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ASTM E3084-17

(Practice)

Standard Practice for Characterizing Particle Irradiations of Materials in Terms of Non-Ionizing Energy Loss (NIEL)

Standard Practice for Characterizing Particle Irradiations of Materials in Terms of Non-Ionizing Energy Loss (NIEL)

SIGNIFICANCE AND USE
4.1 A radiation-hardness assurance program requires a methodology for relating radiation induced changes in materials exposed to a variety of particle species over a wide range of energies, including those encountered in spacecraft and in terrestrial environments as well as those produced by particle accelerators and nuclear fission and fusion reactors.  
4.2 A major source of radiation damage in electronic and photonic devices and materials is the displacement of atoms from their normal lattice site. An appropriate exposure parameter for such damage is the damage energy calculated from NIEL by means of Eq 2. Other analogous measures, which may be used to characterize the irradiation history that is relevant to displacement damage, are damage energy per atom or per unit mass (displacement kerma, when the primary particles are neutral), and displacements per atom (dpa). See Terminology E170 for definitions of those quantities.  
4.3 Each of the quantities mentioned in the previous paragraph should convey similar information, but in a different format. In each case the value of the derived exposure parameter depends on approximate nuclear, atomic, and lattice models, an on measured or calculated cross sections. If consistent comparisons are to be made of irradiation effects caused by different particle species and energies, it is essential that these approximations be consistently applied.  
4.4 No correspondence should be assumed to exist between damage energy as calculated from NIEL and a particular change in a material property or device parameter. Instead, the damage energy should be used as a parameter which describes the exposure. It may be a useful correlation variate, even when different particle species and energies are included. NIEL should not be reported as a measure of damage, however, unless its correlation with a particular damage modality has been demonstrated in that material or device.  
4.5 NIEL is a construct that depends on a model of the part...
SCOPE
1.1 This practice describes a procedure for characterizing particle irradiations of materials in terms of non-ionizing energy loss (NIEL). NIEL is used in published literature to characterize both charged and neutral particle irradiations.  
1.2 Although the methods described in this practice apply to any particles and target materials for which displacement cross sections are known (see Practice E521), this practice is intended for use in irradiations in which observed damage effects may be correlated with atomic displacements. This is true of some, but not all, radiation effects in electronic and photonic materials.  
1.3 Procedures analogous to this one are used for calculation of displacements per atom (dpa) in charged particle irradiations (see Practice E521) or neutron irradiations (see Practice E693).  
1.4 Guidance on calculation of dpa from NIEL is provided.  
1.5 Procedures related to this one are used for calculation of 1-MeV equivalent neutron fluence in electronic materials (see Practice E722), but in that practice the concept of damage efficiency, based on correlation of observed damage effects, is included.  
1.6 Guidance on conversion of NIEL in silicon to monoenergetic neutron fluence in silicon (see Practice E722), and vice versa, is provided.  
1.7 The application of this standard requires knowledge of the particle fluence and energy distribution of particles whose interaction leads to displacement damage.  
1.8 The correlation of radiation effects data is beyond the scope of this standard. A comprehensive review (1)2 of displacement damage effects in silicon and their correlation with NIEL provides appropriate guidance that is applicable to semiconductor materials and electronic devices.

General Information

Status
Historical
Publication Date
31-Jan-2017
ICS
19.100 - Non-destructive testing
Technical Committee
E10 - Nuclear Technology and Applications
Drafting Committee
E10.07 - Radiation Dosimetry for Radiation Effects on Materials and Devices
Current Stage
Ref Project

