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ASTM D5396-04(2020)

(Specification)

Standard Specification for Reclaimed Perchloroethylene

Standard Specification for Reclaimed Perchloroethylene

ABSTRACT
This specification establishes the requirements for reclaimed perchloroethylene typically needed in various industries for noncritical applications such as in metal cleaning formulations. This is not recommended for dry cleaning applications, but may be used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs. Covered here are the following types: Type I, generally recognized for use in precision applications; Type II, used for less demanding precision applications; and Type III, general purpose technical grade. Specimens shall be tested and each type should conform individually to the following properties: specific gravity; maximum compositions for chlorides, nonvolatile residue, water, and 1,1,1-trichloroethane; assay weight; color (Pt-Co scale); appearance; acid acceptance (as NaOH); and acidity (as HCl).
SCOPE
1.1 This specification covers the grade of perchloroethylene typically needed in various industries for noncritical applications, such as in metal cleaning formulations. It is not recommended for dry cleaning applications (see Specification D4081). It may be used as a reference document by purchasers or by persons establishing in-house perchloroethylene recovery programs.  
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Dec-2019
ICS
71.080.20 - Halogenated hydrocarbons
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.02 - Vapor Degreasing
Current Stage
Ref Project

Relations

Replaces
ASTM D5396-04(2015) - Standard Specification for Reclaimed Perchloroethylene
Effective Date
01-Jan-2020
Refers
ASTM E1064-24 - Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
Effective Date
01-Jan-2024
Refers
ASTM D3741-00(2020) - Standard Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents
Effective Date
01-Apr-2020
Refers
ASTM D2988-96(2020) - Standard Test Methods for Water-Soluble Halide Ion in Halogenated Organic Solvents and Their Admixtures
Effective Date
01-Apr-2020
Refers
ASTM D2111-10(2020) - Standard Test Methods for Specific Gravity and Density of Halogenated Organic Solvents and Their Admixtures
Effective Date
01-Apr-2020
Refers
ASTM D2108-10(2020) - Standard Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
Effective Date
01-Jan-2020
Refers
ASTM D2108-10(2015) - Standard Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
Effective Date
01-Jun-2015
Refers
ASTM D2111-10(2015) - Standard Test Methods for Specific Gravity and Density of Halogenated Organic Solvents and Their Admixtures
Effective Date
01-Jun-2015
Refers
ASTM D2988-96(2015) - Standard Test Methods for Water-Soluble Halide Ion in Halogenated Organic Solvents and Their Admixtures
Effective Date
01-Jun-2015
Refers
ASTM D3741-00(2015)e1 - Standard Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents
Effective Date
01-Jun-2015
Refers
ASTM D2942-02(2013) - Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods)
Effective Date
01-Feb-2013
Refers
ASTM D3401-97(2012) - Standard Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
Effective Date
01-Mar-2012
Refers
ASTM D6806-02(2012) - Standard Practice for Analysis of Halogenated Organic Solvents and Their Admixtures by Gas Chromatography
Effective Date
01-Mar-2012
Refers
ASTM D2109-01(2011) - Standard Test Methods for Nonvolatile Matter in Halogenated Organic<br> Solvents and Their Admixtures
Effective Date
01-Aug-2011
Refers
ASTM D4081-00(2011) - Standard Specification for Drycleaning-Grade Perchloroethylene
Effective Date
01-Aug-2011

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ASTM D5396-04(2020) - Standard Specification for Reclaimed PerchloroethyleneASTM D5396-04(2020) - Standard Specification for Reclaimed Perchloroethylene
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ASTM D5396-04(2020) - Standard Specification for Reclaimed Perchloroethylene
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Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5396 −04 (Reapproved 2020)
Standard Specification for
1,2
Reclaimed Perchloroethylene
This standard is issued under the fixed designation D5396; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D3741 Test Methods for Appearance of Admixtures Con-
taining Halogenated Organic Solvents
1.1 This specification covers the grade of perchloroethylene
D4081 Specification for Drycleaning-Grade Perchloroethyl-
typically needed in various industries for noncritical
ene
applications, such as in metal cleaning formulations. It is not
D6806 Practice for Analysis of Halogenated Organic Sol-
recommended for dry cleaning applications (see Specification
vents and Their Admixtures by Gas Chromatography
D4081). It may be used as a reference document by purchasers
E1064 Test Method for Water in Organic Liquids by Coulo-
orbypersonsestablishingin-houseperchloroethylenerecovery
metric Karl Fischer Titration
programs.
2.2 Code of Federal Regulations:
1.2 This international standard was developed in accor-
29 CFR 1910.1200 Department of Labor, OSHA Regula-
dance with internationally recognized principles on standard-
tions on Hazard Communication
ization established in the Decision on Principles for the
49 CFR 100 to 199 Department ofTransportation Hazardous
Development of International Standards, Guides and Recom-
Materials Regulations
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee. 3. Classification
3.1 Type I—Generally recognized for use in precision ap-
2. Referenced Documents
plications.
2.1 ASTM Standards:
3.2 Type II—Use for less demanding precision applications.
D2108 Test Method for Color of Halogenated Organic
3.3 Type III—General-purpose technical grade.
Solvents and Their Admixtures (Platinum-Cobalt Scale)
D2109 Test Methods for Nonvolatile Matter in Halogenated
4. Properties
Organic Solvents and Their Admixtures
4.1 Reclaimed perchloroethylene, Type I, shall meet the
D2111 Test Methods for Specific Gravity and Density of
requirements of Table 1.
Halogenated Organic Solvents and Their Admixtures
D2942 Test Method for Total Acid Acceptance of Haloge-
4.2 Reclaimed perchloroethylene, Type II, shall meet the
nated Organic Solvents (Nonreflux Methods)
requirements of Table 1.
D2988 Test Methods for Water-Soluble Halide Ion in Halo-
4.3 Reclaimed perchloroethylene, Type III, shall meet the
genated Organic Solvents and Their Admixtures
requirements of Table 1.
D2989 Test Method for Acidity-Alkalinity of Halogenated
Organic Solvents and Their Admixtures
5. Packaging and Package Marking
D3401 Test Methods for Water in Halogenated Organic
5.1 Industrial or commercial quantities shall be packaged
Solvents and Their Admixtures
and labeled in accordance with DOT regulations as found in
49 CFR 100 to 199, in acc
...

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