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ASTM E1898-07

(Test Method)

Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption Spectrometry

Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
In the primary metallurgical processes used by the mineral processing industry for copper bearing ores, copper and silver associated with sulfide mineralization are concentrated by the process of flotation for recovery of the metals.
This test method is intended to be a referee method for the determination of silver in copper concentrates. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E 882.
SCOPE
1.1 This test method covers the determination of silver in the range of 50 g/g to 1000 g/g by acid dissolution of the silver and measurement by atomic absorption spectrophotometry. Copper concentrates are internationally traded within the following concentration ranges:
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to its use.

General Information

Status
Historical
Publication Date
31-May-2007
ICS
71.040.50 - Physicochemical methods of analysis
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.02 - Ores, Concentrates, and Related Metallurgical Materials
Current Stage
Ref Project

Relations

Replaces
ASTM E1898-02 - Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption Spectrometry
Effective Date
01-Jun-2007

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ASTM E1898-07 - Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption SpectrometryASTM E1898-07 - Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption Spectrometry
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ASTM E1898-07 - Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption Spectrometry
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E1898 − 07
StandardTest Method for
Determination of Silver in Copper Concentrates by Flame
1
Atomic Absorption Spectrometry
This standard is issued under the fixed designation E1898; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
1.1 This test method covers the determination of silver in 2.1 ASTM Standards:
the range of 50 µg/g to 1000 µg/g by acid dissolution of the D1193 Specification for Reagent Water
silver and measurement by atomic absorption spectrophotom- E29 Practice for Using Significant Digits in Test Data to
etry. Copper concentrates are internationally traded within the Determine Conformance with Specifications
following concentration ranges: E50 Practices for Apparatus, Reagents, and Safety Consid-
erations for Chemical Analysis of Metals, Ores, and
Element Unit Concentration Range
Aluminum % 0.05 to 2.50
Related Materials
Antimony % 0.0001 to 4.50
E135 Terminology Relating to Analytical Chemistry for
Arsenic % 0.01 to 0.50
Metals, Ores, and Related Materials
Barium % 0.003 to 0.10
Bismuth % 0.001 to 0.16
E633 Guide for Use of Thermocouples in Creep and Stress-
Cadmium % 0.0005 to 0.04
Rupture Testing to 1800°F (1000°C) in Air
Calcium % 0.05 to 4.00
E882 Guide for Accountability and Quality Control in the
Carbon % 0.10 to 0.90
Chlorine % 0.001 to 0.006
Chemical Analysis Laboratory
Chromium % 0.0001 to 0.10
E1024 Guide for Chemical Analysis of Metals and Metal
Cobalt % 0.0005 to 0.20
Bearing Ores by Flame Atomic Absorption Spectropho-
Copper % 10.0 to 44.0
3
Fluorine % 0.001 to 0.10
tometry (Withdrawn 2004)
Gold µg/g 1.40 to 100.0
E1601 Practice for Conducting an Interlaboratory Study to
Iron % 12.0 to 30.0
Evaluate the Performance of an Analytical Method
Lead % 0.01 to 1.40
Magnesium % 0.02 to 2.00
E1763 Guide for Interpretation and Use of Results from
Manganese % 0.009 to 0.10
Interlaboratory Testing of Chemical Analysis Methods
Mercury µg/g 0.05 to 50.0
Molybdenum % 0.002 to 0.25
3. Terminology
Nickel % 0.0001 to 0.08
Silicon % 0.40 to 20.0
3.1 Definitions—For definitions of terms used in this test
Silver µg/g 18.0 to 8000
method, refer to Terminology E135.
Sulfur % 10.0 to 36.0
Tin % 0.004 to 0.012
Zinc % 0.005 to 4.30
4. Summary of Test Method
1.2 This standard does not purport to address all of the
4.1 The analyst has the option of either digesting the sample
safety concerns, if any, associated with its use. It is the
in nitric and hydrochloric acids or nitric and perchloric acids,
responsibility of the user of this standard to establish appro-
depending on their preference and equipment availability. The
priate safety and health practices and determine the applica-
filtered solutions are aspirated into an air-acetylene flame of an
bility of regulatory limitations prior to its use.
atomic absorption spectrophotometer. Spectral energy at ap-
proximately 328.1 nm from a silver hollow cathode lamp is
1
This test method is under the jurisdiction of ASTM Committee E01 on
2
Analytical Chemistry for Metals, Ores, and Related Materials and is the direct For referenced ASTM standards, visit the ASTM website, www.astm.org, or
responsibility of Subcommittee E01.02 on Ores, Concentrates, and Related Metal- contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
lurgical Materials. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved June 1, 2007. Published June 2007. Originally the ASTM website.
3
approved in 1997. Last previous edition approved in 2002 as E1898 - 02. DOI: The last approved version of this historical standard is referenced on
10.1520/E1898-07. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1898 − 07
passed through the flame and the absorbance is measured.This 8.4 Silver Standard Solution B(1mL=10µgAg)—Pipet10
absorbance is compared with the absorbance of a series of mL of Silver Standard Solution A into a 1-L volumetric flask
standard calibration solutions. containing about 500 mL of water and 250 mL of HCl. Mix,
cool, dilute to the mark, and remix. If turbid, discard the
5. Significance and Use
solution and repeat the preparation. Transfer to a dark bottle.
Prepare immediately before use.
5.1 In the primary metallurgical processes used by the
mineral processing industry for copper bearing ores, copper
9. Hazards
and silver associated with sulfide mineralization are concen-
trated by the process of flotation for recovery of the m
...

