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ASTM D4811-04

(Specification)

Standard Specification for Nonvulcanized (Uncured) Rubber Sheet Used as Roof Flashing

Standard Specification for Nonvulcanized (Uncured) Rubber Sheet Used as Roof Flashing

SCOPE
1.1 This specification covers nonvulcanized (uncured) rubber sheet made of EPDM (ethylene-propylene-diene terpolymer) or CR (polychloroprene) intended for use as watertight roof flashing exposed to the weather.
1.2 The tests and property limits used to characterize these flashing materials are specific for each classification and are minimum values to make the product fit for its intended purpose.
1.3 SI units shall be used in referee decisions.
1.4 In-place roof system design criteria, such as fire resistance, field seaming strength, material compatibility, and uplift resistance, among others, are beyond the scope of this specification.
1.5 The following precautionary caveat pertains to the test methods portion only, Section 8, of this specification:This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address the safety concerns associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-2003
ICS
83.060 - Rubber
91.100.50 - Binders. Sealing materials
Technical Committee
D08 - Roofing and Waterproofing
Drafting Committee
D08.18 - Nonbituminous Organic Roof Coverings
Current Stage
Ref Project

Relations

Replaces
ASTM D4811-97 - Standard Specification for Nonvulcanized Rubber Sheet Used as Roof Flashing
Effective Date
01-Jan-2004
Replaced By
ASTM D4811-06 - Standard Specification for Nonvulcanized (Uncured) Rubber Sheet Used as Roof Flashing
Effective Date
01-Dec-2006

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ASTM D4811-04 - Standard Specification for Nonvulcanized (Uncured) Rubber Sheet Used as Roof FlashingASTM D4811-04 - Standard Specification for Nonvulcanized (Uncured) Rubber Sheet Used as Roof Flashing
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ASTM D4811-04 - Standard Specification for Nonvulcanized (Uncured) Rubber Sheet Used as Roof Flashing
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 4811 – 04
Standard Specification for
Nonvulcanized (Uncured) Rubber Sheet Used as Roof
1
Flashing
This standard is issued under the fixed designation D4811; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D573 TestMethodsforRubber—DeteriorationinAirOven
D624 Test Method for Tear Strength of Conventional
1.1 This specification covers nonvulcanized (uncured) rub-
Vulcanized Rubber and Thermoplastic Elastomers
ber sheet made of EPDM (ethylene-propylene-diene terpoly-
D1079 Terminology Relating to Roofing, Waterproofing,
mer) or CR (polychloroprene) intended for use as watertight
and Bituminous Materials
roof flashing exposed to the weather.
D1149 Test Method for Rubber Deterioration—Surface
1.2 The tests and property limits used to characterize these
Ozone Cracking in a Chamber
flashing materials are specific for each classification and are
D1204 Test Method for Linear Dimensional Changes of
minimum values to make the product fit for its intended
Nonrigid Thermoplastic Sheeting or Film at Elevated
purpose.
Temperatures
1.3 SI units shall be used in referee decisions.
D 1418 Practice for Rubber and Rubber Latices—
1.4 In-place roof system design criteria, such as fire resis-
Nomenclature
tance, field seaming strength, material compatibility, and uplift
D2137 Test Methods for Rubber Property—Brittleness
resistance, among others, are beyond the scope of this speci-
Point of Flexible Polymers and Coated Fabrics
fication.
D3182 Practice for Rubber—Materials, Equipment, and
1.5 The following precautionary caveat pertains to the test
Procedures for Mixing Standard Compounds and Prepar-
methods portion only, Section 8, of this specification: This
ing Standard Vulcanized Sheets
standard may involve hazardous materials, operations, and
G151 Practice for Exposing Nonmetallic Materials in Ac-
equipment. This standard does not purport to address the
celerated Test Devices that Use Laboratory Light Sources
safety concerns associated with its use. It is the responsibility
G154 Practice for Operating Fluorescent Light Apparatus
of the user of this standard to establish appropriate safety and
for UV Exposure of Nonmetallic Materials
health practices and determine the applicability of regulatory
G155 Practice for Operating Xenon Arc Light Apparatus
limitations prior to use.
for Exposure of Non-Metallic Materials
2. Referenced Documents
3. Classification
2
2.1 ASTM Standards:
3.1 The following types are used to identify the principal
D412 Test Methods for Vulcanized Rubber and Thermo-
polymer components of the flashing material (see Note 1):
plastic Elastomers—Tension
3.1.1 Type I—Ethylene-Propylene-Diene Terpolymer
D471 Test Methods for Rubber Property—Effect of Liq-
(EPDM).
uids
3.1.2 Type II—Chloroprene Polymer (CR).
D518 Test Method for Rubber Deterioration—Surface
Cracking
NOTE 1—For definitions of polymer types, see Practice D1418. For
definitions of terms related to roofing, see Terminology D1079.
1
3.2 The following classes describe the ability to vulcanize
This specification is under the jurisdiction of ASTM Committee D08 on
RoofingandWaterproofingandisthedirectresponsibilityofSubcommitteeD08.18
on the roof:
on Nonbituminous Organic Roof Coverings.
3.2.1 Class V—Vulcanizing.
Current edition approved Jan. 1, 2004. Published January 2004. Originally
3.2.2 Class NV—Nonvulcanizing.
approved in 1990. Last previous edition approved in 1997 as D4811–97.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
NOTE 2—Class V compounds continue to vulcanize (that is, cure) after
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
emplacement on the roof. Class NV indicates non-vulcanizable com-
Standards volume information, refer to the standard’s Document Summary page on
pounds.
the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D4811–04
TABLE 2 Property Requirements for Flashing After Vulcanization
4. Materials and Manufacture
Type I, Type II,
4.1 The flashing material shall be formulated from the
Class V Class V
appropriate polymer type and other compounding ingredients.
Vulcanization, at 160°C (320°F), min 20 6220 6 2
The principal polymer in the flashing material shall be one of
Tensile Strength, min, MPa (psi) 9.0 (1305) 8.3 (1205)
those listed in 3.1 and greater than 95% of the total polymer.
Elongation, min, % 300 250
Tear Resistance, min, kN/m (lb/in.) 22 (125) 22 (125)
4.2 The flashing material shall be capable of being bonded
Britt
...

