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ASTM D4255/D4255M-01(2007)

(Guide)

Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear Method

Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear Method

SIGNIFICANCE AND USE
These shear tests are designed to produce in-plane shear property data for material specifications, research and development, and design. Factors that influence the shear response and should therefore be reported include: material, methods of material preparation and lay-up, specimen stacking sequence, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, time at temperature, void content, and fiber volume reinforcement content. Properties that may be measured by this test method include:
5.1.1 In-plane shear stress versus shear strain response,
5.1.2 In-plane shear chord modulus of elasticity,
5.1.3 Offset shear stress, and
5.1.4 Maximum in-plane shear stress. In cases in which the strain at failure is greater than 5 %, the shear stress corresponding to 5 % shear strain should be reported.
SCOPE
1.1 This test method determines the in-plane shear properties of high-modulus fiber-reinforced composite materials by either of two procedures. In Procedure A, laminates clamped between two pairs of loading rails are tested. When loaded in tension the rails introduce shear forces in the specimen. In Procedure B, laminates clamped on opposite edges with a tensile or compressive load applied to a third pair of rails in the center are tested.
1.2 Application of this test method is limited to continuous-fiber or discontinuous-fiber-reinforced polymer matrix composites in the following material forms:
1.2.1 Laminates composed only of unidirectional fibrous laminae, with the fiber direction oriented either parallel or perpendicular to the fixture rails.
1.2.2 Laminates composed only of woven fabric filamentary laminae with the warp direction oriented either parallel or perpendicular to the fixture rails.
1.2.3 Laminates of balanced and symmetric construction, with the 0 direction oriented either parallel or perpendicular to the fixture rails.
1.2.4 Short-fiber-reinforced composites with a majority of the fibers being randomly distributed.Note 1
Additional test methods for determining in-plane shear properties of polymer matrix composites may be found in Test Methods D 5379/D 5379M and D 5448/D 5448M, and Practice D 3518/D 3518M.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. Within the text the inch-pounds units are shown in brackets. The values stated in each system are not exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.

General Information

Status
Historical
Publication Date
30-Apr-2007
ICS
83.140.20 - Laminated sheets
Technical Committee
D30 - Composite Materials
Drafting Committee
D30.04 - Lamina and Laminate Test Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D4255/D4255M-01 - Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear Method
Effective Date
01-May-2007
Replaced By
ASTM D4255/D4255M-15 - Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear Method
Effective Date
01-Apr-2015
Referred By
ASTM D4762-18 - Standard Guide for Testing Polymer Matrix Composite Materials
Effective Date
01-May-2007
Referred By
ASTM E2478-11(2022) - Standard Practice for Determining Damage-Based Design Stress for Glass Fiber Reinforced Plastic (GFRP) Materials Using Acoustic Emission
Effective Date
01-May-2007
Referred By
ASTM D7078/D7078M-20e1 - Standard Test Method for Shear Properties of Composite Materials by V-Notched Rail Shear Method
Effective Date
01-May-2007
Referred By
ASTM D6856/D6856M-03(2016) - Standard Guide for Testing Fabric-Reinforced “Textile” Composite Materials
Effective Date
01-May-2007

