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ASTM D1582-98(2011)

(Test Method)

Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives

Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives

ABSTRACT
This test method covers the determination of nonvolatile content or total solids of liquid phenol, resorcinol, and melamine adhesives with or without hardener added and containing high-boiling and low-boiling volatile organic solvents or water, or both. The equipments to be used in the test shall include a petri dish, circulating-air oven, desiccator, and analytical balance. In determining the nonvolatile content of the liquid adhesives without hardener, the procedure shall include oven-drying, cooling in a desiccator, and weighing of adhesive and quartz sand . The percent nonvolatile content shall be calculated based on the amount remaining. On the other hand, the procedure for the liquid adhesives with hardener shall include oven-drying, cooling in a desiccator, and weighing of mixed adhesives. Also, the percent nonvolatile content shall be calculated based on the amount remaining.
SCOPE
1.1 This test method covers the determination of nonvolatile content or total solids of liquid phenol, resorcinol, and melamine adhesives with or without hardener (Note 1) added and containing high-boiling and low-boiling volatile organic solvents or water, or both.
Note 1—Some low molecular weight materials in the adhesive may be lost if hardener is not used. When a hardener is used, it must be mixed in accordance with the manufacturer's instructions.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautions, see 5.2.

General Information

Status
Historical
Publication Date
31-Mar-2011
ICS
83.180 - Adhesives
Technical Committee
D14 - Adhesives
Drafting Committee
D14.30 - Wood Adhesives
Current Stage
Ref Project

Relations

Replaces
ASTM D1582-98(2004) - Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives
Effective Date
01-Apr-2011
Referred By
ASTM D4426-01(2021) - Standard Test Method for Determination of Percent Nonvolatile Content of Liquid Phenolic Resins Used for Wood Laminating
Effective Date
01-Apr-2011
Referred By
ASTM D1579-01(2018) - Standard Test Method for Filler Content of Phenol, Resorcinol, and Melamine Adhesives
Effective Date
01-Apr-2011

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ASTM D1582-98(2011) - Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine AdhesivesASTM D1582-98(2011) - Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives
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ASTM D1582-98(2011) - Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1582 − 98 (Reapproved 2011)
Standard Test Method for
Nonvolatile Content of Liquid Phenol, Resorcinol, and
Melamine Adhesives
This standard is issued under the fixed designation D1582; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4.2 With Hardener—A weighed amount of mixed adhesive
is oven dried, cooled in a desiccator, and weighed. The percent
1.1 This test method covers the determination of nonvolatile
nonvolatile content is calculated based on the amount remain-
content or total solids of liquid phenol, resorcinol, and
ing.
melamine adhesives with or without hardener (Note 1) added
and containing high-boiling and low-boiling volatile organic
5. Apparatus
solvents or water, or both.
5.1 Petri Dish, 00 by 22 mm or its equivalent.
NOTE 1—Some low molecular weight materials in the adhesive may be
5.2 Circulating-Air Oven, capable of maintaining tempera-
lost if hardener is not used. When a hardener is used, it must be mixed in
accordance with the manufacturer’s instructions.
tures of 70 6 1°C, 105 6 1°C, and 150 6 1°C. (Warning —A
safety (explosion-proof) oven should be used when volatile
1.2 The values stated in SI units are to be regarded as
materials are likely to burn or explode.)
standard. No other units of measurement are included in this
standard.
5.3 Desiccator, with drying agent and tray.
1.3 This standard does not purport to address all of the
5.4 Analytical Balance, accurate to 1 mg.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
6. Sampling
priate safety and health practices and determine the applica-
6.1 Except in special cases, take a composite sample from
bility of regulatory limitations prior to use. For specific
three or more separate containers chosen at random.Also, take
precautions, see 5.2.
samples from containers which appear to be nonrepresentative
and test such samples separately. Place the samples immedi-
2. Referenced Documents
ately in airtight containers, filled to prevent excessive air space
2.1 ASTM Standards:
above the adhesive, and take precautions to reduce evaporation
D907 Terminology of Adhesives
or drying to a minimum. Mix the adhesive in the container
thoroughly if there is a tendency for the materials to separate.
3. Terminology
6.2 Test three specimens of each sample.
3.1 Definitions—Many of the terms in this test method are
defined in Terminology D907.
7. Procedure
7.1 70°C Drying Temperature Without Hardener:
4. Summary of Test Method
7.1.1 Place approximately 20 g of the adhesive in a covered
4.1 Without Hardener—A weighed amount of adhesive and
weighing bottle.
quartz sand are oven-dried, cooled in a desiccator, and
7.1.2 Place approximately 10 g of fine, oven-dried quartz
weighed. The percent nonvolatile content is calculated based
sand in an open Petri dish, together with a small glass stirring
on the amount remaining.
rod, and weigh the dish, rod, and contents to the nearest 1 mg
on the analytical balance. Weigh out to the nearest 1 mg
This test method is under the jurisdiction of ASTM Committee D14 on
approximately2gofthe adhesive by difference from the
Adhesives and is the direct responsibility of Subcommittee D14.30 on Wood
weighing bottle, keeping the bottle covered as much as
Adhesives.
possible. Mix the adhesive and quartz sand intimately by
Current edition approved April 1, 2011. Published April 2011. Originally
means of the stirring rod and distribute uniformly over the
approved in 1958. Last previous edition approved in 2004 as D1582 – 98 (2004).
DOI: 10.1520/D1582-98R11.
bottom of the dish in as t
...

