Standard Test Method for Density of Adhesives in Fluid Form

SIGNIFICANCE AND USE
4.1 This test method is particularly applicable where the fluid has too high a viscosity or where a component is too volatile for a specific gravity balance determination.
SCOPE
1.1 This test method covers the measurement of density (weight per gallon) of adhesives, and components thereof, when in liquid form.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Sep-2013
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM D1875-03(2013) - Standard Test Method for Density of Adhesives in Fluid Form
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1875 − 03 (Reapproved 2013)
Standard Test Method for
Density of Adhesives in Fluid Form
This standard is issued under the fixed designation D1875; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 5. Apparatus
1.1 This test method covers the measurement of density 5.1 Weight-Per-Gallon Cup—A weight-per-gallon cup of
plated brass or stainless steel with counterbalance is recom-
(weight per gallon) of adhesives, and components thereof,
when in liquid form. mended.Thecapacityofthiscupwithcoverisexactly83.2mL
(2.81 fl oz) at 25°C (77°F).
1.2 The values stated in SI units are to be regarded as the
NOTE 1—The use of cups that are factory calibrated eliminates the need
standard. The values given in parentheses are for information
for further calibration. These cups are calibrated with distilled water so
only.
that their proper net weight is obtained at 25°C.Atemperature of 25°C is
1.3 This standard does not purport to address all of the
therefore recommended when using these cups.Volume expansion of both
cup and the material to be measured causes erroneous results, if the matter
safety concerns, if any, associated with its use. It is the
of temperature is not standardized. However, where less accuracy is
responsibility of the user of this standard to establish appro-
required, consideration of temperature differentials may be ignored.
priate safety and health practices and determine the applica-
5.2 Thermometer—ASTM Saybolt Viscosity Thermometer
bility of regulatory limitations prior to use.
having a range from 19 to 27°C (66 to 80.5°F) and conforming
2. Referenced Documents
to the requirements for Thermometer 17C as prescribed in
Specification E1.
2.1 ASTM Standards:
D907 Terminology of Adhesives
5.3 Constant-Temperature Bath, capable of maintaining a
E1 Specification for ASTM Liquid-in-Glass Thermometers
temperature of 25 6 0.1°C (77 6 0.5°F).
E691 Practice for Conducting an Interlaboratory Study to
5.4 Laboratory Balance, 200 g (0.44 lb) or greater capacity,
Determine the Precision of a Test Method
accurate to 60.1 g (0.0002 lb).
3. Terminology
NOTE 2—A hanging pan, triple-beam balance, or overhead-beam type
ofbalancewithscalesgraduatedto0.1ghasbeenfoundtoprovideresults,
3.1 Definitions—Many terms in this test method are defined
the mean of which was consistent with the over all precision and accuracy
in Terminology D907.
of this test method.
NOTE 3—Fingerprints and smudges on the cup changes the weight and
3.2 Definitions of Terms Specific to This Standard:
is to be avoided. Handle only with tongs and with hands protected by
3.2.1 density, n—the mass (weight in vacuum) of a unit
clean, dry, absorbent material.
volume of the liquid at any given temperature expressed as the
6. Sampling
weight in pounds avoirdupois, of a U.S. gallon measure of the
liquid at 25°C, unless otherwise specified.
6.1 Take representative samples of the lot to be evaluated
from three or more separate containers, chosen at random. Do
4. Significance and Use
not take samples from containers that appear to be nonrepre-
4.1 This test method is particularly applicable where the
sentative. Place the samples in airtight containers, filled to
fluid has too high a viscosity or where a component is too
prevent excessive air space above the adhesive, and stored at
volatile for a specific gravity balance determination.
room temperature to reduce evaporation or drying to a mini-
mum. Ensure that the adhesive in the container is thoroughly
This test method is under the jurisdiction of ASTM Committee D14 on
mixed if there is a tendency for the materials to separate.
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
Properties.
7. Procedure
Current edition approved Oct. 1, 2013. Published October 2013. Originally
ε1
7.1 Test three portions of each sample.
approved in 1961. Last previous edition approved in 2008 as D1875 – 03 (2008) .
DOI: 10.1520/D1875-03R13.
7.2 Clean and dry the cup with nonresidual solvents.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on Weight-per-gallon cups may be obtained from the Paul N. Gardner Co.,
the ASTM website. Pompano Beach, FL.
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