ASTM E2119-20
(Practice)Standard Practice for Quality Systems for Conducting In Situ Measurements of Lead Content in Paint or Other Coatings Using Field-Portable X-Ray Fluorescence (XRF) Devices
Standard Practice for Quality Systems for Conducting In Situ Measurements of Lead Content in Paint or Other Coatings Using Field-Portable X-Ray Fluorescence (XRF) Devices
SIGNIFICANCE AND USE
5.1 This practice provides procedures to generate and document QC data for ensuring that an XRF is operating within acceptable tolerances throughout the testing period when being used to collect lead results during a lead-based paint (LBP) inspection for the purposes of generating lead classification results.
5.2 This practice is intended to supplement XRF instrument manufacturer protocols and PCSs4 through the use of QA and QC procedures to provide uniform lead testing practices among the wide variety of available field-portable XRF instruments.
Note 1: In the United States, an XRF used to perform a lead-based paint inspection shall be utilized according to the PCS for the particular instrument model in use.
5.3 While the QC results collected using this practice can provide assurances that an XRF instrument is operating within acceptable tolerances, this practice does not determine an actual level of confidence for a classification result obtained from an XRF measurement.
5.4 This practice does not address selection of test locations or representative sampling for leaded paint. Additional information on conducting measurements of lead in leaded paint or other coatings may be found in Guide E2115 and the HUD Guidelines, Chapter 7.
5.5 This practice involves the use of field-portable XRF instruments that may contain radioactive materials that emit X-rays and gamma rays. These instruments are intended for use only by qualified, trained personnel.
5.6 The use of field-portable XRF instruments for measurement of lead may not accurately reveal low but still potentially hazardous levels of lead.
SCOPE
1.1 This practice covers the collection and documentation of quality control (QC) measurements for determining acceptable levels of instrumental performance when using field-portable energy-dispersive X-ray fluorescence spectrometry devices (XRFs) for the purposes of generating lead classification results from measurements on paint and other coating films within buildings and related structures.
1.1.1 This practice is not designed to determine the presence of a hazard as defined by authorities having jurisdiction in the United States or other jurisdictions. See Guide E2115 and the HUD Guidelines for more information.
1.2 QC procedures covered in this provisional practice include the performance of calibration checks, substrate bias checks, and specific instructions for documenting the collected data for later use in reporting the results.
1.3 No detailed operating instructions are provided because of differences among the various makes and models of suitable instruments. Instead, the analyst is to follow the instructions provided by the manufacturer of the particular XRF device or other relevant sources of information on XRF operation.
1.4 This practice contains notes which are explanatory and are not part of the mandatory requirements of this provisional practice.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2119 − 20
Standard Practice for
Quality Systems for Conducting In Situ Measurements of
Lead Content in Paint or Other Coatings Using Field-
1
Portable X-Ray Fluorescence (XRF) Devices
This standard is issued under the fixed designation E2119; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.7 This international standard was developed in accor-
dance with internationally recognized principles on standard-
1.1 Thispracticecoversthecollectionanddocumentationof
ization established in the Decision on Principles for the
quality control (QC) measurements for determining acceptable
Development of International Standards, Guides and Recom-
levels of instrumental performance when using field-portable
mendations issued by the World Trade Organization Technical
energy-dispersive X-ray fluorescence spectrometry devices
Barriers to Trade (TBT) Committee.
(XRFs) for the purposes of generating lead classification
results from measurements on paint and other coating films
2. Referenced Documents
within buildings and related structures.
2
1.1.1 Thispracticeisnotdesignedtodeterminethepresence
2.1 ASTM Standards:
of a hazard as defined by authorities having jurisdiction in the
D1356 Terminology Relating to Sampling and Analysis of
United States or other jurisdictions. See Guide E2115 and the
Atmospheres
HUD Guidelines for more information.