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ASTM E3084-17 - Standard Practice for Characterizing Particle Irradiations of Materials in Terms of Non-Ionizing Energy Loss (NIEL)ASTM E3084-17 - Standard Practice for Characterizing Particle Irradiations of Materials in Terms of Non-Ionizing Energy Loss (NIEL)
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ASTM E3084-17 - Standard Practice for Characterizing Particle Irradiations of Materials in Terms of Non-Ionizing Energy Loss (NIEL)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E3084 − 17
Standard Practice for
Characterizing Particle Irradiations of Materials in Terms of
1
Non-Ionizing Energy Loss (NIEL)
This standard is issued under the fixed designation E3084; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.9 This international standard was developed in accor-
dance with internationally recognized principles on standard-
1.1 This practice describes a procedure for characterizing
ization established in the Decision on Principles for the
particle irradiations of materials in terms of non-ionizing
Development of International Standards, Guides and Recom-
energy loss (NIEL). NIEL is used in published literature to
mendations issued by the World Trade Organization Technical
characterize both charged and neutral particle irradiations.
Barriers to Trade (TBT) Committee.
1.2 Althoughthemethodsdescribedinthispracticeapplyto
any particles and target materials for which displacement cross
2. Referenced Documents
sections are known (see Practice E521), this practice is
3
2.1 ASTM Standards
intended for use in irradiations in which observed damage
E170 Terminology Relating to Radiation Measurements and
effects may be correlated with atomic displacements. This is
Dosimetry
true of some, but not all, radiation effects in electronic and
E521 Practice for Investigating the Effects of Neutron Ra-
photonic materials.
diation Damage Using Charged-Particle Irradiation
1.3 Procedures analogous to this one are used for calcula-
E693 Practice for Characterizing Neutron Exposures in Iron
tion of displacements per atom (dpa) in charged particle
and Low Alloy Steels in Terms of Displacements Per
irradiations (see Practice E521) or neutron irradiations (see
Atom (DPA)
Practice E693).
E722 PracticeforCharacterizingNeutronFluenceSpectrain
Terms of an Equivalent Monoenergetic Neutron Fluence
1.4 Guidance on calculation of dpa from NIEL is provided.
for Radiation-Hardness Testing of Electronics
1.5 Procedures related to this one are used for calculation of
1-MeV equivalent neutron fluence in electronic materials (see
3. Terminology
Practice E722), but in that practice the concept of damage
3.1 Definitions of some terms used in this practice can be
efficiency, based on correlation of observed damage effects, is
found in Terminology E170.
included.
3.2 Definitions:
1.6 Guidance on conversion of NIEL in silicon to monoen-
3.2.1 tracked particles—those particles whose position-
ergetic neutron fluence in silicon (see Practice E722), and vice
dependent fluence spectra are calculated in a particle transport
versa, is provided.
calculation for a specific target geometry.
1.7 The application of this standard requires knowledge of
3.2.1.1 Discussion—In calculating displacement damage
the particle fluence and energy distribution of particles whose
energy and NIEL, the tracked particles should include
interaction leads to displacement damage.
neutrons, photons, protons and ions up to Z=2, unless their
contributions are known to be negligible. Heavier ions may
1.8 The correlation of radiation effects data is beyond the
2
also be tracked in some Monte Carlo codes. Except in the case
scope of this standard. A comprehensive review (1) of
of neutrons, particles below a specified minimum energy are
displacement damage effects in silicon and their correlation
not tracked, and are treated as non-tracked particles.
with NIEL provides appropriate guidance that is applicable to
semiconductor materials and electronic devices.
3.2.2 tracked-particle fluence spectrum, Φ (E)—the fluence
p
spectrumofparticles,ofspeciespandatparticleenergy E,that
are tracked in a particle transport calculation. For each species
1
This practice is under the jurisdiction of ASTM Committee E10 on Nuclear
Technology and Applications and is the direct responsibility of Subcommittee
E10.07 on Radiation Dosimetry for Radiation Effects on Materials and Devices.
3
Current edition approved Feb. 1, 2017. Published March 2017. DOI: 10.1520/ For referenced ASTM standards, visit the ASTM website, www.astm.org, or
D3084-17. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
The boldface numbers in parentheses refer to a list of references at the end of Standards volume information, refer to the standard’s Document Summary page on
this standard. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E3084 − 17
-2
of tracked particle other than neutrons there is a specified (cm ) in sili
...

