iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM D446-12(2017)

(Specification)

Standard Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers

Standard Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers

SCOPE
1.1 These specifications cover operating instructions for glass capillary kinematic viscometers of all the types described in detail in Annex A1, Annex A2, and Annex A3 as follows:    
Modified Ostwald viscometers, Annex A1  
Suspended-level viscometers, Annex A2  
Reverse-flow viscometers, Annex A3  
1.2 The calibration of the viscometers is described in Section 6.  
1.3 This standard covers some widely used viscometers suitable for use in accordance with Test Method D445. Other viscometers of the glass capillary type which are capable of measuring kinematic viscosity within the limits of precision given in Test Method D445 may be used.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Nov-2017
ICS
17.060 - Measurement of volume, mass, density, viscosity
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.07 - Flow Properties
Current Stage
Ref Project

Relations

Refers
ASTM D445-16 - Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
Effective Date
15-Dec-2016
Refers
ASTM D2162-14 - Standard Practice for Basic Calibration of Master Viscometers and Viscosity Oil Standards
Effective Date
01-Jun-2014
Refers
ASTM D445-14 - Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
Effective Date
01-Jul-2014
Refers
ASTM D445-14e1 - Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
Effective Date
01-Jul-2014

Buy Standard

ASTM D446-12(2017) - Standard Specifications and Operating Instructions for Glass Capillary Kinematic ViscometersASTM D446-12(2017) - Standard Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers
PreviousNext
Technical specification
ASTM D446-12(2017) - Standard Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers
English language
26 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:D446 −12 (Reapproved 2017)
Designation: 71/2/95
Standard Specifications and Operating Instructions for
1
Glass Capillary Kinematic Viscometers
This standard is issued under the fixed designation D446; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope and Viscosity Oil Standards
3
2.2 ISO Documents:
1.1 These specifications cover operating instructions for
ISO 3104Petroleum Products—Transparent and Opaque
glasscapillarykinematicviscometersofallthetypesdescribed
Liquids—Determination of Kinematic Viscosity and Cal-
in detail in Annex A1, Annex A2, and Annex A3 as follows:
culation of Dynamic Viscosity
Modified Ostwald viscometers, Annex A1
Suspended-level viscometers, Annex A2 ISO 3105 Glass Capillary Kinematic Viscometers—
Reverse-flow viscometers, Annex A3
Specifications and Operating Instructions
1.2 The calibration of the viscometers is described in ISO5725Basic Methods for the Determination of Repeat-
Section 6. ability and Reproducibility of a Standard Measurement
Method
1.3 This standard covers some widely used viscometers
ISO17025General Requirements for the Competence of
suitable for use in accordance with Test Method D445. Other
Testing and Calibration Laboratories
viscometers of the glass capillary type which are capable of
ISO Guide25General Requirements for the Calibration and
measuring kinematic viscosity within the limits of precision
Testing Laboratories
given in Test Method D445 may be used.
4
2.3 NIST Standards:
1.4 The values stated in SI units are to be regarded as
NIST1297Guidelines for Evaluating and Expressing the
standard. No other units of measurement are included in this
Uncertainty of NIST Measurement Results
standard.
1.5 This international standard was developed in accor-
3. Materials and Manufacture
dance with internationally recognized principles on standard-
3.1 Fully annealed, low-expansion borosilicate glass shall
ization established in the Decision on Principles for the
be used for the construction of all viscometers. The size
Development of International Standards, Guides and Recom-
number,serialnumber,andmanufacturer’sdesignationshallbe
mendations issued by the World Trade Organization Technical
permanently marked on each viscometer. All timing marks
Barriers to Trade (TBT) Committee.
shall be etched and filled with an opaque color, or otherwise
made a permanent part of the viscometer. See detailed descrip-
2. Referenced Documents
tion of each type of viscometer in Annex A1, Annex A2, and
2
2.1 ASTM Standards:
Annex A3.
D445Test Method for Kinematic Viscosity of Transparent
3.2 With the exception of the FitzSimons and Atlantic
and Opaque Liquids (and Calculation of DynamicViscos-
viscometers, all viscometers are designed to fit through a
ity)
51-mm hole in the lid of a constant-temperature bath having a
D2162Practice for Basic Calibration of MasterViscometers
liquid depth of at least 280 mm; and it is assumed that the
surfaceoftheliquidwillbenotmorethan45mmfromthetop
of the bath lid. For certain constant-temperature baths, espe-
1
These specifications and operating instructions are under the jurisdiction of
ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and cially at low or high temperatures, it may be necessary to
are the direct responsibility of Subcommittee D02.07 on Flow Properties.
constructtheviscometerswiththeuppermosttubeslongerthan
Current edition approved Dec. 1, 2017. Published December 2017. Originally
approvedin1966asD2515–66.RedesignatedD446in1977.Lastpreviousedition
approved in 2012 as D446–12. DOI: 10.1520/D0446-12R17.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM 4th Floor, New York, NY 10036.
4
Standards volume information, refer to the standard’s Document Summary page on Available from National Institute of Standards and Technology (NIST), 100
the ASTM website. Bureau Dr., Stop 1070, Gaithersburg, MD 20899-1070, http://www.nist.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D446−12 (2017)
shown to ensure adequate immersion in the constant- 6.2 Reference Viscometers:
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM D8092-22(Test Method)
Standard Test Method for Field Determination of Kinematic Viscosity Using a Microchannel Viscometer