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This specification covers nonvulcanized (uncured) rubber sheet made of ethylene-propylene-diene terpolymer (EPDM) or polychloroprene (CR) intended for use as watertight roof flashing exposed to the weather. In-place roof system design criteria such as fire resistance, field seaming strength, material compatibility, and uplift resistance, among others, are beyond the scope of this specification. The flashing material shall be formulated from the appropriate polymer type and other compounding ingredients, and shall be capable of being bonded to itself, to the roofing membrane, and to substrate for making watertight field splices and repairs. Property requirements for flashing before vulcanization include thickness, Green strength modulus, ultimate elongation, shelf stability, vulcanizability, tensile strength and set, dimensional stability, and weatherability. Consequently, the property requirements for flashing after vulcanization includes tensile strength and set, elongation, tear resistance, brittle point, ozone resistance, air oven heat aging, water absorption and weight change, linear dimension change, and weatherability.
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1.1 This specification covers flexible sheet made from ethylene-propylene-diene terpolymer (EPDM) intended for use in single-ply roofing membranes exposed to the weather. The tests and property limits used to characterize the sheet are values to ensure minimum quality for the intended use. The sheet may be non-reinforced, fabric- or scrim-reinforced, or fabric-backed vulcanized rubber sheet.  
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4.1 Designers and installers of waterproofing systems may consult this guide for a discussion of important elements of the use of cold liquid-applied waterproofing membranes and associated elements of construction. This guide is not intended to serve as a specification for waterproofing installation.  
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This specification describes the required properties and test methods for high-solids content, cold liquid-applied elastomeric membrane with integral wearing surface for waterproofing building decks not subject to hydrostatic pressure. This specification does not include specific requirements for skid resistance or fire retardance, although both may be important in specific uses. The properties to which the materials will be tested upon for conformance are as follows: weight loss of base coat; low temperature crack bridging; adhesion-in-peel to cement mortar and plywood substrates after water immersion; chemical resistance after water, ethylene glycol, and mineral spirits exposure; weathering resistance, recovery from elongation, tensile retention, and elongation retention; abrasion resistance; and stability.
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ABSTRACT
This specification covers nonvulcanized (uncured) rubber sheet made of ethylene-propylene-diene terpolymer (EPDM) or polychloroprene (CR) intended for use as watertight roof flashing exposed to the weather. In-place roof system design criteria such as fire resistance, field seaming strength, material compatibility, and uplift resistance, among others, are beyond the scope of this specification. The flashing material shall be formulated from the appropriate polymer type and other compounding ingredients, and shall be capable of being bonded to itself, to the roofing membrane, and to substrate for making watertight field splices and repairs. Property requirements for flashing before vulcanization include thickness, Green strength modulus, ultimate elongation, shelf stability, vulcanizability, tensile strength and set, dimensional stability, and weatherability. Consequently, the property requirements for flashing after vulcanization includes tensile strength and set, elongation, tear resistance, brittle point, ozone resistance, air oven heat aging, water absorption and weight change, linear dimension change, and weatherability.
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Standard Test Method for Adhesion-in-Peel of Elastomeric Joint Sealants