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ABSTRACT
This practice covers the measurement of the mechanical properties of materials during charged-particle irradiation, with the test materials designed to simulate or provide understanding of, or both, the mechanical behavior of materials when exposed to neutron irradiation. This practice includes requirements for test material and particle beam characterization (such as for strain, load, temperature monitoring and control, and specimen environment monitoring), and recommended procedures for measuring mechanical properties and for calculating radiation damage (such as particle ranges, damage energy, damage rates, and damage gradients). Methods for comparing ion damage with neutron damage are also recommended.
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1.2 The word simulation is used here in a broad sense to imply an approximation of the relevant neutron irradiation environment. The degree of conformity can range from poor to nearly exact. The intent is to produce a correspondence between one or more aspects of the neutron and charged-particle irradiations such that fundamental relationships are established between irradiation or material parameters and the material response.  
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Standard Practice for Characterizing Particle Irradiations of Materials in Terms of Non-Ionizing Energy Loss (NIEL)

SIGNIFICANCE AND USE
4.1 A radiation-hardness assurance program requires a methodology for relating radiation-induced changes in materials exposed to a variety of particle species over a wide range of energies, including those encountered in spacecraft and in terrestrial environments as well as those produced by particle accelerators and nuclear fission and fusion reactors.  
4.2 A major source of radiation damage in electronic and photonic devices and materials is the displacement of atoms from their normal lattice site. An appropriate exposure parameter for such damage is the damage energy calculated from NIEL by means of Eq 2. Other analogous measures, which may be used to characterize the irradiation history that is relevant to displacement damage, are damage energy per atom or per unit mass (displacement kerma, when the primary particles are neutral), and displacements per atom (dpa). See Terminology E170 for definitions of those quantities.  
4.3 Each of the quantities mentioned in the previous paragraph should convey similar information, but in a different format. In each case the value of the derived exposure parameter depends on approximate nuclear, atomic, and lattice models, and on measured or calculated cross sections. If consistent comparisons are to be made of irradiation effects caused by different particle species and energies, it is essential that these approximations be consistently applied.  
4.4 No correspondence should be assumed to exist between damage energy as calculated from NIEL and a particular change in a material property or device parameter. Instead, the damage energy should be used as a parameter which describes the exposure. It may be a useful correlation variate, even when different particle species and energies are included. NIEL should not be reported as a measure of damage, however, unless its correlation with a particular damage modality has been demonstrated in that material or device.  
4.5 NIEL is a construct that depends on a model of the par...
SCOPE
1.1 This practice describes a procedure for characterizing particle irradiations of materials in terms of non-ionizing energy loss (NIEL). NIEL is used in published literature to characterize both charged and neutral particle irradiations.  
1.2 Although the methods described in this practice apply to any particles and target materials for which displacement cross sections are known (see Practice E521), this practice is intended for use in irradiations in which observed damage effects may be correlated with atomic displacements. This is true of some, but not all, radiation effects in electronic and photonic materials.  
1.3 Procedures analogous to this one are used for calculation of displacements per atom (dpa) in charged particle irradiations (see Practice E521) or neutron irradiations (see Practice E693).  
1.4 Guidance on calculation of dpa from NIEL is provided.  
1.5 Procedures related to this one are used for calculation of 1-MeV equivalent neutron fluence in electronic materials (see Practice E722), but in that practice the concept of damage efficiency, based on correlation of observed damage effects, is included.  
1.6 Guidance on conversion of NIEL in silicon to monoenergetic neutron fluence in silicon (see Practice E722), and vice versa, is provided.  
1.7 The application of this standard requires knowledge of the particle fluence and energy distribution of particles whose interaction leads to displacement damage.  
1.8 The correlation of radiation effects data is beyond the scope of this standard. A comprehensive review (1)2 of displacement damage effects in silicon and their correlation with NIEL provides appropriate guidance that is applicable to semiconductor materials and electronic devices.  
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ASTM D6855-17(2023)(Test Method)
Standard Test Method for Determination of Turbidity Below 5 NTU in Static Mode

