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ASTM E1833-07

(Practice)

Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical Composition

Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical Composition

SIGNIFICANCE AND USE
This practice for sampling of cast blister copper is intended primarily to test such materials for compliance with compositional specifications. It is assumed that all who use these methods shall be trained samplers capable of performing common sampling procedures skillfully and safely.
The selection of correct test pieces and the preparation of a representative sample from such test pieces are necessary prerequisites to every analysis. The analytical results will be of little value unless the sample represents the average composition of the material from which it was prepared.
SCOPE
1.1 This practice describes a procedure for the sampling and sample preparation of cast blister copper for the determination of chemical composition.
1.2 This practice is intended to cover the general principles of sampling applicable to cast blister copper forms.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Jan-2007
ICS
71.040.50 - Physicochemical methods of analysis
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.05 - Cu, Pb, Zn, Cd, Sn, Be, Precious Metals, their Alloys, and Related Metals
Current Stage
Ref Project

Relations

Replaces
ASTM E1833-96(2001) - Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical Composition
Effective Date
01-Feb-2007
Replaced By
ASTM E1833-07a - Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical Composition
Effective Date
01-Nov-2007

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ASTM E1833-07 - Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical CompositionASTM E1833-07 - Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical Composition
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ASTM E1833-07 - Standard Practice for Sampling of Blister Copper in Cast Form for Determination of Chemical Composition
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E1833–07a
Standard Practice for
Sampling of Blister Copper in Cast Form for Determination
1
of Chemical Composition
This standard is issued under the fixed designation E1833; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope collected with a commercial vacuum cleaner and ground in a
cuttermill.Samplesizereductionisaccomplishedwiththeuse
1.1 Thispracticedescribesaprocedureforthesamplingand
of a riffle and Tyler screens.
sample preparation of cast blister copper for the determination
of chemical composition.
5. Significance and Use
1.2 This practice is intended to cover the general principles
5.1 This practice for sampling of cast blister copper is
of sampling applicable to cast blister copper forms.
intended primarily to test such materials for compliance with
1.3 This standard does not purport to address all of the
compositional specifications. It is assumed that all who use
safety concerns, if any, associated with its use. It is the
these methods shall be trained samplers capable of performing
responsibility of the user of this standard to establish appro-
common sampling procedures skillfully and safely.
priate safety and health practices and determine the applica-
5.2 The selection of correct test pieces and the preparation
bility of regulatory limitations prior to use.
of a representative sample from such test pieces are necessary
2. Referenced Documents prerequisitestoeveryanalysis.Theanalyticalresultswillbeof
2
little value unless the sample represents the average composi-
2.1 ASTM Standards:
tion of the material from which it was prepared.
E88 Practice for Sampling Nonferrous Metals and Alloys
in Cast Form for Determination of Chemical Composition
6. Apparatus
E135 Terminology Relating to Analytical Chemistry for
6.1 Bucket, plastic sack-lined.
Metals, Ores, and Related Materials
6.2 Cards, sampling information.
3. Terminology 6.3 Center Punch-Spring Steel.
6.4 Chalk, blackboard type.
3.1 For definitions of terms used in this practice, refer to
6.5 Cutter Mill or Hance Grinder.
Terminology E135.
3
6.6 Drill Bit, approximately ⁄4-in. diameter and a length
3.2
sufficient to penetrate the blister copper form completely.
3.3 lot, n—as used in this practice, the unit to be sampled,
6.7 Drill Press, commercial type, 610 rpm.
in pounds or pieces.
6.8 Electromagnet, hand-held or other permanent magnet.
4. Summary of Practice 6.9 Hammer, blacksmith type.
6.10 Pan, square metal or plastic, approximately 10 310
4.1 Each selected copper piece is drilled by means of a
3 in.
commercial drill press using a ⁄4-in. carbide-tipped, or tool
6.11 Paper, Kraft.
steel drill bit. The speed of sampling shall be so regulated that
6.12 Pulp Sample Sacks.
excessive heating, and consequent oxidation, is avoided.
6.13 Riffle, Jones Type, or other of similar design.
Carbide-tipped tools are recommended. Drill cuttings are
6.14 Rotap Machine, or similar sieve shaking device.
6.15 Template, drilling sequence, Fig. 1, Note 1.
1
This practice is under the jurisdiction ofASTM Committee E01 onAnalytical
6.16 Tyler Screen, 20 mesh, 12 in.
Chemistry for Metals, Ores and Related Materials and is the direct responsibility of
6.17 Tyler Screen, 60 mesh, 12 in.
Subcommittee E01.05 on Cu, Pb, Zn, Cd, Sn, Be, theirAlloys and Related Metals.
6.18 V-blender, or similar style mixer.
Current edition approved Nov. 1, 2007. Published November 2007. Originally
approved in 1996. Last previous edition approved in 2007 as E1833–07. 6.19 Vacuum Cleaner, commercial quality.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7. Procedure
Standards volume information, refer to the standard’s Document Summary page on
7.1 Sampling:
the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E1833–07a
7.2 Sample Preparation:
7.2.1 Adjust the cutter mill to coarse grind. Slowly pour the
grosssampleintothecuttermilltoreducelargeconglomerates
ofsample.PlacethegrosssampleintotheV-blenderandblend
for 15 min. Riffle the sample to split the gross sample into two
equal representative fractions,Aand B. Place theAincrement
intostorageandlabel,“bulkreserve”sample.Continuetoriffle
the B fraction until approximately 4000 g of sample have been
obtained. Place all surplus increment splits from the B fraction
NOTE 1—Template should have external measurements that would
into the A increment bulk storage container.
1
exactly fit
...

