Standard Test Method for Determining the Presence of Expanding Clays in Rock for Erosion Control Using Ethylene Glycol

SIGNIFICANCE AND USE
5.1 Rock for erosion control consists of individual pieces of natural quarried stone or large boulders and cobbles. The ability of these individual pieces of stone to resist deterioration due to weathering action affects the stability of the integral placement of rock for erosion control and hence, the stability of construction projects, structures, shorelines, and stream banks.  
5.2 Deterioration of stone in this test is one indicator that similar samples exposed to wet/dry and freeze/thaw cycles may break down in a water-soaked environment condition in service.  
5.3 This test method was developed to be used in conjunction with additional test methods listed in Practice D4992. This test method provides a quantitative value indicating potential resistance to weathering; however, the results of this test method are not to be used as the sole basis for the determination of rock durability.
Note 1: The quality of the result produced by this standard is dependent upon the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluation some of those factors.
SCOPE
1.1 This test method covers the testing for and quantitative determination of the presence of swelling clays of the smectite group in rock for erosion control. The test particles are intended to be representative of erosion control rock and its durability. The test is appropriate for breakwater stone, armor stone, riprap and gabion sized rock materials.  
1.2 Ethylene glycol is one of the materials that react with swelling clays to form an organoclay complex having a larger basal spacing than that of the clay mineral itself. Rock containing swelling clay of the smectite group will be expected to undergo expansive breakdown upon soaking in ethylene glycol. If the amount, distribution, state of expansion, and ability to take up glycol is such as to cause such breakdown to occur, it may be expected that similar breakdown may occur of similar rock samples exposed, for longer times, to wetting and drying or freezing and thawing in a water-soaked condition in service.  
1.3 The prepared size of the rock specimens may eliminate some of the internal features present in the gross structure. The test specimens may not be representative of the quality of the larger rock samples used in construction. Careful examination of the rock source and proper sampling are essential in minimizing this limitation.  
1.3.1 The test is time intensive and requires over two weeks to complete the sample preparation, testing and analysis portions of the procedure.  
1.4 The use of reclaimed concrete and materials other than natural rock is beyond the scope of this test method.  
1.5 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.5.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The slug unit is not given unless dynamic (F=ma) calculations are involved.  
1.5.2 The SI units presented for apparatus are substitutions of the inch-pound units, other similar SI units should be acceptable providing they meet the technical requirements established by the inch-po...

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30-Apr-2021
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ASTM D8281/D8281M-21 - Standard Test Method for Determining the Presence of Expanding Clays in Rock for Erosion Control Using Ethylene Glycol
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8281/D8281M − 21
Standard Test Method for
Determining the Presence of Expanding Clays in Rock for
1
Erosion Control Using Ethylene Glycol
This standard is issued under the fixed designation D8281/D8281M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope conformance with the standard. Reporting of test results in
units other than SI shall not be regarded as nonconformance
1.1 This test method covers the testing for and quantitative
with this standard.
determination of the presence of swelling clays of the smectite
1.5.1 The gravitational system of inch-pound units is used
group in rock for erosion control. The test particles are
when dealing with inch-pound units. In this system, the pound
intended to be representative of erosion control rock and its
(lbf) represents a unit of force (weight), while the unit for mass
durability. The test is appropriate for breakwater stone, armor
is slugs. The slug unit is not given unless dynamic (F=ma)
stone, riprap and gabion sized rock materials.
calculations are involved.
1.2 Ethylene glycol is one of the materials that react with
1.5.2 The SI units presented for apparatus are substitutions
swelling clays to form an organoclay complex having a larger
of the inch-pound units, other similar SI units should be
basal spacing than that of the clay mineral itself. Rock
acceptable providing they meet the technical requirements
containing swelling clay of the smectite group will be expected
established by the inch-pound apparatus.
to undergo expansive breakdown upon soaking in ethylene
1.5.3 It is common practice in the engineering/construction
glycol. If the amount, distribution, state of expansion, and
profession to concurrently use pounds to represent both a unit
ability to take up glycol is such as to cause such breakdown to
of mass (lbm) and force (lbf). This practice implicitly com-
occur, it may be expected that similar breakdown may occur of
bines two separate systems of units: the absolute and the
similar rock samples exposed, for longer times, to wetting and
gravitational systems. It is scientifically undesirable to com-
drying or freezing and thawing in a water-soaked condition in
bine the use of two separate sets of inch-pound units within a
service.
single standard. As stated, this standard includes the gravita-
tional system of inch-pound units and does not use/present the
1.3 The prepared size of the rock specimens may eliminate
slug unit for mass. However, the use of balances or scales
some of the internal features present in the gross structure.The
3
recording pounds of mass (lbm) or recording density in lbm/ft
test specimens may not be representative of the quality of the
shall not be regarded as nonconformance with this standard.
larger rock samples used in construction. Careful examination
of the rock source and proper sampling are essential in 1.5.4 Calculations are done using only one set of units;
either SI or gravitational inch pound. Other units are permis-
minimizing this limitation.
sible provided appropriate conversion factors are used to
1.3.1 The test is time intensive and requires over two weeks
maintain consistency of units throughout the calculations, and
to complete the sample preparation, testing and analysis
similar significant digits or resolution, or both are maintained.
portions of the procedure.
1.6 All observed and calculated values shall conform to the
1.4 The use of reclaimed concrete and materials other than
guidelines for significant digits and rounding established in
natural rock is beyond the scope of this test method.
Practice D6026, unless superseded by this standard.
1.5 Units—The values stated in either SI units or inch-
1.6.1 For purposes of comparing measured or calculated
pound units are to be regarded separately as standard. The
value(s) with specified limits, the measured or calculated
values stated in each system may not be exact equivalents;
value(s) shall be rounded to the nearest decimal or significant
therefore,eachsystemshallbeusedindependentlyoftheother.
digits in the specified limits.
Combining values from the two systems may result in non-
1.6.2 Theproceduresusedtospecifyhowdataarecollected/
recorded or calculated, in this standard are regarded as the
industry standard. In addition, they are representative of the
1
This test method is under the jurisdiction ofASTM Committee D18 on Soil and
significant digits that generally should be retai
...

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