SIGNIFICANCE AND USE
5.1 Turbidity is undesirable in drinking water, plant effluent waters, water for food and beverage processing, and for a large number of other water-dependent manufacturing processes. Removal is often accomplished by coagulation, settling, and filtration. Measurement of turbidity provides a rapid means of process control for when, how, and to what extent the water must be treated to meet specifications.  
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5.3.1 Table 1 describes technologies and reporting results (see also Refs (1-3)).6 Those technologies listed are appropriate for the range of measurement prescribed in this test method. Others may come available in the future. Fig. X5.1 provides a flow chart to aid in selection of the appropriate technology for low-level static turbidity applications.  
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1.1 This test method covers the static determination of turbidity in water (see 4.1).  
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Standard Practice for Instrumented Indentation Testing

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5.1 IIT Instruments are used to quantitatively measure various mechanical properties of thin coatings and other volumes of material when other traditional methods of determining material properties cannot be used due to the size or condition of the sample. This practice will establish the basic requirements for those instruments. It is intended that IIT based test methods will be able to refer to this practice for the basic requirements for force and displacement accuracy, reproducibility, verification, reporting, etc., that are necessary for obtaining meaningful test results.  
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3.1 The terms found in this standard are intended to be used uniformly and consistently in all nondestructive testing standards. The purpose of this standard is to promote a clear understanding and interpretation of the NDT standards in which they are used.
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1.1 This standard covers the terminology used in the standards prepared by the E07 Committee on Nondestructive Testing. These nondestructive testing (NDT) methods include: acoustic emission, electromagnetic testing, gamma- and X-radiology, leak testing, liquid penetrant testing, magnetic particle testing, neutron radiology and gauging, ultrasonic testing, and other technical methods.  
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(a) Nondestructive testing methods are used extensively for the examination or inspection of materials and components.
(b) The E07 Committee on Nondestructive Testing has prepared many documents to promote uniform usage of the nondestructive testing methods that are applied to examine or inspect materials and components.  
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SIGNIFICANCE AND USE
5.1 The POD analysis method described herein is based on a well-known and well established statistical regression method. It shall be used to quantify the demonstrated POD for a specific set of examination parameters and known range of discontinuity sizes under the following conditions.  
5.1.1 The initial response from a nondestructive evaluation inspection system is ultimately binary in nature (that is, hit or miss).  
5.1.2 Discontinuity size is the predictor variable and can be accurately quantified.  
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SCOPE
1.1 This practice covers the procedure for performing a statistical analysis on nondestructive testing hit/miss data to determine the demonstrated probability of detection (POD) for a specific set of examination parameters. Topics covered include the standard hit/miss POD curve formulation, validation techniques, and correct interpretation of results.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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Standard Practice for Liquid Penetrant Testing for General Industry

