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ASTM E2019-03(2019)

(Test Method)

Standard Test Method for Minimum Ignition Energy of a Dust Cloud in Air

Standard Test Method for Minimum Ignition Energy of a Dust Cloud in Air

SIGNIFICANCE AND USE
5.1 This test method provides a procedure for performing laboratory tests to determine the minimum ignition energy of a dust cloud.
Note 1: For gases and vapors, see Test Method E582.  
5.2 The data developed by this test method may be used to assess the spark ignitibility of a dust cloud. Additional guidance on the significance of minimum ignition energy is in X1.1.  
5.3 The values obtained are specific to the sample tested, the method used and the test equipment used. The values are not to be considered intrinsic material constants.  
5.4 The MIE of a dust as determined using this procedure can be compared with the MIE's of reference dusts (using the same procedure) to obtain the relative sensitivity of the dust to spark ignition. An understanding of the relative sensitivity to spark ignition can be used to minimize the probability of explosions due to spark ignition.
SCOPE
1.1 This test method determines the minimum ignition energy of a dust cloud in air by a high voltage spark.  
1.2 The minimum ignition energy (MIE) of a dust-cloud is primarily used to assess the likelihood of ignition during processing and handling. The likelihood of ignition is used to evaluate the need for precautions such as explosion prevention systems. The MIE is determined as the electrical energy stored in a capacitor which, when released as a high voltage spark, is just sufficient to ignite the dust cloud at its most easily ignitable concentration in air. The laboratory test method described in this standard does not optimize all test variables that affect MIE. Smaller MIE values might be determined by increasing the number of repetitions or optimizing the spark discharge circuit for each dust tested.  
1.3 In this test method, the test equipment is calibrated using a series of reference dusts whose MIE values lie within established limits. Once the test equipment is calibrated, the relative ignition sensitivity of other dusts can be found by comparing their MIE values with those of the reference dusts or with dusts whose ignition sensitivities are known from experience. X1.1 of this test method includes guidance on the significance of minimum ignition energy with respect to electrostatic discharges.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
14-Feb-2019
ICS
13.230 - Explosion protection
Technical Committee
E27 - Hazard Potential of Chemicals
Drafting Committee
E27.05 - Explosibility and Ignitability of Dust Clouds
Current Stage
Ref Project

Relations

Refers
ASTM D3175-17 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Feb-2017
Refers
ASTM E1226-19 - Standard Test Method for Explosibility of Dust Clouds
Effective Date
15-Dec-2019
Refers
ASTM D3175-20 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Feb-2020
Refers
ASTM D3175-18 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Dec-2018
Referred By
ASTM E1445-08(2015) - Standard Terminology Relating to Hazard Potential of Chemicals
Effective Date
15-Feb-2019