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ASTM D4255/D4255M-01(2007) - Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear MethodASTM D4255/D4255M-01(2007) - Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear Method
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ASTM D4255/D4255M-01(2007) - Standard Test Method for In-Plane Shear Properties of Polymer Matrix Composite Materials by the Rail Shear Method
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D4255/D4255M − 01(Reapproved 2007)
Standard Test Method for
In-Plane Shear Properties of Polymer Matrix Composite
1
Materials by the Rail Shear Method
This standard is issued under the fixed designation D4255/D4255M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope each system are not exact equivalents; therefore, each system
must be used independently of the other. Combining values
1.1 This test method determines the in-plane shear proper-
from the two systems may result in nonconformance with the
ties of high-modulus fiber-reinforced composite materials by
standard.
either of two procedures. In Procedure A, laminates clamped
between two pairs of loading rails are tested. When loaded in
2. Referenced Documents
tension the rails introduce shear forces in the specimen. In
2
2.1 ASTM Standards:
Procedure B, laminates clamped on opposite edges with a
D792 Test Methods for Density and Specific Gravity (Rela-
tensile or compressive load applied to a third pair of rails in the
tive Density) of Plastics by Displacement
center are tested.
D883 Terminology Relating to Plastics
1.2 Application of this test method is limited to continuous-
D2584 Test Method for Ignition Loss of Cured Reinforced
fiber or discontinuous-fiber-reinforced polymer matrix com-
Resins
posites in the following material forms:
D2734 TestMethodsforVoidContentofReinforcedPlastics
1.2.1 Laminates composed only of unidirectional fibrous
D3171 Test Methods for Constituent Content of Composite
laminae, with the fiber direction oriented either parallel or
Materials
perpendicular to the fixture rails.
D3518/D3518M Test Method for In-Plane Shear Response
1.2.2 Laminatescomposedonlyofwovenfabricfilamentary
of Polymer Matrix Composite Materials byTensileTest of
laminae with the warp direction oriented either parallel or
a 645° Laminate
perpendicular to the fixture rails.
D3878 Terminology for Composite Materials
1.2.3 Laminates of balanced and symmetric construction,
D5229/D5229M Test Method for MoistureAbsorption Prop-
withthe0°directionorientedeitherparallelorperpendicularto
erties and Equilibrium Conditioning of Polymer Matrix
the fixture rails.
Composite Materials
1.2.4 Short-fiber-reinforced composites with a majority of
D5379/D5379M Test Method for Shear Properties of Com-
the fibers being randomly distributed.
posite Materials by the V-Notched Beam Method
D5448/D5448M Test Method for Inplane Shear Properties
NOTE 1—Additional test methods for determining in-plane shear
properties of polymer matrix composites may be found in Test Methods
of Hoop Wound Polymer Matrix Composite Cylinders
D5379/D5379M and D5448/D5448M, and Practice D3518/D3518M.
E4 Practices for Force Verification of Testing Machines
1.3 This standard does not purport to address all of the
E6 Terminology Relating to Methods of Mechanical Testing
safety concerns, if any, associated with its use. It is the E111 Test Method for Young’s Modulus, Tangent Modulus,
responsibility of the user of this standard to establish appro-
and Chord Modulus
priate safety and health practices and determine the applica- E122 Practice for Calculating Sample Size to Estimate,With
bility of regulatory limitations prior to use.
Specified Precision, the Average for a Characteristic of a
1.4 The values stated in either SI units or inch-pound units Lot or Process
are to be regarded separately as standard. Within the text the
E177 Practice for Use of the Terms Precision and Bias in
inch-pounds units are shown in brackets. The values stated in ASTM Test Methods
E251 Test Methods for Performance Characteristics of Me-
tallic Bonded Resistance Strain Gages
1
This test method is under the jurisdiction of ASTM Committee D30 on
Composite Materials and is the direct responsibility of Subcommittee D30.04 on
2
Lamina and Laminate Test Methods. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved May 1, 2007. Published June 2007. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1983. Last previous edition approved in 2001 as D4255/D4255M – 01. Standards volume information, refer to the standard’s Document Summary page on
DOI: 10.1520/D4255_D4255M-01R07. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D4255/D4255M − 01 (2007)
to analytical dimensions when used with square brackets, as the
...

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1.1 This test practice defines the procedure for determination of the tensile strength of a tapered or stepped joint of polymer matrix composite materials. It is applicable to secondary bonded or co-bonded laminates with either unidirectional plies or woven fabric reinforcements. The materials to be bonded may be different material systems. In the bondline, a separate adhesive material may or may not be used (example: adhesives may be used with a prepreg system or may not be used with a wet lay-up repair system). The range of acceptable test laminates and thicknesses is described in 8.2.1.  
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1.3 Unidirectional (0° ply orientation) tape composites, textile composites, as well as multidirectional composite laminates, can be tested.  
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5.1 In most cases, because of the complexity of internal stresses and the variety of failure modes that can occur in this specimen, it is not generally possible to relate the short-beam strength to any one material property. However, failures are normally dominated by resin and interlaminar properties, and the test results have been found to be repeatable for a given specimen geometry, material system, and stacking sequence  (4).  
5.2 Short-beam strength determined by this test method can be used for quality control and process specification purposes. It can also be used for comparative testing of composite materials, provided that failures occur consistently in the same mode (5) .  
5.3 This test method is not limited to specimens within the range specified in Section 8, but is limited to the use of a loading span length-to-specimen thickness ratio of 4.0 and a minimum specimen thickness of 2.0 mm [0.08 in.].
SCOPE
1.1 This test method determines the short-beam strength of high-modulus fiber-reinforced composite materials. The specimen is a short beam machined from a curved or a flat laminate up to 6.00 mm [0.25 in.] thick. The beam is loaded in three-point bending.  
1.2 Application of this test method is limited to continuous- or discontinuous-fiber-reinforced polymer matrix composites, for which the elastic properties are balanced and symmetric with respect to the longitudinal axis of the beam.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM E1922/E1922M-22(Test Method)
Standard Test Method for Translaminar Fracture Toughness of Laminated and Pultruded Polymer Matrix Composite Materials