SIGNIFICANCE AND USE
5.1 The significance of this test method is that it provides a means for a reliable field determination of kinematic viscosity at 40 °C without requiring solvents or chemicals for cleaning. Field use implies that the fluid may be very opaque, such as an in-service engine oil. The device may be cleaned with a disposable lint-free oil-absorbent material such as a clean cotton shop rag, and requires only 60 µL of sample for operation. As such the device provides a unique service to a range of industries where it is difficult or undesirable to obtain chemicals of any sort in order to determine the kinematic viscosity of their fluid of interest. Examples of such industries include many marine-based systems where a laboratory does not exist on-board, mines where equipment is needed for on-the-spot determination of asset viscosity, and large industrial plants where a walk-around inspection of oil sumps greatly increases efficiency. By using this test method, one can serve these crucial use-cases where a direct, immediate measure of kinematic viscosity at 40 °C may otherwise be difficult to obtain.
SCOPE
1.1 This test method describes a means for measuring the kinematic viscosity of transparent and opaque liquids such as new and in-service lubricating oils using a miniature microchannel viscometer at 40 °C in the range of 12.9 mm2/s to 174 mm2/s  
1.2 The precision has only been determined for those materials and viscosity ranges, as indicated in Section 17 on Precision and Bias.  
1.3 This test method is specifically tailored to obtaining a rapid, direct, temperature- stabilized measure of the kinematic viscosity of new and in-service lubricants in the field in real- time without the use of solvents or chemical cleaning agents. The measurement takes place at 40 °C and kinematic viscosity is directly obtained. No temperature extrapolations or density corrections are necessary.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in Section 9 on Hazards.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM D7961-22(Practice)
Standard Practice for Calibrating U-tube Density Cells over Large Ranges of Temperature and Pressure

SIGNIFICANCE AND USE
5.1 This practice covers a series of methods offered to aid users in calibrating U-tube density meters to provide a measure of density and an associated expanded uncertainty. The reference density, as obtained from either an equation of state (EOS) or CRM has an uncertainty that arises from the uncertainty of the measurements of temperature, pressure, and also the chemical purity of the substance studied (origin) or for that matter of the certified reference material. This uncertainty results in an additional uncertainty for the density of these samples. Because the measurements made with U-tube density meters are not absolute, the uncertainty with which the instrument calibration is determined is directly related to the uncertainty of the density obtained.
SCOPE
1.1 This practice outlines procedures for the calibration of U-tube density cells. It is applicable to instruments capable of determining fluid density at temperatures in the range –10 °C to 200 °C and pressures from just greater than the saturation pressure to 140 MPa. The practice refers to density cells as they are utilized to make measurements of fluids primarily in the compressed-liquid state. Examples of substances for which the density can be determined with a calibrated U-tube density meter include: crude oils, gasoline and gasoline-oxygenate blends, diesel and jet fuels, hydraulic fluids, and lubricating oils.  
1.2 This practice specifies a procedure for the determination of the expanded uncertainty of the density measurement.  
1.3 This practice pertains to fluids with viscosities  
1.4 4 The values listed in SI units are regarded as the standard, unless otherwise stated. The SI unit for mass density is kilograms per cubic metre (kg·m-3) and can be given as grams per cubic centimetre (g·cm-3).  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D7109-22e1(Test Method)
Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 Cycles