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ASTM E2019-03(2019) - Standard Test Method for Minimum Ignition Energy of a Dust Cloud in AirASTM E2019-03(2019) - Standard Test Method for Minimum Ignition Energy of a Dust Cloud in Air
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ASTM E2019-03(2019) - Standard Test Method for Minimum Ignition Energy of a Dust Cloud in Air
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2019 − 03 (Reapproved 2019)
Standard Test Method for
1
Minimum Ignition Energy of a Dust Cloud in Air
This standard is issued under the fixed designation E2019; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
1.1 This test method determines the minimum ignition
Barriers to Trade (TBT) Committee.
energy of a dust cloud in air by a high voltage spark.
1.2 The minimum ignition energy (MIE) of a dust-cloud is
2. Referenced Documents
primarily used to assess the likelihood of ignition during
2
2.1 ASTM Standards:
processing and handling. The likelihood of ignition is used to
D3173Test Method for Moisture in theAnalysis Sample of
evaluate the need for precautions such as explosion prevention
Coal and Coke
systems.The MIE is determined as the electrical energy stored
D3175Test Method for Volatile Matter in the Analysis
in a capacitor which, when released as a high voltage spark, is
Sample of Coal and Coke
justsufficienttoignitethedustcloudatitsmosteasilyignitable
E582 Test Method for Minimum Ignition Energy and
concentration in air. The laboratory test method described in
Quenching Distance in Gaseous Mixtures
this standard does not optimize all test variables that affect
E789Test Method for Dust Explosions in a 1.2-Litre Closed
MIE. Smaller MIE values might be determined by increasing
3
Cylindrical Vessel (Withdrawn 2007)
the number of repetitions or optimizing the spark discharge
E1226Test Method for Explosibility of Dust Clouds
circuit for each dust tested.
E1445Terminology Relating to Hazard Potential of Chemi-
1.3 Inthistestmethod,thetestequipmentiscalibratedusing
cals
a series of reference dusts whose MIE values lie within
4
2.2 IEC Standards:
established limits. Once the test equipment is calibrated, the
1241-2-3, 1994ElectricalApparatus for Use in the Presence
relative ignition sensitivity of other dusts can be found by
of Combustible Dusts, Part 2: Test Method, Section 3:
comparing their MIE values with those of the reference dusts
Method for Determining Minimum Ignition Energy of
or with dusts whose ignition sensitivities are known from
Dust-Air Mixtures
experience. X1.1 of this test method includes guidance on the
significance of minimum ignition energy with respect to
3. Terminology
electrostatic discharges.
3.1 Definitions—For additional definitions, see Terminol-
1.4 The values stated in SI units are to be regarded as
ogy E1445.
standard. No other units of measurement are included in this
3.2 Definitions of Terms Specific to This Standard:
standard.
3.2.1 ignition delay time, n—the time between the onset of
1.5 This standard does not purport to address all of the
dispersion of the dust sample into a cloud and the activation of
safety concerns, if any, associated with its use. It is the
the ignition source.
responsibility of the user of this standard to establish appro-
3.2.2 minimum ignition energy (MIE), n—electrical energy
priate safety, health, and environmental practices and deter-
discharged from a capacitor, which is just sufficient to effect
mine the applicability of regulatory limitations prior to use.
ignitionofthemosteasilyignitableconcentrationoffuelinair
Specific precautionary statements are given in Section 8.
under the specific test conditions.
1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
1
This test method is under the jurisdiction ofASTM Committee E27 on Hazard the ASTM website.
3
Potential of Chemicals and is the direct responsibility of Subcommittee E27.05 on The last approved version of this historical standard is referenced on
Explosibility and Ignitability of Dust Clouds. www.astm.org.
4
Current edition approved Feb. 15, 2019. Published March 2019. Originally Available from International Electrotechnical Commission (IEC), 3, rue de
approved in 1999. Last previous edition approved in 2013 as E2019–03 (2013). Varembé, 1st floor, P.O. Box 131, CH-1211, Geneva 20, Switzerland, https://
DOI: 10.1520/E2019-03R19. www.iec.ch.
Copyright © ASTM I
...

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SIGNIFICANCE AND USE
5.1 This test method is applicable to dusts and powders, and provides a procedure for performing laboratory tests to evaluate hot-surface ignition temperatures of dust layers.  
5.2 The test data can be of value in determining safe operating conditions in industrial plants, mines, manufacturing processes, and locations of material usage and storage.  
5.3 Due to variation of ignition temperature with layer thickness, the test data at one thickness may not be applicable to all industrial situations (see Appendix X1). Tests at various layer thicknesses may provide a means for extrapolation to thicker layers, as listed in the following for pulverized Pittsburgh bituminous coal dust (2). Mathematical modeling of layer ignition at various layer thicknesses is described in Ref. (3).
Layer Thickness, mm  
Hot-Surface Ignition Temperature, °C  
6.4  
300  
9.4  
260  
12.7  
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5.4 This hot plate test method allows for loss of heat from the top surface of the dust layer, and therefore generally gives a higher ignition temperature for a material than Test Method E771, which is a more adiabatic system.  
5.5 This test method for dust layers generally will give a lower ignition temperature than Test Method E1491, which is for dust clouds. The layer ignition temperature is determined while monitoring for periods of minutes to hours, while the dust cloud is only exposed to the furnace for a period of seconds.
Note 1: Much of the literature data for layer ignition is actually from a basket in a heated furnace (4), known as the modified Godbert-Greenwald furnace test. Other data are from nonstandardized hot plates (5-9).  
5.6 Additional information on the significance and use of this test method may be found in Ref. (10).
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1.1 This test method covers a laboratory procedure to determine the hot-surface ignition temperature of dust layers, that is, measuring the minimum temperature at which a dust layer will self-heat. The test consists of a dust layer heated on a hot plate.2,3  
1.2 Data obtained from this test method provide a relative measure of the hot-surface ignition temperature of a dust layer.  
1.3 This test method should be used to measure and describe the properties of materials in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire hazard risk of materials, products, or assemblies under actual fire conditions. However, results of this test method may be used as elements of a fire risk assessment that takes into account all of the factors that are pertinent to an assessment of the fire hazard risk of a particular end use product.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E1515-14(2022)(Test Method)
Standard Test Method for Minimum Explosible Concentration of Combustible Dusts