SIGNIFICANCE AND USE
5.1 The parameter KTL  determined by this test method is a measure of the resistance of a polymer matrix composite laminate to notch-tip damage and effective translaminar crack growth under opening mode loading. The result is valid only for conditions in which the damage zone at the notch tip is small compared with the notch length and the in-plane specimen dimensions. Alternately, for materials exhibiting distributed damage in a larger volume, observed force-displacement and discrete damage events are still valid structural responses for certain specific engineering applications.  
5.2 This test method can serve the following purposes. In research and development, (a) KTL data can quantitatively establish the effects of fiber and matrix variables and stacking sequence of the laminate on the translaminar fracture resistance of composite laminates; and (b) quantified distributed damage measurements can be used to validate progressive composite damage models. In structural design, KTL data can, within the constraints of the specimen geometry and loading, be used to assess composite laminate resistance to damage growth from edge flaws and notches.  
5.3 The translaminar fracture toughness,  KTL, as well as distributed damage observations, determined by this test method may be a function of the testing speed and temperature. This test method is intended for room temperature and quasi-static conditions, but it can apply to other test conditions provided that the requirements of 13.2 and 13.3 are met. Application of KTL in the design of service components should be made with awareness that the test parameters specified by this test may differ from service conditions, possibly resulting in a different material response than that seen in service. Distributed damage observations are also limited to the material and geometry tested, but may be more generally applied to a variety of structural analysis validation applications.  
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1.1 This test method covers the determination of translaminar fracture toughness, KTL, for laminated, molded, or pultruded polymer matrix composite materials of various fiber orientations using test results from monotonically loaded notched specimens. If the material response is such that the KTL calculation is not valid, alternate reporting methods are provided.  
1.2 This test method is applicable to room temperature laboratory air environments.  
1.3 Composite materials that can be tested by this test method are not limited by thickness or by type of polymer matrix or fiber, provided that the specimen sizes and the test results meet the requirements of this test method. This test method was developed primarily from test results of various carbon fiber – epoxy matrix laminates and from additional results of glass fiber – epoxy matrix, glass fiber-polyester matrix pultrusions and carbon fiber – bismaleimide matrix laminates (1-4, 5, 6).2  
1.4 A range of eccentrically loaded, single-edge-notch tension, ESE(T), specimen sizes with proportional planar dimensions is provided, but planar size may be variable and adjusted, with associated changes in the applied test load. Specimen thickness is a variable, independent of planar size.  
1.5 Specimen configurations other than those contained in this test method may be used. It is particularly important that the requirements discussed in 5.1 and 5.4 regarding contained notch-tip damage be met when using alternative specimen configurations in conjunction with the KTL calculation.  
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6.1 Within the text, the inch-pound units are shown ...

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ASTM
ASTM D5449/D5449M-22(Test Method)
Standard Test Method for Transverse Compressive Properties of Hoop Wound Polymer Matrix Composite Cylinders

SIGNIFICANCE AND USE
5.1 This test method is designed to produce transverse compressive property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors that influence the transverse compressive response and should therefore be reported are: material, method of material preparation, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, void content, and fiber volume fraction. Properties in the test direction that may be obtained from this test method are:  
5.1.1 Transverse compressive strength, σ22uc,  
5.1.2 Transverse compressive strain at failure, ε22uc,  
5.1.3 Transverse compressive modulus of elasticity, E22, and  
5.1.4 Poisson's ratio, γ21.
SCOPE
1.1 This test method determines the transverse compressive properties of wound polymer matrix composites reinforced by high-modulus continuous fibers. It describes testing of hoop wound (90°) cylinders in axial compression for determination of transverse compressive properties.  
1.2 The technical content of this test method has been stable since 1993 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this test method, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards, including editorial changes and incorporation of updated guidance on specimen preconditioning and environmental testing. The test method, therefore, should not be considered to include any significant changes in approach and practice since 1993. Future maintenance of the test method will only be in response to specific requests and performed only as technical support allows.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D5450/D5450M-22(Test Method)
Standard Test Method for Transverse Tensile Properties of Hoop Wound Polymer Matrix Composite Cylinders

SIGNIFICANCE AND USE
5.1 This test method is used to produce transverse tensile property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors which influence the transverse tensile response and should, therefore, be reported are: material, methods of material preparation, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, void content, and fiber volume fraction. Properties, in the test direction, which may be obtained from this test method include:  
5.1.1 Transverse Tensile Strength,    
5.1.2 Transverse Tensile Strain at Failure,    
5.1.3 Transverse Tensile Modulus of Elasticity,  E22, and  
5.1.4 Poisson's Ratio,  υ21.
SCOPE
1.1 This test method determines the transverse tensile properties of wound polymer matrix composites reinforced by high-modulus continuous fibers. It describes testing of hoop wound (90°) cylinders in axial tension for determination of transverse tensile properties.  
1.2 The technical content of this test method has been stable since 1993 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this test method, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards, including editorial changes and incorporation of updated guidance on specimen preconditioning and environmental testing. The test method, therefore, should not be considered to include any significant changes in approach and practice since 1993. Future maintenance of the test method will only be in response to specific requests and performed only as technical support allows.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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