride in Trichlorotrifluoroethane
trichloro 1,2,2-trifluoroethane typically needed in various
D3444 Test Method for Total Acid Number of Trichlorotri-
industries. It may be used as a reference document by purchas-
fluoroethane
ers or by persons establishing in-house, 1,1,2-trichloro 1,2,2-
D3741 Test Methods for Appearance of Admixtures Con-
trifluoroethane recovery programs.
taining Halogenated Organic Solvents
D6806 Practice for Analysis of Halogenated Organic Sol-
2. Referenced Documents
3 vents and Their Admixtures by Gas Chromatography
2.1 ASTM Standards:
D1064 Test Methods for Iron in Rosin Tall Oil Fatty Acids
3. Classification
4
and Other Related Products (Withdrawn 2002)
3.1 Type I—Generally recognized for use in precision ap-
D2108 Test Method for Color of Halogenated Organic
plications.
Solvents and Their Admixtures (Platinum-Cobalt Scale)
3.2 Type II—Use for less demanding precision applications.
D2109 Test Methods for Nonvolatile Matter in Halogenated
Organic Solvents and Their Admixtures
3.3 Type III—General-purpose technical grade.
D2111 Test Methods for Specific Gravity and Density of
4. Properties
Halogenated Organic Solvents and Their Admixtures
4.1 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type I
1 shall meet the requirements prescribed in Table 1.
This specification is under the jurisdiction of ASTM Committee D26 on
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
4.2 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type II
responsibility of Subcommittee D26.02 on Vapor Degreasing.
shall meet the requirements prescribed in Table 2.
Current edition approved June 1, 2015. Published June 2015. Originally
approved in 1992. Last previous edition approved in 2010 as D5248 – 04(2010).
4.3 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type III
DOI: 10.1520/D5248-04R15.
2
shall meet the requirements prescribed in Table 3.
1,1,2-trichloro 1,2,2-trifluoroethane: CAS No. 76-13-1.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
5. Keywords
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
5.1 1,1,2-trichloro 1,2,2-trifluoroethane; CFC 113; Type I;
the ASTM website.
4
Type II; Type III
The last approved version of thi
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5248 − 04 (Reapproved 2010) D5248 − 04 (Reapproved 2015)
Standard Specification for
1
Reclaimed 1,1,2-Trichloro 1,2,2-Trifluoroethane
This standard is issued under the fixed designation D5248; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
2
1.1 This specification covers the three grades of 1,1,2-trichloro 1,2,2-trifluoroethane typically needed in various industries. It
may be used as a reference document by purchasers or by persons establishing in-house, 1,1,2-trichloro 1,2,2-trifluoroethane
recovery programs.
2. Referenced Documents
3
2.1 ASTM Standards:
4
D1064 Test Methods for Iron in Rosin Tall Oil Fatty Acids and Other Related Products (Withdrawn 2002)
D2108 Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
D2109 Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures
D2111 Test Methods for Specific Gravity and Density of Halogenated Organic Solvents and Their Admixtures
D3401 Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
D3443 Test Method for Chloride in Trichlorotrifluoroethane
D3444 Test Method for Total Acid Number of Trichlorotrifluoroethane
D3741 Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents
D6806 Practice for Analysis of Halogenated Organic Solvents and Their Admixtures by Gas Chromatography
3. Classification
3.1 Type I—Generally recognized for use in precision applications.
3.2 Type II—Use for less demanding precision applications.
3.3 Type III—General-purpose technical grade.
4. Properties
4.1 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type I shall meet the requirements prescribed in Table 1.
4.2 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type II shall meet the requirements prescribed in Table 2.
4.3 Reclaimed 1,1,2-trichloro 1,2,2-trifluoroethane Type III shall meet the requirements prescribed in Table 3.
5. Keywords
5.1 1,1,2-trichloro 1,2,2-trifluoroethane ; 1,2,2-trifluoroethane; CFC 113; Type I; Type II; Type III
1
This specification is under the jurisdiction of ASTM Committee D26 on Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct responsibility
of Subcommittee D26.02 on Vapor Degreasing.
Current edition approved Feb. 1, 2010June 1, 2015. Published March 2010June 2015. Originally approved in 1992. Last previous edition approved in 20042010 as
D5248 – 04.D5248 – 04(2010). DOI: 10.1520/D5248-04R10.10.1520/D5248-04R15.
2
1,1,2-trichloro 1,2,2-trifluoroethane: CAS No. 76-13-1.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
4
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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D5248 − 04 (2015)
TABLE 1 Physical Properties Type I
Test
Property Specification
Method
Specific Gravity, 20/20 1.54 to 1.57 D2111
Chloride, ppm, max 0.1 D3443
Acid number 0.003 D3444
Non-volatile residue, ppm, max 10 D2109
Water, ppm, max 25 D3401 or
D1064
1,1,2-trichloro 1,2,2-trifluoroethane content,
wt %, min 99.5 D6806
1,1,1-trichloroethane content, 0.02 D6806
wt %, max
Color, Pt-Co, max 10 D2108
Appearance clear and free from D3741
suspended matter
TABLE 1 Physical Properties Type I
Test
Property Specification
Method
Specific Gravity, 20/20 1.54 to 1.57 D2111
Chloride, ppm, max 0.1 D3443
Acid number 0.003 D3444
Non-volatile residue, ppm, max 10 D2109
Water, ppm, max 25 D3401 or
D1064
1,1,2-trichloro 1,2,2-trifluoroethane
content, wt %, min 99.5 D6806
1,1,1-trichloroethane content, 0.02 D6806
wt %, max
Color, Pt-Co, max 10 D2108
Appearance clear and free from D3741
suspended matter
TABLE 2 Physical Properties Type II
Test
Property Specification
Method
Specific Gravity, 20/20 1.53 to 1.57 D2111
Chloride, ppm, max 0.2 D3443
Acid number not tested D3444
Non-volatile residue, ppm, max 20 D2109
Water, ppm, max 50 D3401 or
D1064
1,1,2-trichloro 1,2,2-trifluoroethane content,
wt %, min 99.0 D6806
1,1,1-trichloroethane content, 0.05 D6806
wt %, max
Color, Pt
...