Standard Test Method for Measuring Heat Stability of Resilient Vinyl Flooring by Color Change

SIGNIFICANCE AND USE
Resilient floor covering is made by fusing polymer materials under heat or pressure, or both, in various manufacturing and decorating processes. The polymer material may be compounded with plasticizers, stabilizers, fillers, and other ingredients for processibility and product performance characteristics. The formulation of the compound can be varied considerably depending on the desired performance characteristics and methods of processing. See Practice D 794 for additional significance and use information.
3.1.1 Heat stability, which is resistance to discoloration from heat, is a basic requirement for processing and functional use.
3.1.2 This test method provides a means of measuring the amount of color change in flooring products when subjected to elevated temperatures over a period of time (functional use of the flooring product).
This test method is not intended to be a means of predicting the amount of color change that occurs during processing (manufacture).
This test method specifies that a sample is subjected to 158°F ± 2°F (70°C ± 1°C) for 7 days, and the color difference is measured by a spectrophotometer and expressed as ΔE* units.
Note 1—It is the intent that this test method be used for testing heat stability performance properties to be referenced in resilient flooring specifications.
SCOPE
1.1 This test method covers a procedure for determining the resistance of resilient floor covering to color change from exposure to elevated temperature over a specified period of time.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.

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Publication Date
09-Mar-2003
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ASTM F1514-03 - Standard Test Method for Measuring Heat Stability of Resilient Vinyl Flooring by Color Change
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:F1514–03
Standard Test Method for
Measuring Heat Stability of Resilient Flooring by Color
1
Change
This standard is issued under the fixed designation F 1514; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope istics and methods of processing. See Practice D 794 for
additional significance and use information.
1.1 This test method covers a procedure for determining the
3.1.1 Heat stability, which is resistance to discoloration
resistance of resilient floor covering to color change from
from heat, is a basic requirement for processing and functional
exposure to elevated temperature over a specified period of
use.
time.
3.1.2 This test method provides a means of measuring the
1.2 This standard does not purport to address all of the
amount of color change in flooring products when subjected to
safety concerns, if any, associated with its use. It is the
elevated temperatures over a period of time (functional use of
responsibility of the user of this standard to establish appro-
the flooring product).
priate safety and health practices and determine the applica-
3.2 This test method is not intended to be a means of
bility of regulatory limitations prior to use.
predicting the amount of color change that occurs during
1.3 The values stated in inch-pound units are to be regarded
processing (manufacture).
as the standard. The values given in parentheses are for
3.3 This test method specifies that a sample is subjected to
information only.
158°F 6 2°F (70°C 6 1°C) for 7 days, and the color difference
2. Referenced Documents
is measured by a spectrophotometer and expressed as DE*
units.
2.1 ASTM Standards:
D 794 Practice for Determining Permanent Effect of Heat
NOTE 1—It is the intent that this test method be used for testing heat
2
on Plastics
stability performance properties to be referenced in resilient flooring
D 2244 Test Method for Calculation of Color Differences specifications.
3
from Instrumentally Measured Color Coordinates
4. Apparatus
E 177 Practice for Use of the Terms Precision and Bias in
4
4.1 CirculatingAirOven, which can be maintained at 158°F
ASTM Test Methods
6 2°F (70°C 6 1°C).
E 691 Practice for Conducting an Interlaboratory Study to
4
4.2 Suitable Spectrophotometer or Colorimeter with a
Determine the Precision of a Test Method
1
minimum ⁄4 in. (6.35 mm) diameter opening having both a
3. Significance and Use
coolwhitefluorescent(CWF)anddaylightlight(D-65)sources
that measure color in CIE L*, a*, b* using CIE 10° Standard
3.1 Resilient floor covering is made by fusing polymer
Observer and Specular Included. See Test Method D 2244.
materials under heat or pressure, or both, in various manufac-
When an individual color cannot be totally covered within the
turing and decorating processes. The polymer material may be
1
⁄4 in. spectrophotometer opening, then the largest spectropho-
compounded with plasticizers, stabilizers, fillers, and other
tometer opening shall be used.
ingredients for processibility and product performance charac-
4.3 A suitable holder rack that separates samples a mini-
teristics. The formulation of the compound can be varied
1
mum ⁄2 in. (12.70 mm) in a standing or vertical position.
considerably depending on the desired performance character-
5. Hazards
5.1 Cautions:
1
ThistestmethodisunderthejurisdictionofASTMCommitteeF06onResilient
5.1.1 Do not stack specimens while being exposed to
Floor Coverings and is the direct responsibility of Subcommittee F06.30 on Test
elevated temperatures.
Methods-Performance.
Current edition approved March 10, 2003. Published May 2003. Originally
5.1.2 Be sure each specimen is marked in the corner and on
approved in 1995. Last previous edition approved in 1998 as F 1514 – 98.
the back for easy identification.
2
Annual Book of ASTM Standards, Vol 08.01.
3 5.1.3 Monitor temperature during duration of test in oven to
Annual Book of ASTM Standards, Vol 06.01.
4
Annual Book of ASTM Standards, Vol 14.02. ensure maintenance of proper temperature.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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F1514–03
5.1.4 Be sure color measuring equipment is properly the effects of exposure to heat was run in 1991 through 1993.
warmed-up and calibrated prior to use. Six laboratories tested three categories of an experimental
5.1.5 Be sure specimens are held flat when measuring color.
unprinted resilient sheet flooring structure having a 0.010 in.
(0.254 mm) transparent top layer containing varying levels of
6. Procedure
stabilize
...

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