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5.1 There are differences in opinion among those concerned with sealant technology whether or not this adhesion-in-peel test simulates the type of strain and e-tensile stresses encountered by a sealant in normal use. Nevertheless, this test provides a valuable measurement of the ability of the cured sealant to maintain a bond to the substrate under severe peel conditions.  
5.2 Many sealant manufacturers utilize the adhesion-in-peel test for determining the adhesive characteristics of sealant/primer combinations with unusual or proprietary substrates. This test is especially useful for quality measurements comparing batches of the same sealant relative to adhesion or for studying adhesion of a given sealant to a variety of substrates.  
5.3 This test method alone is not appropriate for comparing the overall performance of different sealants in a given application. The adhesive force that determines if a given sealant is useful in a given application also depends on the modulus of elasticity and the degree to which the sealant will be strained. This test, as it exists, does not consider the modulus of elasticity, nor amount of stress that will be produced by a given strain in an actual sealant in a moving joint. No known correlations are given to relate and apply modulus values to the peel values.  
5.4 This test requires that the results indicate whether the failure mode is primarily adhesive or cohesive. It is important to note that a cohesive failure is not necessarily better than an adhesive failure, if the adhesive value is sufficient for the application. Having adhesive failure allows one to study the change of adhesion with time and with the various stress conditions.
SCOPE
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1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 The committee with jurisdiction over this standard is not aware of any comparable standards published by other organizations.  
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1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C661-15(2022)(Test Method)
Standard Test Method for Indentation Hardness of Elastomeric-Type Sealants by Means of a Durometer

SIGNIFICANCE AND USE
4.1 The results obtained by this test method are simply a measure of the indentation into the sealant material of the indentor under load; they are not generally considered a measure of abrasion or wear resistance of the sealant.
SCOPE
1.1 This test method describes a laboratory procedure for determining indentation hardness of joint sealing compounds (single- and multicomponent) intended for use in building construction.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 The committee with jurisdiction over this standard is not aware of any comparable standards published by other organizations.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C679-15(2022)(Test Method)
Standard Test Method for Tack-Free Time of Elastomeric Sealants

SIGNIFICANCE AND USE
5.1 The tack-free time is a measure of the surface cure time and may generally be correlated to a variety of useful parameters such as the time interval before the sealant (1) resists damage by touch or light surface contact, (2) resists job-site or airborne dirt pick-up, (3) resists impinging rainfall.  
5.2 The tack-free time is sometimes used as an on-the-job quality assurance test. A quality product that is consistent and reproducible will generally fall within a maximum and minimum tack-free time.  
5.3 This test for tack-free time can be used at any temperature and humidity. It is important that if a sealant will be used in a climate quite different than the standard conditions called out in this test method, then those conditions be used to test the sealant.
SCOPE
1.1 This test method covers a procedure for the determination of the tack-free time property of single- and multi-component elastomeric sealants commonly used for sealing, caulking, and glazing in buildings and related construction.  
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Note 1: See Specification C920 for type and grade definitions.  
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