SIGNIFICANCE AND USE
5.1 This test method provides a procedure for performing laboratory tests to evaluate relative deflagration parameters of dusts.  
5.2 The MEC as measured by this test method provides a relative measure of the concentration of a dust cloud necessary for an explosion.  
5.3 Since the MEC as measured by this test method may vary with the uniformity of the dust dispersion, energy of the ignitor, and propagation criteria, the MEC should be considered a relative rather than absolute measurement.  
5.4 If too weak an ignition source is used, the measured MEC would be higher than the “true” value. This is an ignitability limit rather than a flammability limit, and the test could be described as “underdriven.” Ideally, the ignition energy is increased until the measured MEC is independent of ignition energy. However, at some point the ignition energy may become too strong for the size of the test chamber, and the system becomes “overdriven.” When the ignitor flame becomes too large relative to the chamber volume, a test could appear to result in an explosion, while it is actually just dust burning in the ignitor flame with no real propagation beyond the ignitor.  
5.5 The recommended ignition source for measuring the MEC of dusts in 20-L chambers is a 2500 or 5000 J pyrotechnic ignitor.4 Measuring the MEC at both ignition energies will provide information on the possible overdriving of the system.5 To evaluate the effect of possible overdriving in a 20-L chamber, comparison tests may also be made in a larger chamber, such as a 1 m3-chamber.  
5.6 If a dust ignites with a 5000 J ignitor but not with a 2500 J ignitor in a 20-L chamber, this may be an overdriven system.5 In this case, it is recommended that the dust be tested with a 10 000 J ignitor in a larger chamber, such as a 1 m3-chamber, to determine if it is actually explosible.  
5.7 The values obtained by this test method are specific to the sample tested (particularly the particle size distribution) and the met...
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1.1 This test method covers the determination of the minimum concentration of a dust-air mixture that will propagate a deflagration in a near-spherical closed vessel of 20 L or greater volume.
Note 1: The minimum explosible concentration (MEC) is also referred to as the lower explosibility limit (LEL) or lean flammability limit (LFL).  
1.2 Data obtained from this test method provide a relative measure of the deflagration characteristics of dust clouds.  
1.3 This test method should be used to measure and describe the properties of materials in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire risk assessment that takes into account all of the factors that are pertinent to an assessment of the fire hazard of a particular end use.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  Specific precautionary statements are given in Section 8.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E1226-19(Test Method)
Standard Test Method for Explosibility of Dust Clouds