SIGNIFICANCE AND USE
5.1 This test method evaluates the percent viscosity loss of fluids resulting from physical degradation in the high shear nozzle device. Thermal or oxidative effects are minimized.  
5.2 This test method may be used for quality control purposes by manufacturers of polymeric lubricant additives and their customers.  
5.3 This test method is not intended to predict viscosity loss in field service in different field equipment under widely varying operating conditions, which may cause lubricant viscosity to change due to thermal and oxidative changes, as well as by the mechanical shearing of polymer. However, when the field service conditions, primarily or exclusively, result in the degradation of polymer by mechanical shearing, there may be a correlation between the results from this test method and results from the field.
SCOPE
1.1 This test method covers the evaluation of the shear stability of polymer-containing fluids. The test method measures the viscosity loss, in mm2/s and percent, at 100 °C of polymer-containing fluids when evaluated by a diesel injector apparatus procedure that uses European diesel injector test equipment. The viscosity loss reflects polymer degradation due to shear at the nozzle. Viscosity loss is evaluated after both 30 cycles and 90 cycles of shearing.
Note 1: This test method evaluates the shear stability of oils after both 30 cycles and 90 cycles of shearing. For most oils, there is a correlation between results after 30 cycles and results after 90 cycles of shearing, but this is not universal.
Note 2: Test Method D6278 uses essentially the same procedure with 30 cycles but without the 90 cycles portion of the test. The correlation between results from this test method at 30 cycles and results from Test Method D6278 has been established and shown in Research Report RR:D02-1629 to be equivalent.
Note 3: Test Method D2603 has been used for similar evaluation of shear stability; limitations are as indicated in the significance statement. No detailed attempt has been undertaken to correlate the results of this test method with those of the sonic shear test method.
Note 4: This test method uses test apparatus as defined in CEC L-14-A-93. This test method differs from CEC-L-14-A-93 in the period of time required for calibration.
Note 5: Test Method D5275 also shears oils in a diesel injector apparatus but may give different results.
Note 6: This test method has different calibration and operational requirements than withdrawn Test Method D3945.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Section 8.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
    sale 15% off
ASTM
ASTM D4052-22(Test Method)
Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter

SIGNIFICANCE AND USE
5.1 Density is a fundamental physical property that can be used in conjunction with other properties to characterize both the light and heavy fractions of petroleum and petroleum products.  
5.2 Determination of the density or relative density of petroleum and its products is necessary for the conversion of measured volumes to volumes at the standard temperature of 15 °C.
SCOPE
1.1 This test method covers the determination of the density, relative density, and API Gravity of petroleum distillates and viscous oils that can be handled in a normal fashion as liquids at the temperature of test, utilizing either manual or automated sample injection equipment. Its application is restricted to liquids with total vapor pressures (see Test Method D5191) typically below 100 kPa and viscosities (see Test Method D445 or D7042) typically below about 15 000 mm2/s at the temperature of test. The total vapor pressure limitation however can be extended to >100 kPa provided that it is first ascertained that no bubbles form in the U-tube, which can affect the density determination. Some examples of products that may be tested by this procedure include: gasoline and gasoline-oxygenate blends, diesel, jet, basestocks, waxes, and lubricating oils.  
1.1.1 Waxes and highly viscous samples were not included in the 1999 interlaboratory study (ILS) sample set that was used to determine the current precision statements of the method, since all samples evaluated at the time were analyzed at a test temperature of 15 °C. Wax and highly viscous samples require a temperature cell operated at elevated temperatures necessary to ensure a liquid test specimen is introduced for analysis. Consult instrument manufacturer instructions for appropriate guidance and precautions when attempting to analyze wax or highly viscous samples. Refer to the Precision and Bias section of the method and Note 9 for more detailed information about the 1999 ILS that was conducted.  
1.2 In cases of dispute, the referee method is the one where samples are introduced manually as in 6.2 or 6.3, as appropriate for sample type.  
1.3 When testing opaque samples, and when not using equipment that is capable of automatic bubble detection, proper procedure shall be established so that the absence of air bubbles in the U-tube can be established with certainty. For the determination of density in crude oil samples use Test Method D5002.  
1.4 The values stated in SI units are regarded as the standard, unless stated otherwise. The accepted units of measure for density are grams per millilitre (g/mL) or kilograms per cubic metre (kg/m3).  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 3.2.1, Section 7, 9.1, 10.2, and Appendix X1.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
    sale 15% off
  • Standard
    9 pages
    English language
    sale 15% off
ASTM
ASTM D7042-21a(Test Method)
Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity)