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ASTM E135-23a(Terminology)
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3.1 Definitions given in Section 4 are intended for use in all standards on analytical chemistry for metals, ores, and related materials. The definitions should be used uniformly and consistently. The purpose of these definitions is to promote clear understanding and interpretation of the standards in which the terms are used.
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1.3 The date of last reapproval or revision of a term is in parentheses at the end of the definition.  
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4.1 This practice covers all aspects of sampling and preparing steel and iron for chemical analysis as defined in Test Methods, Practices, and Definitions A751 and Specification A48/A48M. Such subjects as sampling location and the sampling of lots are defined.  
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1.1 This practice covers the sampling of all grades of steel, both cast and wrought, and all types (grades) of cast irons and blast furnace iron for chemical and spectrochemical determination of composition. This practice is similar to ISO 14284.  
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Sections  
Requirements for Sampling and Sample Preparation  
6  
General  
6.1  
Sample  
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Liquid Iron for Steelmaking and Pig Iron Production  
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General  
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Spoon Sampling  
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Probe Sampling  
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Liquid Iron for Cast Iron Production  
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General  
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Spoon Sampling  
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Probe Sampling  
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General  
9.1  
Probe Sampling  
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Spoon Sampling  
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Sampling and Sample Preparation for the Determination  
9.5  
of Oxygen  
Sampling and Sample Preparation for the Determination  
9.6  
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General  
10.1  
Increment Sampling  
10.2  
Preparation of a Sample for Analysis  
10.3  
Cast Iron Products  
11  
General  
11.1  
Sampling and Sample Preparation  
11.2  
Sections  
Steel Products  
12  
General  
12.1  
Selection of a Laboratory Sample or a Sample for  
12.2  
Analysis from a Cast Product  
Selection of a Laboratory Sample or a Sample for  
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Analysis from a Wrought Product  
Preparation of a Sample for Analysis  
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Sampling of Leaded Steel  
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Sampling and Sample Preparation for the Determination  
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Annexes  
Sampling Probes for Use with Liquid Iron and Steel  
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Standard Test Method for Analysis of Cast Iron by Spark Atomic Emission Spectrometry

