Standard Practice for Collection of Floor Dust for Chemical Analysis

SIGNIFICANCE AND USE
This practice may be used to collect dust from carpeted or bare floor surfaces for gravimetric or chemical analysis. The collected sample is substantially unmodified by the sampling procedure.
This practice provides for a reproducible dust removal rate from level loop and plush carpets, as well as bare floors. It has the ability to achieve relatively constant removal efficiency at different loadings of surface dust.
This practice also provides for the efficient capture of semivolatile organic chemicals associated with the dust. The test system can be fitted with special canisters downstream of the cyclone for the capture of specific semivolatile organic chemicals that may volatilize from the dust particles during collection.
This practice does not describe procedures for evaluation of the safety of floor surfaces or the potential human exposure to carpet dust. It is the user’responsibility to evaluate the data collected by this practice and make such determinations in the light of other available information.
FIG. 1 Floor Dust Sampler Using a Commercial Vacuum Cleaner as the Suction Source
SCOPE
1.1 This practice covers a procedure for the collection of a sample of dust from carpets and bare floors that can be analyzed for lead, pesticides, or other chemical compounds and elements.
1.2 This practice is applicable to a variety of carpeted and bare floor surfaces. It has been tested for level loop and plush pile carpets and bare wood floors, specifically.
1.3 This practice is not intended for the collection and evaluation of dust for the presence of asbestos fibers.
1.4 The values stated in SI units are to be regarded as the standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
28-Feb-2005
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM D5438-05 - Standard Practice for Collection of Floor Dust for Chemical Analysis
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation: D5438 – 05
Standard Practice for
1
Collection of Floor Dust for Chemical Analysis
This standard is issued under the fixed designation D5438; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3.1.1 carpet-embedded dust—soilandotherparticulatemat-
ter, approximately 5-µm equivalent aerodynamic diameter and
1.1 This practice covers a procedure for the collection of a
larger, embedded in carpet pile and normally removable by
sample of dust from carpets and bare floors that can be
household vacuum cleaners.
analyzedforlead,pesticides,orotherchemicalcompoundsand
3.1.2 surface dust—soil and other particulate matter, ap-
elements.
proximately 5-µm equivalent aerodynamic diameter and larger,
1.2 This practice is applicable to a variety of carpeted and
adhering to floor surfaces and normally removable by house-
bare floor surfaces. It has been tested for level loop and plush
hold vacuum cleaners.
pile carpets and bare wood floors, specifically.
1.3 This practice is not intended for the collection and
4. Summary of Practice
evaluation of dust for the presence of asbestos fibers.
4.1 The sampling method described in this practice is taken
1.4 The values stated in SI units are to be regarded as the
3
from work published in Roberts, et al (1-3), and Stamper, et al
standard.
(4).
1.5 This standard does not purport to address all of the
4.2 Particulate matter is withdrawn from the carpet or bare
safety concerns, if any, associated with its use. It is the
floor by means of vacuum-induced suction which draws
responsibility of the user of this standard to establish appro-
through a sampling nozzle at a specific velocity and flow rate,
priate safety and health practices and determine the applica-
and the particles are separated mechanically by a cyclone. The
bility of regulatory limitations prior to use.
cyclone is designed to efficiently separate and collect particles
2. Referenced Documents approximately 5-µm mean aerodynamic diameter and larger.
2
However,muchsmallerparticlesarealsocollectedatunknown
2.1 ASTM Standards:
efficiencies. The sampling system allows for height, air flow,
D422 Test Method for Particle-Size Analysis of Soils
and suction adjustments to reproduce systematically a specific
D1356 Terminology Relating to Sampling and Analysis of
air velocity for the removal of particulate matter from carpeted
Atmospheres
and bare floor surfaces, so that these sampling conditions can
E1 Specification for ASTM Liquid-in-Glass Thermometers
be repeated.
E337 Test Method for Measuring Humidity with a Psy-
chrometer (the Measurement of Wet- and Dry-Bulb Tem-
NOTE 1—Side-by-side comparison of the HVS3 and a conventional
peratures) upright vacuum cleaner revealed that both collected particles down to at
least 0.2 µm and that the HVS3 was more efficient at collecting particles
F608 Test Method for Evaluation of Carpet Embedded Dirt
smaller than 20 µm than conventional vacuum cleaners (5). If desired, a
Removal Effectiveness of Household/Commercial Vacuum
fine-particle filter may be added downstream of the cyclone to collect
Cleaners
99.9 % of particles above 0.2 µm aerodynamic mean diameter.
3. Terminology
4.3 The particulate matter in the air stream is collected in a
catch bottle attached to the bottom of the collection cyclone.
3.1 Definitions—For definitions of terms used in this prac-
This catch bottle shall be capped for storage of the sample and
tice, refer to Terminology D1356.
transported to the laboratory for analysis.
1 5. Significance and Use
This practice is under the jurisdiction of ASTM Committee D22 on Sampling
and Analysis of Atmospheres and is the direct responsibility of Subcommittee
5.1 This practice may be used to collect dust from carpeted
D22.05 on Indoor Air.
or bare floor surfaces for gravimetric or chemical analysis.The
Current edition approved March 1, 2005. Published March 2005. Originally
collected sample is substantially unmodified by the sampling
approved in 1993. Last previous edition approved in 2000 as D5438 - 00. DOI:
10.1520/D5438-05.
procedure.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The boldface numbers in parentheses refer to the list of references at the end of
the ASTM website. this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D5438 – 05
FIG. 1 Floor Dust
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