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ASTM D5606-09

(Specification)

Standard Specification for Toluene for Toluene Diisocyanate (TDI) Feedstock

Standard Specification for Toluene for Toluene Diisocyanate (TDI) Feedstock

ABSTRACT
This specification covers toluene for toluene diisocyanate (TDI) feedstock. The purity, acid wash color, benzene, nanoromatics, ethylbenzene, xylenes, and appearance of toluene shall be tested to meet the requirements prescribed.
SCOPE
1.1 This specification covers toluene for toluene diisocyanate (TDI) feedstock.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 Consult OSHA regulations and suppliers' material safety data sheets for all materials used in this specification.
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

General Information

Status
Historical
Publication Date
30-Nov-2009
ICS
71.080.15 - Aromatic hydrocarbons
Technical Committee
D16 - Aromatic, Industrial, Specialty and Related Chemicals
Drafting Committee
D16.01 - Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives
Current Stage
Ref Project

Relations

Replaces
ASTM D5606-01(2006)e1 - Standard Specification for Toluene for Toluene Diisocyanate (TDI) Feedstock
Effective Date
01-Dec-2009
Replaced By
ASTM D5606-09(2013) - Standard Specification for Toluene for Toluene Diisocyanate (TDI) Feedstock
Effective Date
01-Jul-2013

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5606 −09
StandardSpecification for
1
Toluene for Toluene Diisocyanate (TDI) Feedstock
This standard is issued under the fixed designation D5606; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D6526 Test Method for Analysis of Toluene by Capillary
Column Gas Chromatography
1.1 This specification covers toluene for toluene diisocya-
D7504 Test Method for Trace Impurities in Monocyclic
nate (TDI) feedstock.
Aromatic Hydrocarbons by Gas Chromatography and
1.2 The following applies to all specified limits in this
Effective Carbon Number
specification: for purposes of determining conformance with
E29 Practice for Using Significant Digits in Test Data to
this specification, an observed value or a calculated value shall
Determine Conformance with Specifications
be rounded off to the nearest unit in the last right-hand digit
2.2 Other Document:
used in expressing the specification limit, in accordance with
OSHA Regulations, 29 CFR paragraphs 1910.1000 and
3
the rounding-off method of Practice E29.
1910.1200
1.3 Consult OSHA regulations and suppliers’ material
3. Properties
safety data sheets for all materials used in this specification.
3.1 Toluene for TDI feedstock shall conform to the follow-
1.4 The values stated in SI units are to be regarded as
ing requirements:
standard. The values given in parentheses are for information
Property Specification ASTM Test Method
only.
A
Purity, min, wt % 99.9 D2360 or D6526 or
D7504
2. Referenced Documents
Acid wash color, max pass with 2 D848
A
Benzene, max, mg/kg 300 D2360 or D6526 or
2
2.1 ASTM Standards:
D7504
A
D848 Test Method for Acid Wash Color of Industrial Aro- Nonaromatics, max, wt % 0.1 D2360 or D6526 or
D7504
matic Hydrocarbons
A
Ethylbenzene, max, mg/kg 300 D2360 or D6526 or
D1209 Test Method for Color of Clear Liquids (Platinum-
D7504
A
Xylenes, max, mg/kg 500 D2360 or D6526 or
Cobalt Scale)
D7504
D2360 Test Method for Trace Impurities in Monocyclic
B
Appearance .
Aromatic Hydrocarbons by Gas Chromatography
Color, max, Pt–Co scale 10 D1209 or D5386
_________________________
D3437 Practice for Sampling and Handling Liquid Cyclic
A
Products If more than one method is listed, the producer and user should agree on the
referee method.
D5386 Test Method for Color of Liquids Using Tristimulus
B
Clear liquid free of sediment and haze when observed at 18.3 to 25.6°C (65 to
Colorimetry
78°F).
4. Sampling
1
This specification is under the jurisdiction of ASTM Committee D16 on
4.1 Sample the material in accordance with Pra
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
´1
Designation:D5606–01(Reapproved2006) Designation: D5606 – 09
Standard Specification for
1
Toluene for Toluene Diisocyanate (TDI) Feedstock
This standard is issued under the fixed designation D5606; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
´ NOTE—Editorial changes were made to Footnote A of table in 3.1 and a Summary of Changes was added in January 2006.
1. Scope*
1.1 This specification covers toluene for toluene diisocyanate (TDI) feedstock.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this
specification, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in
expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 Consult OSHA regulations and suppliers’ material safety data sheets for all materials used in this specification.
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
2. Referenced Documents
2
2.1 ASTM Standards:
D848 Test Method for Acid Wash Color of Industrial Aromatic Hydrocarbons
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D2360 Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
D6526 Test Method for Analysis of Toluene by Capillary Column Gas Chromatography
D7504 Test Method forTrace Impurities in MonocyclicAromatic Hydrocarbons by Gas Chromatography and Effective Carbon
Number
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
2.2 Other Document:
3
OSHA Regulations, 29 CFRCFR, paragraphs paragraphs 1910.1000 and 1910.1200
3. Properties
3.1 Toluene for TDI feedstock shall conform to the following requirements:
Property Specification ASTM Test Method
A
Purity, min, wt % 99.9 D2360 or D6526
A
Purity, min, wt % 99.9 D2360 or D6526 or
D7504
Acid wash color, max pass with 2 D848
A
Benzene, max, mg/kg 300 D2360 or D6526
A
Benzene, max, mg/kg 300 D2360 or D6526 or
D7504
A
Nonaromatics, max, wt % 0.1 D2360 or D6526
A
Nonaromatics, max, wt % 0.1 D2360 or D6526 or
D7504
A
Ethylbenzene, max, mg/kg 300 D2360 or D6526
1
This specification is under the jurisdiction ofASTM Committee D16 onAromatic Hydrocarbons and Related Chemicals and is the direct responsibility of Subcommittee
D16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives.
Current edition approved Jan. 1, 2006. Published January 2006. Originally approved in 1994. Last previous edition approved in 200
...

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