SIGNIFICANCE AND USE
5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.  
5.2 Density is a fundamental physical property that can be used in conjunction with other properties to characterize both the light and heavy fractions of petroleum and petroleum products.  
5.3 Determination of the density or relative density of petroleum and its products is necessary for the conversion of measured volumes to volumes at the standard temperature of 15 °C.
SCOPE
1.1 This test method covers and specifies a procedure for the concurrent measurement of both the dynamic viscosity, η, and the density, ρ, of liquid petroleum products and crude oils, both transparent and opaque. The kinematic viscosity, ν, can be obtained by dividing the dynamic viscosity, η, by the density, ρ, obtained at the same test temperature.  
1.2 The result obtained from this test method is dependent upon the behavior of the sample and is intended for application to liquids for which primarily the shear stress and shear rate are proportional (Newtonian flow behavior).  
1.3 The precision has only been determined for those materials, viscosity ranges, density ranges, and temperatures as indicated in Section 15 on Precision and Bias. The test method can be applied to a wider range of materials, viscosity, density, and temperature. For materials not listed in Section 15 on Precision and Bias, the precision and bias may not be applicable.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    14 pages
    English language
    sale 15% off
  • Standard
    14 pages
    English language
    sale 15% off
ASTM
ASTM D445-21e2(Test Method)
Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

SIGNIFICANCE AND USE
5.1 Many petroleum products, and some non-petroleum materials, are used as lubricants, and the correct operation of the equipment depends upon the appropriate viscosity of the liquid being used. In addition, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.
SCOPE
1.1 This test method specifies a procedure for the determination of the kinematic viscosity, ν, of liquid petroleum products, both transparent and opaque, by measuring the time for a volume of liquid to flow under gravity through a calibrated glass capillary viscometer. The dynamic viscosity, η, can be obtained by multiplying the kinematic viscosity, ν, by the density, ρ, of the liquid.  
Note 1: For the measurement of the kinematic viscosity and viscosity of bitumens, see also Test Methods D2170 and D2171.
Note 2: ISO 3104 corresponds to Test Method D445 – 03.  
1.2 The result obtained from this test method is dependent upon the behavior of the sample and is intended for application to liquids for which primarily the shear stress and shear rates are proportional (Newtonian flow behavior). If, however, the viscosity varies significantly with the rate of shear, different results may be obtained from viscometers of different capillary diameters. The procedure and precision values for residual fuel oils, which under some conditions exhibit non-Newtonian behavior, have been included.  
1.3 The range of kinematic viscosities covered by this test method is from 0.2 mm2/s to 300 000 mm2/s (see Table A1.1) at all temperatures (see 6.3 and 6.4). The precision has only been determined for those materials, kinematic viscosity ranges and temperatures as shown in the footnotes to the precision section.  
1.4 The values stated in SI units are to be regarded as standard. The SI unit used in this test method for kinematic viscosity is mm2/s, and the SI unit used in this test method for dynamic viscosity is mPa·s. For user reference, 1 mm2/s = 10-6 m2/s = 1 cSt and 1 mPa·s = 1 cP = 0.001 Pa·s.  
1.5 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    17 pages
    English language
    sale 15% off
ASTM
ASTM D1480-21(Test Method)
Standard Test Method for Density and Relative Density (Specific Gravity) of Viscous Materials by Bingham Pycnometer

SIGNIFICANCE AND USE
5.1 Density is a fundamental physical property that can be used in conjunction with other properties to characterize both the light and heavy fractions of petroleum and to assess the quality of crude oils.  
5.2 Determination of the density or relative density of petroleum and its products is necessary for the conversion of measured volumes to volumes at the standard temperatures of 15 °C.  
5.3 The determination of densities at the elevated temperatures of 40 °C and 100 °C is particularly useful in providing the data needed for the conversion of kinematic viscosities in mm2/s (centistokes) to the corresponding dynamic viscosities in mPa·s (centipoises).
SCOPE
1.1 This test method covers two procedures for the measurement of the density of materials which are fluid at the desired test temperature. Its application is restricted to liquids of vapor pressures below 80 kPa (600 mm Hg) and viscosities below 40 000 mm2/s (cSt) at the test temperature. The method is designed for use at any temperature between 20 °C and 100 °C. It can be used at higher temperatures; however, in this case the precision section does not apply.  
Note 1: For the determination of density of materials which are fluid at normal temperatures, see Test Method D1217.  
1.2 This test method provides a calculation procedure for converting density to specific gravity.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D2162-21(Practice)
Standard Practice for Basic Calibration of Master Viscometers and Viscosity Oil Standards