E1605 Terminology Relating to Lead in Buildings
E1645 Practice for Preparation of Dried Paint Samples by
1.2 QC procedures covered in this provisional practice
Hotplate or Microwave Digestion for Subsequent Lead
include the performance of calibration checks, substrate bias
Analysis
checks, and specific instructions for documenting the collected
E1729 Practice for Field Collection of Dried Paint Samples
data for later use in reporting the results.
for Subsequent Lead Determination
1.3 No detailed operating instructions are provided because
E2115 Guide for Conducting Lead Hazard Assessments of
of differences among the various makes and models of suitable
Dwellings and of Other Child-Occupied Facilities
instruments. Instead, the analyst is to follow the instructions
E3193 Test Method for Measurement of Lead (Pb) in Dust
provided by the manufacturer of the particular XRF device or
by Wipe, Paint, and Soil by Flame Atomic Absorption
other relevant sources of information on XRF operation.
Spectrophotometry (FAAS)
1.4 This practice contains notes which are explanatory and E3203 Test Method for Determination of Lead in Dried
are not part of the mandatory requirements of this provisional Paint, Soil, and Wipe Samples by Inductively Coupled
practice. Plasma-Optical Emission Spectroscopy (ICP-OES)
2.2 Other Documents:
1.5 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this 40 CFR 745 Lead-Based Paint Poisoning Prevention in
3
Certain Residential Structures
standard.
HUD Guidelines Guidelines for the Evaluation and Control
1.6 This standard does not purport to address all of the
of Lead-Based Paint Hazards in Housing, 2nd Edition,
safety concerns, if any, associated with its use. It is the
4
July 2012
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
1
This practice is under the jurisdiction ofASTM Committee D22 on Air Quality the ASTM website.
3
and is the direct responsibility of Subcommittee D22.12 on Sampling and Analysis AvailablefromUnitedStatesEnvironmentalProtectionAgency(EPA),William
of Lead for Exposure and Risk Assessment. Jefferson Clinton Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460,
Current edition approved Sept. 1, 2020. Published September 2020. Originally http://www.epa.gov.
4
approved in 2000. Last previous edition approved in 2016 as E2119 – 16. DOI: Available from U.S. Department of Housing and Urban Development, 451 7th
10.1520/E2119-20. Street, SW, Washington, DC 20410, http://www.hud.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2119 −
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2119 − 16 E2119 − 20
Standard Practice for
Quality Systems for Conducting In Situ Measurements of
Lead Content in Paint or Other Coatings Using Field-
1
Portable X-Ray Fluorescence (XRF) Devices
This standard is issued under the fixed designation E2119; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers the collection and documentation of quality control (QC) measurements for determining acceptable levels
of instrumental performance when using field-portable energy-dispersive x-rayX-ray fluorescence spectrometry devices (XRFs) for
the purposes of generating lead classification results from measurements on paint and other coating films within buildings and
related structures.
1.1.1 This practice is not designed to determine the presence of a hazard as defined by authorities having jurisdiction in the United
States or other jurisdictions. See Guide E2115 and the HUD Guidelines for more information.
1.2 QC procedures covered in this provisional practice include the performance of calibration checks, substrate bias checks, and
specific instructions for documenting the collected data for later use in reporting the results.
1.3 No detailed operating instructions are provided because of differences among the various makes and models of suitable
instruments. Instead, the analyst is to follow the instructions provided by the manufacturer of the particular XRF device or other
relevant sources of information on XRF operation.
1.4 This practice contains notes which are explanatory and are not part of the mandatory requirements of this provisional practice.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory requirementslimitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
1
This practice is under the jurisdiction of ASTM Committee D22 on Air Quality and is the direct responsibility of Subcommittee D22.12 on Sampling and
Analysis,Analysis of Lead,Lead for Exposure and Risk Assessment.
Current edition approved March 1, 2016Sept. 1, 2020. Published April 2016September 2020. Originally published as PS 95-98. approved in 2000. Last previous edition
approved in 20002016 as E2119-00 which was withdrawn January 2009 and reinstated in March 2016. DOI: 10.1520/E2119-16. – 16. DOI: 10.1520/E2119-20.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2119 − 20
2. Referenced Documents
2
2.1 ASTM Standards:
E1583D1356 Practice for Evaluating Laboratories Engaged in Determination of Lead in Paint, Dust, Airborne Particulates, and
Soil Taken From and Around Buildings and Related StructuresTerminology Relating to Sampling and Analysis of
Atmospheres
E1605 Terminology Relating to Lead in Buildings
E1613 Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES),
Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
E1645 Practice for Preparation of Dried Paint Samples by Hotplate or Microwave Digestion for Subsequent Lead Analysis
E1729 Practice for Field Collection of Dried Paint Samples for Subsequent Lead Determination
E2115 Guide for Conducting Lead Hazard Assessments of Dwellings and of Other Child-Occupied Facilities
E3193 Test Method for Measurement of Lead (Pb) in Dust by Wipe, Paint, and Soil by Flame Atomic Absorption
Spectrophotometry (FAAS)
E3203 Test Method for Determination of Lead in Dried Paint, Soil, and Wipe Samples by Inductively Coupled Plasma-Optical
Emission Spectroscopy (ICP-OES)
2.2 HUD Document:Other Documents:
3
4
...