SIGNIFICANCE AND USE
5.1 Liquid penetrant testing methods indicate the presence, location, and to a limited extent, the nature and magnitude of the detected discontinuities. Each of the various penetrant methods has been designed for specific uses such as critical service items, volume of parts, portability, or localized areas of examination. The method selected will depend accordingly on the design and service requirements of the parts or materials being tested.
SCOPE
1.1 This practice2 covers procedures for penetrant examination of materials. Penetrant testing is a nondestructive testing method for detecting discontinuities that are open to the surface such as cracks, seams, laps, cold shuts, shrinkage, laminations, through leaks, or lack of fusion and is applicable to in-process, final, and maintenance examinations. It can be effectively used in the examination of nonporous, metallic materials, ferrous and nonferrous metals, and of nonmetallic materials such as nonporous glazed or fully densified ceramics, as well as certain nonporous plastics, and glass.  
1.2 This practice also provides a reference:  
1.2.1 By which a liquid penetrant examination process recommended or required by individual organizations can be reviewed to ascertain its applicability and completeness.  
1.2.2 For use in the preparation of process specifications and procedures dealing with the liquid penetrant testing of parts and materials. Agreement by the customer requesting penetrant testing is strongly recommended. All areas of this practice may be open to agreement between the cognizant engineering organization and the supplier, or specific direction from the cognizant engineering organization.  
1.2.3 For use in the organization of facilities and personnel concerned with liquid penetrant testing.  
1.3 This practice does not indicate or suggest criteria for evaluation of the indications obtained by penetrant testing. It should be pointed out, however, that after indications have been found, they must be interpreted or classified and then evaluated. For this purpose there must be a separate code, standard, or a specific agreement to define the type, size, location, and direction of indications considered acceptable, and those considered unacceptable.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
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6.1 This guide provides procedures for the application of contact straight-beam examination for the detection and quantitative evaluation of discontinuities in materials.  
6.2 Although not all requirements of this guide can be applied universally to all examinations, situations, and materials, it does provide basis for establishing contractual criteria between the users, and may be used as a general guide for preparing detailed specifications for a particular application.  
6.3 This guide is directed towards the evaluation of discontinuities detectable with the beam normal to the entry surface. If discontinuities or other orientations are of concern, alternate scanning techniques are required.
SCOPE
1.1 This guide covers procedures for the contact ultrasonic examination of bulk materials or parts by transmitting pulsed ultrasonic waves into the material and observing the indications of reflected waves. This guide covers only examinations in which one search unit is used as both transmitter and receiver (pulse-echo). This guide includes general requirements and procedures that may be used for detecting discontinuities, locating depth and distance from a point of reference and for making a relative or approximate evaluation of the size of discontinuities as compared to a reference standard.  
1.2 This guide complements Practice E114 by providing more detailed procedures for the selection and standardization of the examination system and for evaluation of the indications obtained.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This guide does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this guide to establish the appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E3370-23(Practice)
Standard Practice for Matrix Array Ultrasonic Testing of Composites, Sandwich Core Constructions, and Metals

SIGNIFICANCE AND USE
5.1 The procedures described in this practice have proven utility in the inspecting (1) monolithic polymer matrix composites (laminates) for bulk defects, (2) metals for corrosion during the service life of the part of interest, (3) thickness checks, (4) adhesive bonding of metals, composites, and sandwich core constructions, (5) coatings, and (6) composite filament windings. Both unpressurized, and with suitable precautions, pressurized materials and components are inspected.  
5.2 This practice provides guidelines for the application of longitudinal wave examination to the detection and quantitative evaluation of damage, discontinuities, and thickness variations in materials.  
5.3 This practice is intended primarily for the testing of parts to acceptance criteria most typically specified in a purchase order or other contractual document, and for testing of parts in-service to detect and evaluate damage.  
5.4 MAUT search units provide near-surface resolution and detection of small discontinuities comparable to phased array transducers. They may or may not be capable of beam steering. The advantage of MAUT for straight-beam longitudinal wave inspections is the ability to provide real-time C-scan data, which facilitates data interpretation and shortens inspection time. Depending on inspection needs, data can be displayed as A-, B- or C-scans, or three-dimensional renderings. Toggling between pulse-echo and through transmission ultrasonic (TTU) modes without having to use another system or changing transducers is also possible.  
5.5 The MAUT technique has proven utility in the inspection of multi-ply carbon-fiber reinforced laminates used in primary aircraft structures.11  
5.6 For ultrasonic testing of laminate composites and sandwich core materials using conventional UT equipment consult Practice E2580. Consult Practice E114 for ultrasonic testing of materials by the pulse-echo method using straightbeam longitudinal waves introduced by a piezoelectric elemen...
SCOPE
1.1 This practice covers procedures for matrix array ultrasonic testing (MAUT) of monolithic composites, composite sandwich constructions, and metallic test articles. These procedures can be used throughout the life cycle of a part during product and process design optimization, on line process control, post-manufacturing inspection, and in-service inspection.  
1.2 In general, ultrasonic testing is a common volumetric method for detection of embedded or subsurface discontinuities. This practice includes general requirements and procedures which may be used for detecting flaws and for making a relative or approximate evaluation of the size of discontinuities and part anomalies. The types of flaws or discontinuities detected include interply delaminations, foreign object debris (FOD), inclusions, disbond/un-bond, fiber debonding, fiber fracture, porosity, voids, impact damage, thickness variation, and corrosion.  
1.3 Typical test articles include monolithic composite layups such as uniaxial, cross ply and angle ply laminates, sandwich constructions, bonded structures, and filament windings, as well as forged, wrought and cast metallic parts. Two techniques can be considered based on accessibility of the inspection surface: namely, pulse echo inspection for one-sided access and through-transmission for two-sided access. As used in this practice, both require the use of a pulsed straight-beam ultrasonic longitudinal wave followed by observing indications of either the reflected (pulse-echo) or received (through transmission) wave.  
1.4 This practice provides two ultrasonic test procedures. Each has its own merits and requirements for inspection and shall be selected as agreed upon in a contractual document.  
1.4.1 Test Procedure A, Pulse Echo (non-contacting and contacting) is at a minimum a single matrix array transducer transmitting and receiving longitudinal waves in the range of 0.5 MHz to 20 MHz (see Fig. 1). Th...