SIGNIFICANCE AND USE
5.1 This test method provides a procedure for performing laboratory tests to evaluate deflagration parameters of dusts.  
5.2 The data developed by this test method may be used for the purpose of sizing deflagration vents in conjunction with the nomographs and equations published in NFPA 68, ISO 6184/1, or VDI 3673.  
5.3 The values obtained by this testing technique are specific to the sample tested and the method used and are not to be considered intrinsic material constants.  
5.4 For dusts with low KSt values, discrepancies have been observed between tests in 20-L and 1-m3 chambers. A strong ignitor may overdrive a 20-L chamber, as discussed in Test Method E1515 and Refs (1-4).8 Conversely, more recent testing has shown that some metal dusts can be prone to underdriving in the 20-L chamber, exhibiting significantly lower KSt values than in a 1-m3 chamber (5). Ref (6) provides supporting calculations showing that a test vessel of at least 1-m3 of volume is necessary to obtain the maximum explosibility index for a burning dust cloud having an abnormally high flame temperature. In these two overdriving and underdriving scenarios described above, it is therefore recommended to perform tests in 1-m3 or larger calibrated test vessels in order to measure dusts explosibility parameters accurately.
Note 5: Ref (2) concluded that dusts with KSt values below 45 bar m/s when measured in a 20-L chamber with a 10 000-J ignitor, may not be explosible when tested in a 1-m3 chamber with a 10 000-J ignitor. Ref (2) and unpublished testing has also shown that in some cases the KSt values measured in the 20-L chamber can be lower than those measured in the 1-m3 chamber. Refs (1) and (3) found that for some dusts, it was necessary to use lower ignition energy in the 20-L chamber in order to match MEC or MIC test data in a 1-m3 chamber. If a dust has measurable (nonzero) Pmax and KSt values with a 5000 or 10 000-J ignitor when tested in a 20-L chamber but no measurable Pmax and ...
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1.1 Purpose. The purpose of this test method is to provide standard test methods for characterizing the “explosibility” of dust clouds in two ways, first by determining if a dust is “explosible,” meaning a cloud of dust dispersed in air is capable of propagating a deflagration, which could cause a flash fire or explosion; or, if explosible, determining the degree of “explosibility,” meaning the potential explosion hazard of a dust cloud as characterized by the dust explosibility parameters, maximum explosion pressure, Pmax; maximum rate of pressure rise, (dP/dt)max; and explosibility index, KSt.  
1.2 Limitations. Results obtained by the application of the methods of this standard pertain only to certain combustion characteristics of dispersed dust clouds. No inference should be drawn from such results relating to the combustion characteristics of dusts in other forms or conditions (for example, ignition temperature or spark ignition energy of dust clouds, ignition properties of dust layers on hot surfaces, ignition of bulk dust in heated environments, etc.)  
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1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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5.1 This practice provides nine figures of merit which may be used to estimate the relative thermal hazard of thermally unstable materials. Since numerous assumptions must be made in order to obtain these figures of merit, care must be exercised to avoid too rigorous interpretation (or even misapplication) of the results.  
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1.1 This practice covers the calculation of hazard potential figures of merit for exothermic reactions, including:
(1) Time-to-thermal-runaway,
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(3) Critical half thickness,
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1.2 The kinetic parameters needed in this calculation may be obtained from differential scanning calorimetry (DSC) curves by methods described in other documents.  
1.3 This technique is the best applicable to simple, single reactions whose behavior can be described by the Arrhenius equation and the general rate law. For reactions which do not meet these conditions, this technique may, with caution, serve as an approximation.  
1.4 The calculations and results of this practice might be used to estimate the relative degree of hazard for experimental and research quantities of thermally unstable materials for which little experience and few data are available. Comparable calculations and results performed with data developed for well characterized materials in identical equipment, environment, and geometry are key to the ability to estimate relative hazard.  
1.5 The figures of merit calculated as described in this practice are intended to be used only as a guide for the estimation of the relative thermal hazard potential of a system (materials, container, and surroundings). They are not intended to predict actual thermokinetic performance. The calculated errors for these parameters are an intimate part of this practice and must be provided to stress this. It is strongly recommended that those using the data provided by this practice seek the consultation of qualified personnel for proper interpretation.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method provides a procedure for performing laboratory tests to evaluate relative deflagration parameters of dusts.  
5.2 Knowledge of the limiting oxygen (oxidant) concentration is needed for safe operation of some chemical processes. This information may be needed in order to start up, shut down or operate a process while avoiding the creation of flammable dust-gas atmospheres therein, or to pneumatically transport materials safely. NFPA 69 provides guidance for the practical use of LOC data, including the appropriate safety margin to use.  
5.3 Since the LOC as measured by this method may vary with the energy of the ignitor and the propagation criteria, the LOC should be considered a relative rather than absolute measurement.  
5.4 If too weak an ignition source is used, the measured LOC would be higher than the “true” value and would not be sufficiently conservative. This is an ignitability limit rather than a flammability limit, and the test could be described as “underdriven.” Ideally, the ignition energy is increased until the measured LOC is independent of ignition energy (that is, the “true” value). However, at some point the ignition energy may become too strong for the size of the test chamber, and the system becomes “overdriven.” When the ignitor flame becomes too large relative to the chamber volume, a test could appear to result in an explosion, while it is actually just dust burning in the ignitor flame with no real propagation beyond the ignitor (1-3).5 This LOC value would be overly conservative.  
5.5 The recommended ignition source for measuring the LOC of dusts in 20-L chambers is a 2500-J pyrotechnic ignitor.6 This ignitor contains 0.6 g of a powder mixture of 40 % zirconium, 30 % barium nitrate, and 30 % barium peroxide. Measuring the LOC at several ignition energies will provide information on the possible overdriving of the system to evaluate the effect of possible overdriving in a 20-L chamber, comparison tests may also be m...
SCOPE
1.1 This test method is designed to determine the limiting oxygen concentration of a combustible dust dispersed in a mixture of air with an inert/nonflammable gas in a near-spherical closed vessel of 20 L or greater volume.  
1.2 Data obtained from this method provide a relative measure of the deflagration characteristics of dust clouds.  
1.3 This test method should be used to measure and describe the properties of materials in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire risk assessment that takes into account all of the factors that are pertinent to an assessment of the fire hazard of a particular end use.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Minimum Autoignition Temperature of Dust Clouds

