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ASTM D509-05

(Test Method)

Standard Test Methods of Sampling and Grading Rosin

Standard Test Methods of Sampling and Grading Rosin

SIGNIFICANCE AND USE
Rosin is an important product of the centuries old Naval Stores industry and is produced and consumed in many countries throughout the world. Consequently, reliable methods of sampling and grading rosin are necessary. The test methods based on the use of the USDA Official Standards described herein, were developed many years ago for the sampling and grading of rosin and are similar to those included in the Naval Stores Act.3  
Although these test methods based on the use of the USDA Official Standards are still applicable, many additional test methods are now used to grade rosin. In particular, the color of rosin is now more commonly reported using the Gardner color scale rather than the USDA Official Standards. In addition, Test Methods E 28, D 465, and D 5974 are widely used to assess the quality of rosin in addition to the color grading methods described in this standard.
SCOPE
1.1 These test methods cover procedures for sampling and determining the grade of rosin delivered in commercial bags, barrels, drums or in molten form. Although developed for rosin, these methods can also be used for the grading of modified rosins and rosin based resins.
Note1—All rosin sold in interstate commerce must be described by reference to the U. S. Standards for rosin, and is therefore subject to grading prior to such sale. The grading procedure described in these test methods is used for checking grades or regrading after the rosin has moved from the primary markets to distributing or consuming points.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
14-May-2005
ICS
87.060.20 - Binders
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.34 - Pine Chemicals and Hydrocarbon Resins
Current Stage
Ref Project

Relations

Replaces
ASTM D509-03 - Standard Test Methods of Sampling and Grading Rosin
Effective Date
15-May-2005
Replaced By
ASTM D509-05(2011)e1 - Standard Test Methods of Sampling and Grading Rosin
Effective Date
15-May-2005
Referred By
ASTM D5974-20 - Standard Test Methods for Fatty and Rosin Acids in Tall Oil Fractionation Products by Capillary Gas Chromatography
Effective Date
15-May-2005
Referred By
ASTM B678-86(2017) - Standard Test Method for Solderability of Metallic-Coated Products
Effective Date
15-May-2005
Referred By
ASTM B32-20 - Standard Specification for Solder Metal
Effective Date
15-May-2005
Referred By
ASTM D1065-18(2022) - Standard Test Method for Unsaponifiable Matter in Pine Chemicals, Including Rosin, Tall Oil, and Related Products
Effective Date
15-May-2005

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ASTM D509-05 - Standard Test Methods of Sampling and Grading RosinASTM D509-05 - Standard Test Methods of Sampling and Grading Rosin
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ASTM D509-05 - Standard Test Methods of Sampling and Grading Rosin
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D509 – 05
Standard Test Methods of
1
Sampling and Grading Rosin
This standard is issued under the fixed designation D509; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Significance and Use
1.1 These test methods cover procedures for sampling and 3.1 Rosin is an important product of the centuries old Naval
determining the grade of rosin delivered in commercial bags, Stores industry and is produced and consumed in many
barrels, drums or in molten form. Although developed for countries throughout the world. Consequently, reliable meth-
rosin, these methods can also be used for the grading of ods of sampling and grading rosin are necessary. The test
modified rosins and rosin based resins. methods based on the use of the USDA Official Standards
described herein, were developed many years ago for the
NOTE 1—All rosin sold in interstate commerce must be described by
sampling and grading of rosin and are similar to those included
reference to the U. S. Standards for rosin, and is therefore subject to
3
in the Naval Stores Act.
grading prior to such sale. The grading procedure described in these test
3.2 Although these test methods based on the use of the
methods is used for checking grades or regrading after the rosin has
moved from the primary markets to distributing or consuming points.
USDA Official Standards are still applicable, many additional
test methods are now used to grade rosin. In particular, the
1.2 The values stated in SI units are to be regarded as the
color of rosin is now more commonly reported using the
standard. The values given in parentheses are for information
Gardner color scale rather than the USDA Official Standards.
only.
In addition, Test Methods E28, D465, and D5974 are widely
1.3 This standard does not purport to address all of the
used to assess the quality of rosin in addition to the color
safety concerns, if any, associated with its use. It is the
grading methods described in this standard.
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
4. Sampling
bility of regulatory limitations prior to use.
4.1 Number of Packages to Be Sampled—A preliminary
2. Referenced Documents sampling of 20 % of the entire lot or shipment shall be made.
2
Ifthegradeof85 %ormoreofthenumberofsuchpreliminary
2.1 ASTM Standards:
samples agrees with the grade indicated on the package or
D465 Test Methods for Acid Number of Naval Stores
invoice, with none of the samples disagreeing by more than
Products Including Tall Oil and Other Related Products
one grade, the original grading shall be considered confirmed
D1544 Test Method for Color of Transparent Liquids
and the shipment accepted as a good delivery. If the grades of
(Gardner Color Scale)
more than 15 % of the preliminary samples are in disagree-
D5974 Test Methods for Fatty and Rosin Acids in Tall Oil
ment, or if any appreciable number are under grade by more
Fractionation Products by Capillary Gas Chromatography
thanonegrade,additionalpackagesinthelottomakeupatotal
D6090 Test Method for Softening Point Resins (Mettler
equal to not less than 50 % of the entire shipment (preferably
Cup and Ball Method)
the entire shipment if accessible and not too great) shall be
D6166 Test Method for Color of Naval Stores and Related
sampled.Thefindingsonsuchlargerquantityshallbeaccepted
Products (Instrumental Determination of Gardner Color)
as the basis for settlement between the purchaser and the seller.
E28 Test Methods for Softening Point of Resins Derived
4.2 Method of Sampling—Take samples that are approxi-
from Naval Stores by Ring-and-Ball Apparatus
7
matelycubicalinshapeandexactly22.225mm( ⁄8in.)thickin
the direction in which they are to be viewed, by any of the
following methods:
1
These test methods are under the jurisdiction of ASTM Committee D01 on
(a) by cutting or cleaving the same from a lump of rosin
Paint and Related Coatings, Materials, and Applications and are the direct
removed from the solid mass in the barrel or drum, the top side
responsibility of Subcommittee D01.34 on Naval Stores.
Current edition approved May 15, 2005. Published June 2005. Originally of which lump shall come from not less than 101.6 mm (4 in.)
approved in 1938. Last previous edition approved in 2003 as D509 – 03. DOI:
below the surface of the rosin.
10.1520/D0509-05.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Docu
...