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ASTM
ASTM E2663-23(Practice)
Standard Practice for Digital Imaging and Communication in Nondestructive Evaluation (DICONDE) for Ultrasonic Test Methods

SIGNIFICANCE AND USE
5.1 Personnel that are responsible for the creation, transfer, and storage of ultrasonic test results will use this standard. This practice defines a set of information modules that, along with Practice E2339 and the DICOM standard, provides a standard means to organize ultrasonic test parameters and results. The ultrasonic test results may be displayed and analyzed on any device that conforms to this standard. Personnel wishing to view any ultrasonic inspection data stored in DICONDE format may use this document to help them decode and display the data contained in the DICONDE compliant inspection record.
SCOPE
1.1 This practice covers the interoperability of ultrasonic imaging equipment by specifying image data transfer and archival storage methods in commonly accepted terms. This document is intended to be used in conjunction with Practice E2339. Practice E2339 defines an industrial adaptation of NEMA PS3 / ISO 12052 (DICOM, see http://medical.nema.org), an international standard for image data acquisition, review, transfer, and archival storage. The goal of Practice E2339, commonly referred to as DICONDE, is to provide a standard that facilitates the display and analysis of NDE test results on any system conforming to the DICONDE standard. Toward that end, Practice E2339 provides a data dictionary and set of information modules that are applicable to all NDE modalities. This practice supplements Practice E2339 by providing information object definitions, information modules, and data dictionary that are specific to ultrasonic test methods.  
1.2 This practice has been developed to overcome the issues that arise when analyzing or archiving data from ultrasonic test equipment using proprietary data transfer and storage methods. As digital technologies evolve, data must remain decipherable through the use of open, industry-wide methods for data transfer and archival storage. This practice defines a method where all the ultrasonic technique parameters and test results are communicated and stored in a standard format regardless of changes in digital technology.  
1.3 This practice does not specify:  
1.3.1 A testing or validation procedure to assess an implementation's conformance to the standard.  
1.3.2 The implementation details of any features of the standard on a device claiming conformance.  
1.3.3 The overall set of features and functions to be expected from a system implemented by integrating a group of devices each claiming DICONDE conformance.  
1.4 Although this practice contains no values that require units, it does describe methods to store and communicate data that do require units to be properly interpreted. The SI units required by this practice are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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