SIGNIFICANCE AND USE
5.1 The chemical composition of cast iron alloys shall be determined accurately in order to ensure the desired metallurgical properties. This procedure is suitable for manufacturing control and inspection testing.
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1.1 This test method covers the analysis of cast iron by spark atomic emission spectrometry for the following elements in the ranges shown (Note 1):
Ranges, %  
Elements  
Applicable Range, %  
Quantitative Range, %A  
Carbon  
1.9 to 3.8  
1.90 to 3.8  
Chromium  
0 to 2.0  
0.025 to 2.0  
Copper  
0 to 0.75  
0.015 to 0.75  
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0.03 to 1.8  
Molybdenum  
0 to 1.2  
0.01 to 1.2  
Nickel  
0 to 2.0  
0.02 to 2.0  
Phosphorus  
0 to 0.4  
0.005 to 0.4  
Silicon  
0 to 2.5  
0.15 to 2.5  
Sulfur  
0 to 0.08  
0.01 to 0.08  
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0 to 0.14  
0.004 to 0.14  
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0 to 0.12  
0.003 to 0.12  
Vanadium  
0 to 0.22  
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5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.  
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1.1 This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:    
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Application
Range (wt.%)  
Quantitative
Range (wt.%)  
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0.009 to 8.0  
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Cobalt  
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Chromium  
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0.005 to 4.0  
Copper  
0–0.6  
0.004 to 0.5  
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0.003 to 0.01  
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1.4 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety hazards statements are given in Section 9.  
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ASTM E1898-21(Test Method)
Standard Test Method for Determination of Silver in Copper Concentrates by Flame Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
5.1 In the primary metallurgical processes used by the mineral processing industry for copper bearing ores, copper and silver associated with sulfide mineralization are concentrated by the process of flotation for recovery of the metals.  
5.2 This test method is a comparative method and is intended to be a referee method for compliance with compositional specifications for metal content or to monitor processes.  
5.3 It is assumed that all who use this method will be trained analysts capable of performing skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of silver in the range of 13 μg/g to 500 μg/g by acid dissolution of the silver and measurement by atomic absorption spectrometry. Copper concentrates are internationally traded within the following content ranges:    
Element  
Unit  
Content Range  
Aluminum  
%  
0.05  
to  
2.50  
Antimony  
%  
0.0001  
to  
4.50  
Arsenic  
%  
0.01  
to  
0.50  
Barium  
%  
0.003  
to  
0.10  
Bismuth  
%  
0.001  
to  
0.16  
Cadmium  
%  
0.0005  
to  
0.04  
Calcium  
%  
0.05  
to  
4.00  
Carbon  
%  
0.10  
to  
0.90  
Chlorine  
%  
0.001  
to  
0.006  
Chromium  
%  
0.0001  
to  
0.10  
Cobalt  
%  
0.0005  
to  
0.20  
Copper  
%  
10.0  
to  
44.0  
Fluorine  
%  
0.001  
to  
0.10  
Gold  
μg/g  
1.40  
to  
100.0  
Iron  
%  
12.0  
to  
30.0  
Lead  
%  
0.01  
to  
1.40  
Magnesium  
%  
0.02  
to  
2.00  
Manganese  
%  
0.009  
to  
0.10  
Mercury  
μg/g  
0.05  
to  
50.0  
Molybdenum  
%  
0.002  
to  
0.25  
Nickel  
%  
0.0001  
to  
0.08  
Silicon  
%  
0.40  
to  
20.0  
Silver  
μg/g  
18.0  
to  
8000  
Sulfur  
%  
10.0  
to  
36.0  
Tin  
%  
0.004  
to  
0.012  
Zinc  
%  
0.005  
to  
4.30  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E1805-21(Test Method)
Standard Test Method for Determination of Gold in Copper Concentrates by Fire Assay Gravimetry

SIGNIFICANCE AND USE
5.1 In the metallurgical process used in the mining industries, gold is often carried along with copper during the flotation concentration process. Metallurgical accounting, process control, and concentrate evaluation procedures for this type of material depend on an accurate, precise measurement of the gold in the copper concentrate. This test method is intended to be a reference method for metallurgical laboratories and a referee method to settle disputes in commercial transactions. It is also a definitive method intended to test materials for compliance with compositional specifications and to provide data for certification of reference materials. It is essential that each performance of the method be validated by applying it to appropriate reference materials at the same time and in the same manner as it is applied to the unknowns.  
5.2 It is assumed that all who use this test method will be trained analysts capable of performing skillfully and safely. It is expected that the work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method is for the determination of gold in copper concentrates in the content range from 0.2 μg/g to 17 μg/g.
Note 1: The lower scope limit is set in accordance with Practice E1601.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 11.3.1, 11.5.4, and 11.6.5.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E508-21(Test Method)
Standard Test Method for Determination of Calcium and Magnesium in Iron Ores by Flame Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
5.1 This test method is intended as a referee method for compliance with compositional specifications for impurity content. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of calcium and magnesium in iron ores, concentrates, and agglomerates in the mass fraction (%) range from 0.05 % to 5 % of calcium and 0.05 % to 3 % of magnesium.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E507-21(Test Method)
Standard Test Method for Determination of Aluminum in Iron Ores by Flame Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
5.1 This test method is intended as a referee method for compliance with compositional specifications for impurity content. It is assumed that all who use this procedure will be trained analysts capable of performing common laboratory practices skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Follow appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method covers the determination of aluminum in iron ores, concentrates, and agglomerates in the mass fraction (%) range from 0.1 to 5.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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  • Standard
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