ASTM D5217-17
(Guide)Standard Guide for Detection of Fouling and Degradation of Particulate Ion Exchange Materials
Standard Guide for Detection of Fouling and Degradation of Particulate Ion Exchange Materials
SIGNIFICANCE AND USE
4.1 Resins used in demineralization systems may deteriorate due to many factors including chemical attack, fouling by organic and inorganic materials, mishandling, or the effects of aging. Detection of degradation or fouling may be important in determining the cause of poor demineralizer performance.
SCOPE
1.1 This guide presents a series of tests and evaluations intended to detect fouling and degradation of particulate ion exchange materials. Suggestions on reducing fouling and on cleaning resins are given.
1.2 This guide is to be used only as an aid in the evaluation of particulate ion exchange material performance and does not purport to address all possible causes of unsatisfactory performance. The evaluations of mechanical and operational problems are not addressed.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5217 − 17
Standard Guide for
Detection of Fouling and Degradation of Particulate Ion
1
Exchange Materials
This standard is issued under the fixed designation D5217; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2687 PracticesforSamplingParticulateIon-ExchangeMa-
terials
1.1 This guide presents a series of tests and evaluations
D3087 Test Method for Operating Performance of Anion-
intended to detect fouling and degradation of particulate ion
Exchange Materials for Strong Acid Removal
exchange materials. Suggestions on reducing fouling and on
D3375 Test Method for Column Capacity of Particulate
cleaning resins are given.
Mixed Bed IonExchange Materials
1.2 This guide is to be used only as an aid in the evaluation
D3682 Test Method for Major and Minor Elements in
of particulate ion exchange material performance and does not
Combustion Residues from Coal Utilization Processes
purport to address all possible causes of unsatisfactory perfor-
D3683 Test Method for Trace Elements in Coal and Coke
mance. The evaluations of mechanical and operational prob-
Ash by Atomic Absorption
lems are not addressed.
D5042 Test Method for Estimating the Organic Fouling of
1.3 This standard does not purport to address all of the Particulate Anion Exchange Resins
safety concerns, if any, associated with its use. It is the
D6302 Practice for Evaluating the Kinetic Behavior of Ion
responsibility of the user of this standard to establish appro- Exchange Resins
priate safety, health, and environmental practices and deter-
E830 Test Method for Ash in the Analysis Sample of
3
mine the applicability of regulatory limitations prior to use. Refuse-Derived Fuel (Withdrawn 2011)
1.4 This international standard was developed in accor-
3. Terminology
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
3.1 Definitions:
Development of International Standards, Guides and Recom-
3.1.1 For definitions of terms used in this standard, refer to
mendations issued by the World Trade Organization Technical
Terminology D1129.
Barriers to Trade (TBT) Committee.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 air lance, v—to subject to a stream of air under
2. Referenced Documents
pressure.
2
2.1 ASTM Standards:
3.2.2 organic fouling, n—the buildup of organic material in
D1129 Terminology Relating to Water
or on anion exchange resins by sorption during the service
D1782 Test Methods for Operating Performance of Particu-
cycle and incomplete removal during normal regeneration.
late Cation-Exchange Materials
D2187 Test Methods and Practices for Evaluating Physical
4. Significance and Use
and Chemical Properties of Particulate Ion-Exchange
4.1 Resinsusedindemineralizationsystemsmaydeteriorate
Resins
due to many factors including chemical attack, fouling by
D2332 Practice for Analysis of Water-Formed Deposits by
organic and inorganic materials, mishandling, or the effects of
Wavelength-Dispersive X-Ray Fluorescence
aging. Detection of degradation or fouling may be important in
determining the cause of poor demineralizer performance.
1
This guide is under the jurisdiction of ASTM Committee D19 on Water and is
5. Sampling
the direct responsibility of Subcommittee D19.08 on Membranes and Ion Exchange
Materials.
5.1 Follow the recommendations of Practices D2687 for
Current edition approved Nov. 1, 2017. Published November 2017. Originally
obtaining samples of particulate ion exchange materials. Core
approved in 1991. Last previous edition approved in 2009 as D5217 – 91 (2009).
DOI: 10.1520/D5217-17. samples are important for obtaining representative samples;
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D5217 − 17
however, special problems may dictate other sampling cence analysis to determine major elements (see Practice
requirements, such as surface, interface, or other samples. D2332). Employ digestion, fusion, and analysis techniques as
would be us
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5217 − 91 (Reapproved 2009) D5217 − 17
Standard Guide for
Detection of Fouling and Degradation of Particulate Ion
1
Exchange Materials
This standard is issued under the fixed designation D5217; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This guide presents a series of tests and evaluations intended to detect fouling and degradation of particulate ion exchange
materials. Suggestions on reducing fouling and on cleaning resins are given.
1.2 This guide is to be used only as an aid in the evaluation of particulate ion exchange material performance and does not
purport to address all possible causes of unsatisfactory performance. The evaluations of mechanical and operational problems are
not addressed.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1129 Terminology Relating to Water
D1782 Test Methods for Operating Performance of Particulate Cation-Exchange Materials
D2187 Test Methods and Practices for Evaluating Physical and Chemical Properties of Particulate Ion-Exchange Resins
D2332 Practice for Analysis of Water-Formed Deposits by Wavelength-Dispersive X-Ray Fluorescence
D2687 Practices for Sampling Particulate Ion-Exchange Materials
D3087 Test Method for Operating Performance of Anion-Exchange Materials for Strong Acid Removal
D3375 Test Method for Column Capacity of Particulate Mixed Bed IonExchange Materials
D3682 Test Method for Major and Minor Elements in Combustion Residues from Coal Utilization Processes
D3683 Test Method for Trace Elements in Coal and Coke Ash by Atomic Absorption
D5042 Test Method for Estimating the Organic Fouling of Particulate Anion Exchange Resins
D6302 Practice for Evaluating the Kinetic Behavior of Ion Exchange Resins
3
E830 Test Method for Ash in the Analysis Sample of Refuse-Derived Fuel (Withdrawn 2011)
3. Terminology
3.1 Definitions—Definitions: For definitions of terms used in this guide, refer to Terminology D1129.
3.1.1 For definitions of terms used in this standard, refer to Terminology D1129.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 air lance, v—to subject to a stream of air under pressure.
3.2.2 organic fouling—fouling, n—the buildup of organic material in or on anion exchange resins by sorption during the service
cycle and incomplete removal during normal regeneration.
1
This guide is under the jurisdiction of ASTM Committee D19 on Water and is the direct responsibility of Subcommittee D19.08 on Membranes and Ion Exchange
Materials.
Current edition approved May 1, 2009Nov. 1, 2017. Published June 2009November 2017. Originally approved in 1991. Last previous edition approved in 20042009 as
D5217 – 91 (2009). (2004). DOI: 10.1520/D5217-91R09.10.1520/D5217-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D5217 − 17
4. Significance and Use
4.1 Resins used in demineralization systems may deteriorate due to many factors including chemical attack, fouling by organic
and inorganic materials, mishandling, or the effects of aging. Detection of degradation or fouling may be important in determining
the cause of poor demineralizer performance.
5. Sampling
5.1 Follow the recommendations of Practices D2687 for obtaining samples of particulate ion exchange materials. Core sam
...
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