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E2119 − 20
Standard Practice for
Quality Systems for Conducting In Situ Measurements of
Lead Content in Paint or Other Coatings Using Field-
1
Portable X-Ray Fluorescence (XRF) Devices
This standard is issued under the fixed designation E2119; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.7 This international standard was developed in accor-
dance with internationally recognized principles on standard-
1.1 This practice covers the collection and documentation of
ization established in the Decision on Principles for the
quality control (QC) measurements for determining acceptable
Development of International Standards, Guides and Recom-
levels of instrumental performance when using field-portable
mendations issued by the World Trade Organization Technical
energy-dispersive X-ray fluorescence spectrometry devices
Barriers to Trade (TBT) Committee.
(XRFs) for the purposes of generating lead classification
results from measurements on paint and other coating films
2. Referenced Documents
within buildings and related structures.
2
1.1.1 This practice is not designed to determine the presence
2.1 ASTM Standards:
of a hazard as defined by authorities having jurisdiction in the
D1356 Terminology Relating to Sampling and Analysis of
United States or other jurisdictions. See Guide E2115 and the
Atmospheres
HUD Guidelines for more information.
E1605 Terminology Relating to Lead in Buildings
E1645 Practice for Preparation of Dried Paint Samples by
1.2 QC procedures covered in this provisional practice
Hotplate or Microwave Digestion for Subsequent Lead
include the performance of calibration checks, substrate bias
Analysis
checks, and specific instructions for documenting the collected
E1729 Practice for Field Collection of Dried Paint Samples
data for later use in reporting the results.
for Subsequent Lead Determination
1.3 No detailed operating instructions are provided because
E2115 Guide for Conducting Lead Hazard Assessments of
of differences among the various makes and models of suitable
Dwellings and of Other Child-Occupied Facilities
instruments. Instead, the analyst is to follow the instructions
E3193 Test Method for Measurement of Lead (Pb) in Dust
provided by the manufacturer of the particular XRF device or
by Wipe, Paint, and Soil by Flame Atomic Absorption
other relevant sources of information on XRF operation.
Spectrophotometry (FAAS)
1.4 This practice contains notes which are explanatory and E3203 Test Method for Determination of Lead in Dried
are not part of the mandatory requirements of this provisional Paint, Soil, and Wipe Samples by Inductively Coupled
practice. Plasma-Optical Emission Spectroscopy (ICP-OES)
1.5 The values stated in SI units are to be regarded as 2.2 Other Documents:
40 CFR 745 Lead-Based Paint Poisoning Prevention in
standard. No other units of measurement are included in this
3
standard. Certain Residential Structures
HUD Guidelines Guidelines for the Evaluation and Control
1.6 This standard does not purport to address all of the
of Lead-Based Paint Hazards in Housing, 2nd Edition,
safety concerns, if any, associated with its use. It is the
4
July 2012
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
1
This practice is under the jurisdiction of ASTM Committee D22 on Air Quality the ASTM website.
3
and is the direct responsibility of Subcommittee D22.12 on Sampling and Analysis Available from United States Environmental Protection Agency (EPA), William
of Lead for Exposure and Risk Assessment. Jefferson Clinton Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460,
Current edition approved Sept. 1, 2020. Published September 2020. Originally http://www.epa.gov.
4
approved in 2000. Last previous edition approved in 2016 as E2119 – 16. DOI: Available from U.S. Department of Housing and Urban Development, 451 7th
10.1520/E2119-20. Street, SW, Washington, DC 20410, http://www.hud.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2119 − 20
3. Terminology 3.2.11.2 Discussion—For some makes and models of XRF
instruments, lead measurement values obtained near an a
...
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