ASTM D802-02(2013)

Standard Test Methods for Sampling and Testing Pine Oils

SIGNIFICANCE AND USE
3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical properties of pine oil rather than its chemical composition. Test Methods D6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in pine oils.
SCOPE
1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons.  
1.2 The procedures given in these test methods appear in the following order:    
Section  
Sampling  
4  
Appearance  
5  
Color  
6  
Specific Gravity  
7  
Refractive Index  
8  
Composition  
9  
Moisture  
10  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

• Status: Historical
• Publication Date: 31-May-2013
• ICS: 67.200.10 - Animal and vegetable fats and oils
• ICS: 87.060.20 - Binders
• Technical Committee: D01 - Paint and Related Coatings, Materials, and Applications
• Drafting Committee: D01.34 - Pine Chemicals and Hydrocarbon Resins

Relations

• Replaces: ASTM D802-02(2009) - Standard Test Methods for Sampling and Testing Pine Oils
• Effective Date: 01-Jun-2013
• Referred By: ASTM E1405-98(2022) - Standard Specification for Laboratory Glass Distillation Flasks
• Effective Date: 01-Jun-2013
• Referred By: ASTM D6387-19 - Standard Test Methods for Composition of Turpentine and Related Terpene Products by Capillary Gas Chromatography
• Effective Date: 01-Jun-2013

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D802 − 02 (Reapproved 2013)
Standard Test Methods for
Sampling and Testing Pine Oils
This standard is issued under the fixed designation D802; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D6166 Test Method for Color of Pine Chemicals and Re-
lated Products (Instrumental Determination of Gardner
1.1 These test methods cover procedures for sampling and
Color)
testing pine oils, and are applicable to both natural pine oils
D6387 Test Methods for Composition of Turpentine and
derived from pine stumps either by the steam and solvent
Related Terpene Products by Capillary Gas Chromatogra-
process or by destructive distillation, and also to synthetic pine
phy
oils obtained by the chemical hydration of terpene hydrocar-
E300 Practice for Sampling Industrial Chemicals
bons.
1.2 Theproceduresgiveninthesetestmethodsappearinthe
3. Significance and Use
following order:
3.1 The testing procedures described in these test methods
Section
have been in use for many years and emphasize the physical
Sampling 4
Appearance 5
properties of pine oil rather than its chemical composition.Test
Color 6
Methods D6387 describe a capillary gas chromatography
Specific Gravity 7
method which is suitable for determining both the major and
Refractive Index 8
Composition 9
minor components found in pine oils.
Moisture 10
1.3 The values stated in SI units are to be regarded as
4. Sampling
standard. No other units of measurement are included in this
4.1 Sample the material in accordance with the procedure
standard.
described in Guide D268 and Practice E300.
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Appearance
responsibility of the user of this standard to establish appro-
5.1 Examine a portion of the sample after agitation to
priate safety and health practices and determine the applica-
determine its clarity and freedom from foreign matter and
bility of regulatory limitations prior to use.
separated water.
2. Referenced Documents
6. Color
2.1 ASTM Standards:
D268 Guide for Sampling and Testing Volatile Solvents and
6.1 Compare the color of the sample in any suitable or
Chemical Intermediates for Use in Paint and Related
designated apparatus with the accepted or specific color
Coatings and Material
standard.Accepted color standards are the Gardner color scale
D803 Test Methods for Testing Tall Oil
found in Test Method D6166 and the platinum-cobalt scale
D890 Test Method for Water in Liquid Pine Chemicals
found in Test Method D1209.
D1209 Test Method for Color of Clear Liquids (Platinum-
Cobalt Scale)
7. Specific Gravity
1 7.1 Determine the specific gravity at 15.6/15.6°C by any
These test methods are under the jurisdiction of ASTM Committee D01 on
Paint and Related Coatings, Materials, and Applications and are the direct
convenient method, reporting the value to the nearest 0.0005.
responsibility of Subcommittee D01.34 on Pine Chemicals and Hydrocarbon
(A pycnometer or specific gravity balance is recommended. A
Resins.
hydrometer should not be used, on account of errors caused by
Current edition approved June 1, 2013. Published June 2013. Originally
surface tension on the hydrometer stem.) Correct determina-
approved in 1944. Last previous edition approved in 2009 as D802 – 02 (2009).
DOI: 10.1520/D0802-02R13.
tions made at any other temperature, using apparatus standard-
For reference
...