SIGNIFICANCE AND USE
5.1 Because there are surface tension or kinematic viscosity differences, or both, between the primary standard (7.4) and kinematic viscosity standards (7.5), special procedures using master viscometers are required to “step-up” from the kinematic viscosity of the primary standard to the kinematic viscosities of oil standards.  
5.2 Using master viscometers calibrated according to this practice, an operator can calibrate kinematic viscometers in accordance with Specifications D446.  
5.3 Using viscosity oil standards established in this practice, an operator can calibrate kinematic viscometers in accordance with Specifications D446.
SCOPE
1.1 This practice covers the calibration of master viscometers and viscosity oil standards, both of which may be used to calibrate routine viscometers as described in Test Method D445 and Specifications D446 over the temperature range from 15 °C to 100 °C.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 The SI-based units for calibration constants and kinematic viscosities are mm2/s2 and mm 2/s, respectively.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off
  • Standard
    8 pages
    English language
    sale 15% off
ASTM
ASTM D7483-21(Test Method)
Standard Test Method for Determination of Dynamic Viscosity and Derived Kinematic Viscosity of Liquids by Oscillating Piston Viscometer

SIGNIFICANCE AND USE
5.1 Many petroleum products, as well as non-petroleum materials, are used as lubricants for bearings, gears, compressor cylinders, hydraulic equipment, etc. Proper operation of this equipment depends upon the viscosity of these liquids.  
5.2 Oscillating piston viscometers allow viscosity measurement of a broad range of materials including transparent, translucent and opaque liquids. The measurement principle and stainless steel construction makes the Oscillating Piston Viscometer resistant to damage and suitable for portable operations. The measurement itself is automatic and does not require an operator to time the oscillation of the piston. The electromagnetically driven piston mixes the sample while under test. The instrument requires a sample volume of less than 5 mL and typical solvent volume of less than 10 mL which minimizes cleanup effort and waste.
SCOPE
1.1 This test method covers the measurement of dynamic viscosity and derivation of kinematic viscosity of liquids, such as new and in-service lubricating oils, by means of an oscillating piston viscometer.  
1.2 This test method is applicable to Newtonian and non-Newtonian liquids; however the precision statement was developed using Newtonian liquids.  
1.3 The range of dynamic viscosity covered by this test method is from 0.2 mPa·s to 20 000 mPa·s (which is approximately the kinematic viscosity range of 0.2 mm2/s to 22 000 mm2/s for new oils) in the temperature range between –40 °C to 190 °C; however the precision has been determined only for new and used oils in the range of 34 mPa·s to 1150 mPa·s at 40 °C, 5.7 mPa·s to 131 mPa·s at 100 °C, and 46.5 mm2/s to 436 mm2/s at 40 °C.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM D6616-21(Test Method)
Standard Test Method for Measuring Viscosity at High Shear Rate by Tapered Bearing Simulator Viscometer at 100 °C

SIGNIFICANCE AND USE
5.1 Viscosity at the shear rate and temperature of this test method is thought to be particularly representative of bearing conditions in large medium speed reciprocating engines as well as automotive and heavy duty engines operating in this temperature regime.  
5.2 The importance of viscosity under these conditions has been stressed in railroad specifications.  
5.3 For other industry needs this method may also be run at 80 °C by using different crossover calibration oils available from the manufacturer. No precision has been determined at this temperature. The equipment is also used at higher temperatures as shown in Test Method D4683 and CEC L-36-90 (also referenced from IP 370).
SCOPE
1.1 This test method covers the laboratory determination of the viscosity of engine oils at 100 °C and 1·106s–1 using the Tapered Bearing Simulator (TBS) viscometer.2
Note 1: This test method is similar to Test Method D4683 which uses the same TBS viscometer to measure high shear viscosity at 150 °C.  
1.2 The Newtonian calibration oils used to establish this test method range from approximately 5 mPa·s (cP) to 12 mPa·s (cP) at 100 °C and either the manual or automated protocol was used by each participant in developing the precision statement. The viscosity range of the test method at this temperature is from 1 mPa·s (cP) to above 25 mPa·s (cP), depending on the model of TBS.  
1.3 The non-Newtonian reference oil used to establish the shear rate of 1·106s–1 for this test method has a viscosity of approximately 10 mPa·s at 100 °C.  
1.4 Application to petroleum products other than engine oil has not been determined in preparing the viscometric information for this test method.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. This test method uses the milliPascal second (mPa·s) as the unit of viscosity. This unit is equivalent to the centiPoise (cP), which is shown in parentheses.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    14 pages
    English language
    sale 15% off
  • Standard
    14 pages
    English language
    sale 15% off