SIGNIFICANCE AND USE
5.1 This test method provides a procedure for performing laboratory tests to determine the minimum autoignition temperature (MAIT) of a dust cloud.  
5.2 The test data developed from this test method can be used to limit the temperature to which a dust cloud is exposed so as to prevent ignition of the cloud. Because of the short duration of the test, the data obtained are most applicable to industrial equipment where dust is present as a cloud for a short time. Because of the small scale of the test and the possible variation of the MAIT value with scale, the data obtained by this test method may not be directly applicable to all industrial conditions.  
5.3 The MAIT data can also be used in conjunction with minimum spark ignition data to evaluate the hazards of grinding and impact sparks in the presence of dust clouds (1 and 2).3  
5.4 The test values obtained are specific to the sample tested, the method used, and the test equipment utilized. The test values are not to be considered intrinsic material constants, but may be used as a relative measure of the temperature at which a dust cloud self ignites.  
5.5 The test data are for cloud ignition. Dust in the form of a layer may ignite at significantly lower temperatures than the same dust in the form of a cloud (3). For liquid chemicals, see Test Method E659.
SCOPE
1.1 This test method covers the minimum temperature at which a given dust cloud will autoignite when exposed to air heated in a furnace at local atmospheric pressure.  
1.2 Data obtained from this test method provide a relative measure of dust cloud autoignition temperatures.  
1.3 This test method should be used to measure and describe the properties of materials, products, or assemblies in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test method may be used as elements of a fire risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard of a particular end use.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM G126-16(2023)(Terminology)
Standard Terminology Relating to the Compatibility and Sensitivity of Materials in Oxygen Enriched Atmospheres

SCOPE
1.1 This terminology defines terms related to the compatibility and sensitivity of materials in oxygen enriched atmospheres. It includes those standards under the jurisdiction of ASTM Committee G04.  
1.2 The terminology concentrates on terms commonly encountered in and specific to practices and methods used to evaluate the compatibility and sensitivity of materials in oxygen. This evaluation is usually performed in a laboratory environment, and this terminology does not attempt to include laboratory terms.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E2021-15(2023)(Test Method)
Standard Test Method for Hot-Surface Ignition Temperature of Dust Layers

