ASTM D802-02(2009)
(Test Method)Standard Test Methods for Sampling and Testing Pine Oils
Standard Test Methods for Sampling and Testing Pine Oils
SIGNIFICANCE AND USE
The testing procedures described in these test methods have been in use for many years and emphasize the physical properties of pine oil rather than its chemical composition. Test Methods D 6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in pine oils.
SCOPE
1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by the chemical hydration of terpene hydrocarbons.
1.2 The procedures given in these test methods appear in the following order:
Section Sampling4 Appearance5 Color6 Specific Gravity7 Refractive Index8 Composition9 Moisture10
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D802 − 02 (Reapproved2009)
Standard Test Methods for
Sampling and Testing Pine Oils
This standard is issued under the fixed designation D802; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D6166 Test Method for Color of Pine Chemicals and Re-
lated Products (Instrumental Determination of Gardner
1.1 These test methods cover procedures for sampling and
Color)
testing pine oils, and are applicable to both natural pine oils
D6387 Test Methods for Composition of Turpentine and
derived from pine stumps either by the steam and solvent
Related Terpene Products by Capillary Gas Chromatogra-
process or by destructive distillation, and also to synthetic pine
phy
oils obtained by the chemical hydration of terpene hydrocar-
E300 Practice for Sampling Industrial Chemicals
bons.
1.2 Theproceduresgiveninthesetestmethodsappearinthe
3. Significance and Use
following order:
3.1 The testing procedures described in these test methods
Section
have been in use for many years and emphasize the physical
Sampling 4
Appearance 5
properties of pine oil rather than its chemical composition.Test
Color 6
Methods D6387 describe a capillary gas chromatography
Specific Gravity 7
method which is suitable for determining both the major and
Refractive Index 8
Composition 9
minor components found in pine oils.
Moisture 10
1.3 The values stated in SI units are to be regarded as
4. Sampling
standard. No other units of measurement are included in this
4.1 Sample the material in accordance with the procedure
standard.
described in Guide D268 and Practice E300.
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Appearance
responsibility of the user of this standard to establish appro-
5.1 Examine a portion of the sample after agitation to
priate safety and health practices and determine the applica-
determine its clarity and freedom from foreign matter and
bility of regulatory limitations prior to use.
separated water.
2. Referenced Documents
6. Color
2.1 ASTM Standards:
D268 Guide for Sampling and Testing Volatile Solvents and
6.1 Compare the color of the sample in any suitable or
Chemical Intermediates for Use in Paint and Related
designated apparatus with the accepted or specific color
Coatings and Material
standard.Accepted color standards are the Gardner color scale
D803 Test Methods for Testing Tall Oil
found in Test Method D6166 and the platinum-cobalt scale
D890 Test Method for Water in Liquid Pine Chemicals
found in Test Method D1209.
D1209 Test Method for Color of Clear Liquids (Platinum-
Cobalt Scale)
7. Specific Gravity
1 7.1 Determine the specific gravity at 15.6/15.6°C by any
These test methods are under the jurisdiction of ASTM Committee D01 on
Paint and Related Coatings, Materials, and Applications and are the direct
convenient method, reporting the value to the nearest 0.0005.
responsibility of Subcommittee D01.34 on Pine Chemicals and Hydrocarbon
(A pycnometer or specific gravity balance is recommended. A
Resins.
hydrometer should not be used, on account of errors caused by
CurrenteditionapprovedJune1,2009PublishedJune2009.Originallyapproved
surface tension on the hydrometer stem.) Correct determina-
in 1944. Last previous edition approved in 2002 as D802 – 02. DOI: 10.1520/
D0802-02R09.
tions made at any other temperature, using apparatus standard-
For referenced ASTM st
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D802–97 Designation: D 802 – 02 (Reapproved 2009)
Standard Test Methods for
Sampling and Testing Pine Oils
This standard is issued under the fixed designation D 802; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 These test methods cover procedures for sampling and testing pine oils, and are applicable to both natural pine oils derived
from pine stumps either by the steam and solvent process or by destructive distillation, and also to synthetic pine oils obtained by
the chemical hydration of terpene hydrocarbons.
1.2 The procedures given in these test methods appear in the following order:
Section
Sampling 4
Appearance 5
Color 6
Specific Gravity 7
Refractive Index 8
Composition 9
Moisture10 10
Moisture 10
1.3
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 268 Guide for Sampling andTestingVolatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and
MaterialsMaterial
D 803 Test Methods for Testing Tall Oil
D 890 Test Method for Water in Liquid Naval Stores
D3009Test Method for Compositon of Turpentine by Gas Chromatography
E300Practice for Sampling Industrial Chemicals 1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D 6166 Test Method for Color of Naval Stores and Related Products (Instrumental Determination of Gardner Color)
D 6387 Test Methods for Composition of Turpentine and Related Terpene Products by Capillary Gas Chromatography
E 300 Practice for Sampling Industrial Chemicals
3. Significance and Use
3.1Thetestingproceduresdescribedinthesetestmethodshavebeeninuseformanyyearsandemphasizethephysicalproperties
of pine oil rather than its chemical composition. Gas chromatography is the accepted method for determining the chemical
composition of pine oil. An ASTM test method based on capillary gas chromatography can be used for the major components of
pine oil. A capillary GC procedure is currently being written which is suitable for both major and minor components.
3.1 The testing procedures described in these test methods have been in use for many years and emphasize the physical
properties of pine oil rather than its chemical composition. Test Methods D 6387 describe a capillary gas chromatography method
which is suitable for determining both the major and minor components found in pine oils.
These test methods are under the jurisdiction ofASTM Committee D-1D01 on Paint and Related Coatings, Materials, andApplications and are the direct responsibility
of Subcommittee D01.34 on Naval Stores.
Current edition approved Nov. 10, 1997. Published June 1998. Originally published as D802–44T. Last previous edition D802–82 (1987).
Current edition approved June 1, 2009 Published June 2009. Originally approved in 1944. Last previous edition approved in 2002 as D 802 – 02.
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book ofASTM Standards
, Vol 06.04.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 802 – 02 (2009)
4. Sampling
4.1 Sample the material in accordance with the procedure described in Guide D 268 and Practice E 300.
5. Appearance
5.1 Examineaportionofthesampleafteragitat
...
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