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ABSTRACT
This test method covers the determination of nonvolatile content or total solids of liquid phenol, resorcinol, and melamine adhesives with or without hardener added and containing high-boiling and low-boiling volatile organic solvents or water, or both. The equipments to be used in the test shall include a petri dish, circulating-air oven, desiccator, and analytical balance. In determining the nonvolatile content of the liquid adhesives without hardener, the procedure shall include oven-drying, cooling in a desiccator, and weighing of adhesive and quartz sand . The percent nonvolatile content shall be calculated based on the amount remaining. On the other hand, the procedure for the liquid adhesives with hardener shall include oven-drying, cooling in a desiccator, and weighing of mixed adhesives. Also, the percent nonvolatile content shall be calculated based on the amount remaining.
SCOPE
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SCOPE
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This specification provides the means to measure and evaluate the performance of adhesives for structural or semistructural bonding of wood-to-wood in manufactured homes. Wood as used in this specification includes lumber, plywood, particleboard, gypsum board, and all materials having woodbased surfaces at the bondline. The adhesives can be classified according to resistance to deformation: Group A or structural, and Group B or semistructural. Also, the adhesives may be designated into three types, according to their recommended use based on their resistance to water and water vapor: Type 1 for interior and exterior use, Type 2 for weather-protected interior use, and Type 3 for interior use only. Different tests shall be performed in order to determine the following properties of adhesives: shear strength, gap-filling ability, total deformation resistance, moisture and temperature limitation during fabrication, high-temperature resistance, low-temperature resistance, moisture resistance, aging, oxidation resistance, and mold resistance.
SCOPE
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1.1.1 The performance of the adhesives is measured in the following tests:    
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ASTM D907-15(2023)(Terminology)
Standard Terminology of Adhesives

SCOPE
1.1 This terminology standard is a compilation of definitions used in the science and technology of the adhesives industry. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 Any changes in this standard since 1988 are documented as follows:  
1.2.1 Appendix X1 gives a history of revisions made since 1988. Table X1.1 lists the terms that are affected as: (1) Terms Added, (2) Terms Revised, and (3) Terms Deleted.
1.2.1.1 In Table X1.1, the year of publication in Volume 15.06 is shown in parentheses following the term.  
1.2.2 In the text of the standard, the year of publication is shown following each definition. Also, the following codes are included after the year of publication to describe the type change that was made: (A) Addition, (R) Revision, or (E) Edited.  
1.2.3 Deletions are shown in Appendix X1, suitably footnoted. The deleted terms do not appear in the text of the standard.  
1.2.4 Any special circumstances not covered by 1.2.2 and 1.2.3 are documented in Table X1.1, suitably footnoted.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D7966/D7966M-16(2023)(Test Method)
Standard Test Method for Resistance to Creep of Adhesives in Static Shear by Compression Loading (Wood-to-Wood)

SIGNIFICANCE AND USE
5.1 This test method evaluates the performance of the adhesive in laminated wood as measured by resistance to creep under static load.  
5.2 Test results from the evaluation of adhesive creep resistance, under designated environmental conditions of the test, provide a measure of the adhesive’s ability to withstand constant loading over a relatively long period of time.  
5.3 Creep measured with this test method is normally used in conjunction with specifications such as, but not limited to Specification D2559 and CSA O112.9 to confirm suitability of an adhesive to resist creep under designed loads when subjected to specific levels of stress, load duration and environmental conditions.
SCOPE
1.1 This test method covers the determination of creep properties of structural adhesives in wood-to-wood bonds when a standardized specimen is subjected to shearing stresses at various levels of static load, constant temperature, and relative humidity. Apparatus and procedures are provided for shear deformation (creep) of adhesive bonds under static load. This test method is used under the indicated conditions to evaluate resistance to creep properties of a structural wood adhesive.  
1.2 The test method is used to evaluate creep performance of adhesives suitable for the bonding of wood, including treated wood, into structural wood products for general construction, marine use, or for other uses where a high-strength general construction, creep-resistant, durable adhesive bond is required. Individual block shear specimens are prepared from adhesively bonded laminations, subjected to a constant load under various combinations of temperature and relative humidity, and the amount of creep measured.  
1.3 Creep of structural wood adhesives as measured by this test method may not be comparative to other ASTM methods and is limited to the conditions of the test and procedures contained herein.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4800-94(2023)(Guide)
Standard Guide for Classifying and Specifying Adhesives

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4.1 The purpose of this classification system is to provide a method of identifying adhesives in order to give industry a system that can be used universally for materials. It further provides a means for specifying these materials by the use of the standards that are developed using this guide.  
4.2 This classification system was developed to permit the addition of future adhesives.
SCOPE
1.1 This guide provides a classification system for tabulating the properties of adhesives suitable for holding parts or assemblies together. The use of this guide also provides information necessary for the development of standard specifications for adhesives.  
Note 1: This classification system may serve many of the needs of industries using adhesives. This guide is subject to revision as the need requires; therefore, the latest revision should always be used.  
1.2 Limitations—This classification system is intended to be a means of identifying adhesives. It is not intended for the selection of materials. Material selection should be made by those having expertise in the adhesives field after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the attachment process to be employed, the inherent properties of the material not covered in this document, and the economic factors.  
1.3 This classification system is based on the premise that adhesives can be arranged into broad generic families using basic properties to arrange the materials into groups, classes, and grades.  
1.4 In all cases where the provisions of this classification system would conflict with the referenced ASTM specification for a particular material, the latter shall take precedence.  
1.5 The values stated in SI units, as detailed in IEEE/ASTM SI 10, are to be regarded as the standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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