SIGNIFICANCE AND USE
5.1 This test method is applicable to dusts and powders, and provides a procedure for performing laboratory tests to evaluate hot-surface ignition temperatures of dust layers.  
5.2 The test data can be of value in determining safe operating conditions in industrial plants, mines, manufacturing processes, and locations of material usage and storage.  
5.3 Due to variation of ignition temperature with layer thickness, the test data at one thickness may not be applicable to all industrial situations (see Appendix X1). Tests at various layer thicknesses may provide a means for extrapolation to thicker layers, as listed in the following for pulverized Pittsburgh bituminous coal dust (2). Mathematical modeling of layer ignition at various layer thicknesses is described in Ref. (3).
Layer Thickness, mm  
Hot-Surface Ignition Temperature, °C  
6.4  
300  
9.4  
260  
12.7  
240  
25.4  
210  
5.4 This hot plate test method allows for loss of heat from the top surface of the dust layer, and therefore generally gives a higher ignition temperature for a material than Test Method E771, which is a more adiabatic system.  
5.5 This test method for dust layers generally will give a lower ignition temperature than Test Method E1491, which is for dust clouds. The layer ignition temperature is determined while monitoring for periods of minutes to hours, while the dust cloud is only exposed to the furnace for a period of seconds.
Note 1: Much of the literature data for layer ignition is actually from a basket in a heated furnace (4), known as the modified Godbert-Greenwald furnace test. Other data are from nonstandardized hot plates (5-9).  
5.6 Additional information on the significance and use of this test method may be found in Ref. (10).
SCOPE
1.1 This test method covers a laboratory procedure to determine the hot-surface ignition temperature of dust layers, that is, measuring the minimum temperature at which a dust layer will self-heat. The test consists of a dust layer heated on a hot plate.2,3  
1.2 Data obtained from this test method provide a relative measure of the hot-surface ignition temperature of a dust layer.  
1.3 This test method should be used to measure and describe the properties of materials in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire hazard risk of materials, products, or assemblies under actual fire conditions. However, results of this test method may be used as elements of a fire risk assessment that takes into account all of the factors that are pertinent to an assessment of the fire hazard risk of a particular end use product.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E1515-14(2022)(Test Method)
Standard Test Method for Minimum Explosible Concentration of Combustible Dusts

SIGNIFICANCE AND USE
5.1 This test method provides a procedure for performing laboratory tests to evaluate relative deflagration parameters of dusts.  
5.2 The MEC as measured by this test method provides a relative measure of the concentration of a dust cloud necessary for an explosion.  
5.3 Since the MEC as measured by this test method may vary with the uniformity of the dust dispersion, energy of the ignitor, and propagation criteria, the MEC should be considered a relative rather than absolute measurement.  
5.4 If too weak an ignition source is used, the measured MEC would be higher than the “true” value. This is an ignitability limit rather than a flammability limit, and the test could be described as “underdriven.” Ideally, the ignition energy is increased until the measured MEC is independent of ignition energy. However, at some point the ignition energy may become too strong for the size of the test chamber, and the system becomes “overdriven.” When the ignitor flame becomes too large relative to the chamber volume, a test could appear to result in an explosion, while it is actually just dust burning in the ignitor flame with no real propagation beyond the ignitor.  
5.5 The recommended ignition source for measuring the MEC of dusts in 20-L chambers is a 2500 or 5000 J pyrotechnic ignitor.4 Measuring the MEC at both ignition energies will provide information on the possible overdriving of the system.5 To evaluate the effect of possible overdriving in a 20-L chamber, comparison tests may also be made in a larger chamber, such as a 1 m3-chamber.  
5.6 If a dust ignites with a 5000 J ignitor but not with a 2500 J ignitor in a 20-L chamber, this may be an overdriven system.5 In this case, it is recommended that the dust be tested with a 10 000 J ignitor in a larger chamber, such as a 1 m3-chamber, to determine if it is actually explosible.  
5.7 The values obtained by this test method are specific to the sample tested (particularly the particle size distribution) and the met...
SCOPE
1.1 This test method covers the determination of the minimum concentration of a dust-air mixture that will propagate a deflagration in a near-spherical closed vessel of 20 L or greater volume.
Note 1: The minimum explosible concentration (MEC) is also referred to as the lower explosibility limit (LEL) or lean flammability limit (LFL).  
1.2 Data obtained from this test method provide a relative measure of the deflagration characteristics of dust clouds.  
1.3 This test method should be used to measure and describe the properties of materials in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire risk assessment that takes into account all of the factors that are pertinent to an assessment of the fire hazard of a particular end use.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  Specific precautionary statements are given in Section 8.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM G74-13(2021)(Test Method)
Standard Test Method for Ignition Sensitivity of Nonmetallic Materials and Components by Gaseous Fluid Impact

