Standard Test Methods for Quantitative Extraction of Asphalt Binder from Asphalt Mixtures

SIGNIFICANCE AND USE
4.1 All of these test methods can be used for quantitative determinations of asphalt binder in asphalt mixtures and pavement samples for specification acceptance, service evaluation, control, and research. Each method prescribes the solvent or solvents and any other reagents that can be used in the test method.
Note 2: Further testing of the asphalt mixture may be performed by using sieve analysis on the extracted aggregate, Test Method D5444, or recovering the extracted asphalt binder from solution by Test Method D1856, Practice D5404/D5404M, or Practice D7906 for asphalt binder property testing. When recovering the asphalt binder for property testing, all mineral matter should be removed from the effluent.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing/sampling/inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 These test methods cover the quantitative determination of asphalt binder content in asphalt mixtures and pavement samples. Aggregate obtained by these methods may be used for sieve analysis using Test Method D5444. This test is not appropriate for testing asphalt mixtures containing coal tar.  
1.2 Asphalt binder may be recovered using Test Method D1856, Practice D5404/D5404M, or Practice D7906.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards are given in Section 7.
Note 1: The results obtained by these test methods may be affected by the age of the material tested, with older samples tending to yield slightly lower asphalt binder content. Best quantitative results are obtained when the test is made on mixtures and pavements shortly after their preparation. It is difficult to remove all the asphalt when some aggregates are used and some chlorides may remain within the mineral matter affecting the measured asphalt content.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
31-Mar-2017
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ASTM D2172/D2172M-17e1 - Standard Test Methods for Quantitative Extraction of Asphalt Binder from Asphalt Mixtures
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
´1
Designation: D2172/D2172M − 17
Standard Test Methods for
Quantitative Extraction of Asphalt Binder from Asphalt
1
Mixtures
This standard is issued under the fixed designation D2172/D2172M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—11.2.5.1 was corrected editorially in May 2018.
1. Scope ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
1.1 These test methods cover the quantitative determination
mendations issued by the World Trade Organization Technical
of asphalt binder content in asphalt mixtures and pavement
Barriers to Trade (TBT) Committee.
samples.Aggregateobtainedbythesemethodsmaybeusedfor
sieve analysis using Test Method D5444. This test is not
2. Referenced Documents
appropriate for testing asphalt mixtures containing coal tar.
2
2.1 ASTM Standards:
1.2 Asphalt binder may be recovered using Test Method
C128 Test Method for Relative Density (Specific Gravity)
D1856, Practice D5404/D5404M, or Practice D7906.
and Absorption of Fine Aggregate
C670 Practice for Preparing Precision and Bias Statements
1.3 Units—The values stated in either SI units or inch-
pound units are to be regarded separately as standard. The for Test Methods for Construction Materials
D70 Test Method for Density of Semi-Solid Asphalt Binder
values stated in each system may not be exact equivalents;
therefore,eachsystemshallbeusedindependentlyoftheother. (Pycnometer Method)
D604 Specification for Diatomaceous Silica Pigment (With-
Combining values from the two systems may result in noncon-
3
formance with the standard. drawn 2003)
D979/D979M Practice for Sampling Bituminous Paving
1.4 The text of this standard references notes and footnotes
Mixtures
which provide explanatory material. These notes and footnotes
D1461 Test Method for Moisture or Volatile Distillates in
(excluding those in tables and figures) shall not be considered
Asphalt Mixtures
as requirements of the standard.
D1856 Test Method for Recovery of Asphalt From Solution
1.5 This standard does not purport to address all of the
by Abson Method
safety concerns, if any, associated with its use. It is the
D2111 Test Methods for Specific Gravity and Density of
responsibility of the user of this standard to establish appro-
Halogenated Organic Solvents and Their Admixtures
priate safety, health, and environmental practices and deter-
D3666 Specification for Minimum Requirements for Agen-
mine the applicability of regulatory limitations prior to use.
cies Testing and Inspecting Road and Paving Materials
Specific hazards are given in Section 7.
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
ances and Standard Masses for Use in Soil, Rock, and
NOTE 1—The results obtained by these test methods may be affected by
the age of the material tested, with older samples tending to yield slightly
Construction Materials Testing
lower asphalt binder content. Best quantitative results are obtained when
D5404/D5404M Practice for Recovery of Asphalt from So-
the test is made on mixtures and pavements shortly after their preparation.
lution Using the Rotary Evaporator
It is difficult to remove all the asphalt when some aggregates are used and
D5444 Test Method for Mechanical Size Analysis of Ex-
some chlorides may remain within the mineral matter affecting the
measured asphalt content. tracted Aggregate
D6368 Specification for Vapor-Degreasing Solvents Based
1.6 This international standard was developed in accor-
on normal-Propyl Bromide and Technical Grade normal-
dance with internationally recognized principles on standard-
Propyl Bromide
1 2
These test methods are under the jurisdiction of ASTM Committee D04 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Road and Paving Materials and are the direct responsibilities of Subcommittee contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
D04.25 on Analysis of Asphalt Mixtures. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved April 1, 2017. Published April 2017. Originally the ASTM website.
3
approved in 1963. Last previous edition approved in 2011 as D2172/D2172M – 11. The last approved version of this historical standard is referenced on
DOI: 10.1520/D2172_D2172M-17E01. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United S
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