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3.1 Rosin is an important product of the centuries old Naval Stores industry, now known as the Pine Chemical industry, and is produced and consumed in many countries throughout the world. Consequently, reliable methods of sampling and grading rosin are necessary. The test methods based on the use of the USDA Official Standards described herein, were developed many years ago for the sampling and grading of rosin and are similar to those included in the Naval Stores Act.3  
3.2 Although these test methods based on the use of the USDA Official Standards are still applicable, many additional test methods are now used to grade rosin. In particular, the color of rosin is now more commonly reported using the Gardner color scale rather than the USDA Official Standards. In addition, Test Methods E28, D465, and D5974 are widely used to assess the quality of rosin in addition to the color grading methods described in this standard. The Naval Stores Act of 1923 established the methods for grading rosin and authorized the “Official Naval Stores Standard of the United States”. Based upon a request from the chairman of the ASTM D01.34 Pine Chemicals and Hydrocarbon Resins subcommittee requesting that the Gardner color scale be used for grading the color of rosin, a letter from the Food and Drug Administration was received and is archived in Pine Chemicals Association4 files. It documents a no-objection response to the request to use the Gardner color scale as a standard for grading rosin and rosin derivatives. The no-objection response was conditioned on having a reliable correlation between the USRG Scale (the “Official Naval Stores Standard of the United States”) and the Gardner Color Scale. A correlation study of color measurements on the Gardner Color Scale and the USRG Scale was carried out by scientists at Tintometer, Inc, Amesbury, England. The results of the correlation were submitted to the Food and Drug Administration as supporting evidence for the use of the Gardner Co...
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1.1 These test methods cover procedures for sampling and determining the grade of rosin delivered in commercial bags, barrels, drums or in molten form. Although developed for rosin, these methods can also be used for the grading of modified rosins and rosin based resins.
Note 1: All rosin sold in interstate commerce must be described by reference to the U. S. Standards for rosin, and is therefore subject to grading prior to such sale. The grading procedure described in these test methods is used for checking grades or regrading after the rosin has moved from the primary markets to distributing or consuming points.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SIGNIFICANCE AND USE
3.1 Rosin is an important product of the centuries old Naval Stores industry, now known as the Pine Chemical industry, and is produced and consumed in many countries throughout the world. Consequently, reliable methods of sampling and grading rosin are necessary. The test methods based on the use of the USDA Official Standards described herein, were developed many years ago for the sampling and grading of rosin and are similar to those included in the Naval Stores Act.3  
3.2 Although these test methods based on the use of the USDA Official Standards are still applicable, many additional test methods are now used to grade rosin. In particular, the color of rosin is now more commonly reported using the Gardner color scale rather than the USDA Official Standards. In addition, Test Methods E28, D465, and D5974 are widely used to assess the quality of rosin in addition to the color grading methods described in this standard. The Naval Stores Act of 1923 established the methods for grading rosin and authorized the “Official Naval Stores Standard of the United States”. Based upon a request from the chairman of the ASTM D01.34 Pine Chemicals and Hydrocarbon Resins subcommittee requesting that the Gardner color scale be used for grading the color of rosin, a letter from the Food and Drug Administration was received and is archived in Pine Chemicals Association4 files. It documents a no-objection response to the request to use the Gardner color scale as a standard for grading rosin and rosin derivatives. The no-objection response was conditioned on having a reliable correlation between the USRG Scale (the “Official Naval Stores Standard of the United States”) and the Gardner Color Scale. A correlation study of color measurements on the Gardner Color Scale and the USRG Scale was carried out by scientists at Tintometer, Inc, Amesbury, England. The results of the correlation were submitted to the Food and Drug Administration as supporting evidence for the use of the Gardner Co...
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1.1 These test methods cover procedures for sampling and determining the grade of rosin delivered in commercial bags, barrels, drums or in molten form. Although developed for rosin, these methods can also be used for the grading of modified rosins and rosin based resins.
Note 1: All rosin sold in interstate commerce must be described by reference to the U. S. Standards for rosin, and is therefore subject to grading prior to such sale. The grading procedure described in these test methods is used for checking grades or regrading after the rosin has moved from the primary markets to distributing or consuming points.  
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1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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