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ASTM D6050-97(2003)

(Test Method)

Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous Waste

Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous Waste

SCOPE
1.1 This test method covers the determination of the approximate amount of insoluble, suspended solid material in organic liquid hazardous waste (OLHW).  
1.2 This test method is intended to be used in approximating the amount of insoluble, suspended solids in determining the material handling characteristics and fuel quality of OLHW. It is not intended to replace more sophisticated procedures for the determination of total solids.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Mar-2003
Technical Committee
D34 - Waste Management
Drafting Committee
D34.01.06 - Analytical Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D6050-97 - Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous Waste
Effective Date
10-Mar-2003
Replaced By
ASTM D6050-97(2003)e1 - Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous Waste
Effective Date
10-Mar-2003

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ASTM D6050-97(2003) - Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous WasteASTM D6050-97(2003) - Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous Waste
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ASTM D6050-97(2003) - Standard Test Method for Determination of Insoluble Solids in Organic Liquid Hazardous Waste
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn. Contact ASTM
International (www.astm.org) for the latest information.
Designation:D6050–97 (Reapproved 2003)
Standard Test Method for
Determination of Insoluble Solids in Organic Liquid
1
Hazardous Waste
This standard is issued under the fixed designation D 6050; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Significance and Use
1.1 This test method covers the determination of the ap- 4.1 Facilities utilizing bulk liquid hazardous waste fuels are
proximate amount of insoluble, suspended solid material in concerned about material handling characteristics and the
organic liquid hazardous waste (OLHW). overall quality of the fuel. A high percentage of insoluble,
1.2 Thistestmethodisintendedtobeusedinapproximating suspended solid material can create pumping, filtering, or
the amount of insoluble, suspended solids in determining the grinding difficulties in the off-loading of bulk shipments of
material handling characteristics and fuel quality of OLHW. It OLHW and can contribute to excessive wear on processing
isnotintendedtoreplacemoresophisticatedproceduresforthe equipment. High solids can also decrease the quality and
determination of total solids. consistency of commingled fuel by decreasing the effective-
1.3 This standard does not purport to address all of the ness of agitation in storage tanks.
safety concerns, if any, associated with its use. It is the
5. Apparatus
responsibility of the user of this standard to establish appro-
5.1 Centrifuge—Capable of spinning two or more centri-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. fuge tubes at a speed controlled to give a relative centrifugal
force of between 1200 to 1400. The speed to achieve this is
2. Referenced Documents
generally between 3100 to 3600 rpm. The rotation speed
2.1 ASTM Standards: necessary to achieve the relative centrifugal force can be
D 96 Test Methods for Water and Sediment in Crude Oil by determined from one of the following equations:
2
Centrifuge Method (Field Procedure)
rpm 5 1335 rcf/d (1)
rpm 5 265 rcf/d (2)
3. Summary of Test Method
3.1 A 10-mL aliquot of OLHW sample is decanted into a
where:
15-mL graduated centrifuge tube and centrifuged for 3 min.
rpm = rotation speed, in revolutions per min,
The separated liquid phase of the OLHW is decanted into an rcf = relative centrifugal force,
appropriate waste vessel. The centrifuge tube with the sepa- d = diameter of swing, in mm (Eq 1) or in. (Eq 2),
rated solid material is brought back to its original 10-mL measured between the tips of opposite tubes when
volume with a user-selected blend of clean solvents and the tubes are in rotating position.
agitated to mix the solid and liquid phases. The tube is
NOTE 1—Eq 1 and Eq 2 are described in Test Method D 96.
centrifuged for 2 min, and the amount of remaining solid
5.2 Centrifuge Tubes— Centrifuge tubes shall be cone
material is read.
shaped, made of glass or a solvent resistant plastic or polymer,
have a minimum capacity of 15 mLwhen filled to volume, and
1
This test method is under the jurisdiction of ASTM Committee D34 on Waste graduated with minimum subdivisions of 0.5 mL. Class A
Management and is the direct responsibility of Subcommittee D34.01.06 on
centrifuge tubes are recommended. If any grade other than
Analytical Methods.
Class A is used, refer to the section on Calibration and
Current edition approved March 10, 2003. Published June 2003. Originally
Standardization.
approved in 1997. Last previous edition approved in 1997 as D 6050 – 97.
2
Discontinued. See 1999 Annual Book of ASTM Standards, Vol 05.01.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn. Contact ASTM
International (www.astm.org) for the latest information.
D6050–97 (2003)
6. Reagents and Materials 9.2 Place the tubes from 8.1 in the trunnion cups or
centrifuge tube slots on opposite sides of the centrifuge. Close
6.1 Purity of Reagents—Reagent grade chemicals shall be
the centrifuge lid and engage safety lock, if so equipped.
used in all tests. Unless otherwise indicated, it is intended that
9.3 Set the centrifuge speed (r/min) to provide a minimum
all reagents conform to the specifications of the Committee on
relative centrifugal force between 1200 to 1400 (see 5.1).
Analytical Reagents of the American Chemical Society where
3
9.4 Engage centrifuge, and allow to spin for 3 min.
such specifications are available. Other grades ma
...

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