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ASTM E135-23a(Terminology)
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4.1 This practice covers all aspects of sampling and preparing steel and iron for chemical analysis as defined in Test Methods, Practices, and Definitions A751 and Specification A48/A48M. Such subjects as sampling location and the sampling of lots are defined.  
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Sections  
Requirements for Sampling and Sample Preparation  
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General  
6.1  
Sample  
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Selection of a Sample  
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General  
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Spoon Sampling  
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Probe Sampling  
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Preparation of a Sample for Analysis  
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Liquid Iron for Cast Iron Production  
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General  
8.1  
Spoon Sampling  
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General  
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Probe Sampling  
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Spoon Sampling  
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Preparation of a Sample for Analysis  
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Sampling and Sample Preparation for the Determination  
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Sampling and Sample Preparation for the Determination  
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General  
10.1  
Increment Sampling  
10.2  
Preparation of a Sample for Analysis  
10.3  
Cast Iron Products  
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General  
11.1  
Sampling and Sample Preparation  
11.2  
Sections  
Steel Products  
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General  
12.1  
Selection of a Laboratory Sample or a Sample for  
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Analysis from a Cast Product  
Selection of a Laboratory Sample or a Sample for  
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Analysis from a Wrought Product  
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Sampling of Leaded Steel  
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Annexes  
Sampling Probes for Use with Liquid Iron and Steel  
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1.3 The values stated in SI units are regarded as standard. No other units of measurement are included in this standard.  
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5.1 The chemical composition of cast iron alloys shall be determined accurately in order to ensure the desired metallurgical properties. This procedure is suitable for manufacturing control and inspection testing.
SCOPE
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5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.  
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Standard Test Method for Determination of Gold in Copper Concentrates by Fire Assay Gravimetry

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5.1 In the metallurgical process used in the mining industries, gold is often carried along with copper during the flotation concentration process. Metallurgical accounting, process control, and concentrate evaluation procedures for this type of material depend on an accurate, precise measurement of the gold in the copper concentrate. This test method is intended to be a reference method for metallurgical laboratories and a referee method to settle disputes in commercial transactions. It is also a definitive method intended to test materials for compliance with compositional specifications and to provide data for certification of reference materials. It is essential that each performance of the method be validated by applying it to appropriate reference materials at the same time and in the same manner as it is applied to the unknowns.  
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SCOPE
1.1 This test method is for the determination of gold in copper concentrates in the content range from 0.2 μg/g to 17 μg/g.
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