Standard Test Method for Measuring Heat Stability of Resilient Flooring by Color Change

SIGNIFICANCE AND USE
3.1 Resilient floor covering is made by fusing polymer materials under heat or pressure, or both, in various manufacturing and decorating processes. The polymer material may be compounded with plasticizers, stabilizers, fillers, and other ingredients for processibility and product performance characteristics. The formulation of the compound can be varied considerably depending on the desired performance characteristics and methods of processing. See Practice D794 for additional significance and use information.  
3.1.1 Heat stability, which is resistance to discoloration from heat, is a basic requirement for processing and functional use.  
3.1.2 This test method provides a means of measuring the amount of color change in flooring products when subjected to elevated temperatures over a period of time (functional use of the flooring product).  
3.2 This test method is not intended to be a means of predicting the amount of color change that occurs during processing (manufacture).  
3.3 This test method specifies that a sample is subjected to 158°F ± 2°F (70°C ± 1°C) for 7 days, and the color difference is measured by a spectrophotometer and expressed as ΔE* units.Note 1—It is the intent that this test method be used for testing heat stability performance properties to be referenced in resilient flooring specifications.
SCOPE
1.1 This test method covers a procedure for determining the resistance of resilient floor covering to color change from exposure to elevated temperature over a specified period of time.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Apr-2013
Drafting Committee
Current Stage
Ref Project

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ASTM F1514-03(2013) - Standard Test Method for Measuring Heat Stability of Resilient Flooring by Color Change
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: F1514 − 03 (Reapproved 2013)
Standard Test Method for
Measuring Heat Stability of Resilient Flooring by Color
Change
This standard is issued under the fixed designation F1514; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope E691 Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method
1.1 This test method covers a procedure for determining the
resistance of resilient floor covering to color change from
3. Significance and Use
exposure to elevated temperature over a specified period of
3.1 Resilient floor covering is made by fusing polymer
time.
materials under heat or pressure, or both, in various manufac-
1.2 The values stated in inch-pound units are to be regarded
turing and decorating processes. The polymer material may be
as standard. The values given in parentheses are mathematical
compounded with plasticizers, stabilizers, fillers, and other
conversions to SI units that are provided for information only
ingredients for processibility and product performance charac-
and are not considered standard.
teristics. The formulation of the compound can be varied
1.3 This standard does not purport to address all of the considerably depending on the desired performance character-
safety concerns, if any, associated with its use. It is the istics and methods of processing. See Practice D794 for
responsibility of the user of this standard to establish appro- additional significance and use information.
priate safety, health, and environmental practices and deter- 3.1.1 Heat stability, which is resistance to discoloration
mine the applicability of regulatory limitations prior to use. from heat, is a basic requirement for processing and functional
1.4 This international standard was developed in accor- use.
dance with internationally recognized principles on standard- 3.1.2 This test method provides a means of measuring the
amount of color change in flooring products when subjected to
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom- elevated temperatures over a period of time (functional use of
the flooring product).
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
3.2 This test method is not intended to be a means of
predicting the amount of color change that occurs during
2. Referenced Documents
processing (manufacture).
2.1 ASTM Standards:
3.3 This test method specifies that a sample is subjected to
D794 Practice for Determining Permanent Effect of Heat on
158°F 6 2°F (70°C 6 1°C) for 7 days, and the color difference
Plastics (Withdrawn 1998)
is measured by a spectrophotometer and expressed as ∆E*
D2244 Practice for Calculation of Color Tolerances and
units.
Color Differences from Instrumentally Measured Color
NOTE 1—It is the intent that this test method be used for testing heat
Coordinates
stability performance properties to be referenced in resilient flooring
E177 Practice for Use of the Terms Precision and Bias in
specifications.
ASTM Test Methods
4. Apparatus
4.1 CirculatingAirOven, which can be maintained at 158°F
ThistestmethodisunderthejurisdictionofASTMCommitteeF06onResilient
6 2°F (70°C 6 1°C).
Floor Coverings and is the direct responsibility of Subcommittee F06.20 on Test
Methods.
4.2 SuitableSpectrophotometerorColorimeter with a mini-
Current edition approved May 1, 2013. Published May 2013. Originally
mum ⁄4 in. (6.35 mm) diameter opening having both a cool
approved in 1995. Last previous edition approved in 2008 as F1514 – 03 (2008).
white fluorescent (CWF) and daylight light (D-65) sources that
DOI: 10.1520/F1514-03R13.
measure color in CIE L*, a*, b* using CIE 10° Standard
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Observer and Specular Included. See Test Method D2244.
Standards volume information, refer to the standard’s Document Summary page on
When an individual color cannot be totally covered within the
the ASTM website.
⁄4 in. spectrophotometer opening, then the largest spectropho-
The last approved version of this historical standard is referenced on
www.astm.org. tometer opening shall be used.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
F1514 − 03 (2013)
4.3 A suitable holder rack that separates samples a mini- 7.2 Record initial and final L*, a*, b*, and ∆E* values for
mum ⁄2 in. (12.70 mm) in a standing or vertical position. each specimen and report the individual and average ∆E*
values.
5. Hazards
8. Precision and Bias
5.1 Cautions:
8.1 Interlaboratory Test Program —An interlaboratory
5.1.1 Do not stack specimens while being exposed to
study evaluating the color stability of resilient vinyl flooring to
elevated temperatures.
the effects of exposure to heat was run in 1991 through 1993.
5.1.2 Be sure each specimen is marked in the corner and on
Six
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