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ASTM D5200-03

(Test Method)

Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol Cans

Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol Cans

SIGNIFICANCE AND USE
This test method is the procedure of choice for determining the volatile content in aerosol coatings under specified test conditions modeled after Method 354 . The inverse value, nonvolatile, is used to determine the weight percent solids content. This information is useful to the paint producer, user, and to environmental interests for determining the grams of volatile organic compounds per gram of solids emitted from aerosol cans.
FIG. 1 Adapter Glass Tube Assembly
SCOPE
1.1 This test method is for the determination of the weight percent volatile organic compounds of solvent-borne paints in aerosol cans. It offers a unique way to obtain paint specimens from aerosol cans.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. A specific hazard statement is given in Note 1.

General Information

Status
Historical
Publication Date
09-Jan-2003
ICS
87.040 - Paints and varnishes
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.21 - Chemical Analysis of Paints and Paint Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D5200-92(1997)e1 - Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol Cans
Effective Date
10-Jan-2003
Replaced By
ASTM D5200-03(2008)e1 - Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol Cans
Effective Date
01-Nov-2008

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ASTM D5200-03 - Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol CansASTM D5200-03 - Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol Cans
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ASTM D5200-03 - Standard Test Method for Determination of Weight Percent Volatile Content of Solvent-Borne Paints in Aerosol Cans
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5200–03
Standard Test Method for
Determination of Weight Percent Volatile Content of Solvent-
1
Borne Paints in Aerosol Cans
This standard is issued under the fixed designation D 5200; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method is for the determination of the weight
percent volatile organic compounds of solvent-borne paints in
aerosol cans. It offers a unique way to obtain paint specimens
from aerosol cans.
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. A specific hazard
statement is given in Note 1.
2. Referenced Documents
2.1 ASTM Standards:
E 145 Specification for Gravity-Convection and Forced-
2
Ventilation Ovens
E 180 Practice for Determining the Precision of ASTM
Methods for Analysis and Testing of Industrial and Spe-
3
cialty Chemicals
2.2 Other Standard:
Method 35 Determination of PercentVolatile Organic Com-
4
pounds (VOC) in Solvent Based Aerosol Paints
3. Summary of Test Method
3.1 Adesignatedquantityfromanaerosolcoatingissprayed
into an adapter glass tube assembly and heated in an oven at
FIG. 1 Adapter Glass Tube Assembly
110 6 5°C for 60 min. The percent volatile is calculated from
the loss in weight.
content. This information is useful to the paint producer, user,
4. Significance and Use
and to environmental interests for determining the grams of
4.1 This test method is the procedure of choice for deter-
volatile organic compounds per gram of solids emitted from
mining the volatile content in aerosol coatings under specified
aerosol cans.
4
test conditions modeled after Method 35 . The inverse value,
nonvolatile, is used to determine the weight percent solids 5. Apparatus
5.1 Adapter Glass Tube Assembly, (Fig. 1).
5.1.1 Sample Adapter Tube, straight connecting with 35/25
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint spherical joints. Loosely fill with glass wool and precondition
and Related Coatings, Materials, andApplications and is the direct responsibility of
for 30 min in an oven at 110 6 5°C and store in a dessicator
Subcommittee D01.21 on Chemical Analysis of Paints and Paint Materials.
5,6
prior to use.
Current edition approved Jan. 10, 2003. Published March 2003. Originally
e1.
approved in 1991. Last previous edition approved in 1997 as D 5200 – 92 (1997) .
2
Annual Book of ASTM Standards, Vol 14.04.
3 5
Annual Book of ASTM Standards, Vol 15.05. The sole source of supply of the adapter tube, No. 5035-35 known to the
4
Bay Area Air Quality Management District, (BAAQMD) Manual of Proce- committee at this time is Ace Glass Inc., P.O. Box 688, 1430 Northwest Blvd.,
dures, Vol III, 939 Ellis St., San Francisco, CA 94109. Vineland, NJ 08360.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D5200–03
spreading out the coating by moving the extension tube around
the wall of the adapter tube. The spraying is done with the
vacuum on.
6.6 Obtain the specimen weight by difference by weighing
the aerosol can again to 0.01 g after spraying out the specimen.
6.7 Place the sample adapter tube in the drying oven for 60
min at 110 6 5°C.
NOTE 1—Warning: Provide adequate ventilation, consistent with ac-
ceptedlaboratorypractice,topreventsolventvaporsfromaccumulatingto
a dangerous level.
FIG. 2 Aerosol Can on Eberbach Shaker
6.8 Remove the adapter tubes from the oven, place imme-
diately in a dessicator, cool to ambient temperature, and weigh
5.1.2 Charcoal Adapter Tube, straight connecting with
to 0.01 g.
35/25 spherical joints. Fill with activated charcoal and plug
both ends with glass wool. This tube is used to prevent the
7. Calculations
6,7
solvent vapors from contaminating the vacuum pump.
,
6 8
7.1 Calculate the weight percent nonvolatile content (NV),
5.1.3 Adapters, connecting hose with 35/25 socket joints.
6,9
in the aerosol can as follows:
5.1.4 Adapter, connecting hose with 35/25 ball joint.
,
6 10
5.1.5 Clamps, pinch type, with screw-locking device. NV,% 5 W /W 3 100 (1)
~ !
2 1
5.1.6 Glass Wool, medium-fine silk.
where:
5.1.7 Activated Charcoal, coconut, 8 to 12 mesh.
W = weight of aerosol can before spraying sample minus
1
5.1.8 Tygon Tubing.
weight of aerosol can after spraying sample, g, and
5.1.9 Iron Stands.
W = weight of sample adapter tube w
...

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