SIGNIFICANCE AND USE
4.1 This test standard describes how to evaluate the relative sensitivity of materials and components to dynamic pressure impacts by various gaseous fluid media (can include gas mixtures).  
4.2 Changes or variations in test specimen configurations, thickness, preparation, and cleanliness can cause a significant change in their impact ignition sensitivity/reaction. For material tests, the test specimen configuration shall be specified on the test report.  
4.3 Changes or variation in the test system configuration from that specified herein may cause a significant change in the severity produced by a dynamic pressure surge of the gaseous media.  
4.4 A reaction is indicated by an abrupt increase in test specimen temperature, by obvious changes in odor, color, or material appearance, or a combination thereof, as observed during post-test examinations. Odor alone is not considered positive evidence that a reaction has occurred. When an increase in test specimen temperature is observed, a test specimen reaction must be confirmed by visual inspection. To aid with visual inspection, magnification less than 10× can be used.  
4.5 When testing components, the test article must be disassembled and the nonmetallic materials examined for evidence of ignition after completion of the specified pressure surge cycles.  
4.6 Ignition or precursors to ignition for any test sample shall be considered a failure and are indicated by burning, material loss, scorching, or melting of a test material detected through direct visual means. Ignition is often indicated by consumption of the non-metallic material under test, whether as an individual material or within a component. Partial ignition can also occur, as shown in Fig. 3a, b, and c, and shall also be considered an ignition (failure) for the purpose of this test standard.
FIG. 3 a Untested PCTFE (10X Magnification) (Polychlorotrifluoroethylene) Sample.  
FIG. 3 b Untested Nylon (PA, polyamide) Valve Seat (10X magnification) (c...
SCOPE
1.1 This test method describes a method to determine the relative sensitivity of nonmetallic materials (including plastics, elastomers, coatings, etc.) and components (including valves, regulators flexible hoses, etc.) to dynamic pressure impacts by gases such as oxygen, air, or blends of gases containing oxygen.  
1.2 This test method describes the test apparatus and test procedures employed in the evaluation of materials and components for use in gases under dynamic pressure operating conditions up to gauge pressures of 69 MPa and at elevated temperatures.  
1.3 This test method is primarily a test method for ranking of materials and qualifying components for use in gaseous oxygen. The material test method is not necessarily valid for determination of the sensitivity of the materials in an “as-used” configuration since the material sensitivity can be altered because of changes in material configuration, usage, and service conditions/interactions. However, the component testing method outlined herein can be valid for determination of the sensitivity of components under service conditions. The current provisions of this method were based on the testing of components having an inlet diameter (ID bore) less than or equal to 14 mm (see Note 1).  
1.4 A 5 mm Gaseous Fluid Impact Sensitivity (GFIS) test system and a 14 mm GFIS test system are described in this standard. The 5 mm GFIS system is utilized for materials and components that are directly attached to a high-pressure source and have minimal volume between the material/component and the pressure source. The 14 mm GFIS system is utilized for materials and components that are attached to a high pressure source through a manifold or other higher volume or larger sized connection. Other sizes than these may be utilized but no attempt has been made to characterize the thermal profiles of other volumes and geometries (see Note 1).
Note 1: The energy delivered by this t...

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