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ASTM D95-99e1

(Test Method)

Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation

Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation

SCOPE
1.1 This test method covers the determination of water in the range from 0 to 25 % volume in petroleum products, tars, and other bituminous materials by the distillation method.
Note 1—Volatile water-soluble material, if present, may be measured as water.
1.2 The specific products considered during the development of this test method are listed in Table 1. For bituminous emulsions refer to Test Method D 244. For crude oils, refer to Test Method D 4006 (API MPMS Chapter 10.2).
Note 2—With some types of oil, satisfactory results may be obtained from Test Method D 1796 (API MPMS Chapter 10.6).
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 5.

General Information

Status
Historical
Publication Date
09-Jun-1999
ICS
75.140 - Waxes, bituminous materials and other petroleum products
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.02 - Hydrocarbon Measurement for Custody Transfer (Joint ASTM-API)
Current Stage
Ref Project

Relations

Replaces
ASTM D95-99 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
Effective Date
10-Jun-1999
Replaced By
ASTM D95-05 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
Effective Date
01-Jun-2005
Referred By
ASTM D5372-20 - Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids
Effective Date
10-Jun-1999
Referred By
ASTM D2523/D2523M-13(2019)e1 - Standard Practice for Testing Load-Strain Properties of Roofing Membranes
Effective Date
10-Jun-1999
Referred By
ASTM D2028/D2028M-15(2021)e1 - Standard Specification for Cutback Asphalt (Rapid-Curing Type)
Effective Date
10-Jun-1999
Referred By
ASTM D2982-07(2019) - Standard Test Methods for Detecting Glycol-Base Antifreeze in Used Lubricating Oils
Effective Date
10-Jun-1999
Referred By
ASTM D450/D450M-07(2018) - Standard Specification for Coal-Tar Pitch Used in Roofing, Dampproofing, and Waterproofing
Effective Date
10-Jun-1999
Referred By
ASTM D7666-12(2019) - Standard Specification for Triglyceride Burner Fuel
Effective Date
10-Jun-1999
Referred By
ASTM D4072-98(2018) - Standard Test Method for Toluene-Insoluble (TI) Content of Tar and Pitch
Effective Date
10-Jun-1999
Referred By
ASTM D4868-17 - Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
Effective Date
10-Jun-1999
Referred By
ASTM D7832/D7832M-14(2021) - Standard Guide for Performance Attributes of Waterproofing Membranes Applied to Below-Grade Walls / Vertical Surfaces (Enclosing Interior Spaces)
Effective Date
10-Jun-1999
Referred By
ASTM D1208-96(2019) - Standard Test Methods for Common Properties of Certain Pigments
Effective Date
10-Jun-1999
Referred By
ASTM D2318-20 - Standard Test Method for Quinoline-Insoluble (QI) Content of Tar and Pitch
Effective Date
10-Jun-1999
Referred By
ASTM D8125-18(2023) - Standard Specification for Re-Refined Engine Oil Bottoms (REOB)/Vacuum Tower Asphalt Extender (VTAE)
Effective Date
10-Jun-1999
Referred By
ASTM D6373-23 - Standard Specification for Performance-Graded Asphalt Binder
Effective Date
10-Jun-1999

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ASTM D95-99e1 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by DistillationASTM D95-99e1 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
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ASTM D95-99e1 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
AnAmerican National Standard
e1
Designation: D 95 – 99
AmericanAssociation State
Highway Transportation Standard
AASHTO No. T55
Designation: Manual of Petroleum Measurement Standards (MPMS), Chapter 10.5
Designation: 74/82 (88)
Standard Test Method for
Water in Petroleum Products and Bituminous Materials by
1
Distillation
ThisstandardisissuedunderthefixeddesignationD 95;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1
e NOTE—Footnote 1 and the Referenced Documents were corrected editorially to comply with the ASTM-API joint standard
contract in October 2002. Warning notes were editorially moved into the standard text in October 2002.
1. Scope D 1796 TestMethodforWaterandSedimentinFuelOilsby
the Centrifuge Method (Laboratory Procedure) (API
1.1 This test method covers the determination of water in
3
MPMS Chapter 10.6)
the range from 0 to 25 % volume in petroleum products, tars,
D 4006 Test Method for Water in Crude Oil by Distillation
and other bituminous materials by the distillation method.
4
(API MPMS Chapter 10.2)
NOTE 1—Volatile water-soluble material, if present, may be measured
D 4057 Practice for Manual Sampling of Petroleum and
as water.
4
Petroleum Products (API MPMS Chapter 8.1)
1.2 The specific products considered during the develop-
D 4177 Practice for Automatic Sampling of Petroleum and
4
ment of this test method are listed in Table 1. For bituminous
Petroleum Products (API MPMS Chapter 8.2)
emulsions refer to Test Method D 244. For crude oils, refer to
D 5854 Practice for Mixing and Handling of Liquid
Test Method D 4006 (API MPMS Chapter 10.2).
Samples of Petroleum and Petroleum Products (API
5
MPMS Chapter 8.3)
NOTE 2—With some types of oil, satisfactory results may be obtained
E 123 Specification for Apparatus for Determination of
from Test Method D 1796 (API MPMS Chapter 10.6).
6
Water by Distillation
1.3 The values stated in SI units are to be regarded as the
7
2.2 API Standards:
standard. The values in parentheses are for information only.
MPMS Chapter 8.1 Manual Sampling of Petroleum and
1.4 This standard does not purport to address all of the
Petroleum Products (ASTM Practice D 4057)
safety concerns, if any, associated with its use. It is the
MPMS Chapter 8.2 Automatic Sampling of Petroleum and
responsibility of the user of this standard to establish appro-
Petroleum Products (ASTM Practice D 4177)
priate safety and health practices and determine the applica-
MPMSChapter8.3 MixingandHandlingofLiquidSamples
bility of regulatory limitations prior to use. For specific hazard
of Petroleum and Petroleum Products (ASTM Practice
statements, see Section 5.
D 5854)
MPMS Chapter 10.2 Determination of Water in Crude Oil
2. Referenced Documents
by the Distillation Method (ASTM Test Method D 4006)
2.1 ASTM Standards:
MPMSChapter10.6 TestMethodforWaterandSedimentin
2
D 244 Test Methods for Emulsified Asphalts
1
This test method is under the jurisdiction of ASTM Committee D02 on
3
Petroleum Products and Lubricants and theAPI Committee on Petroleum Measure- Annual Book of ASTM Standards, Vol 05.01.
4
ment, and is the direct responsibility of Subcommittee D02.02/COMQ, the joint Annual Book of ASTM Standards, Vol 05.02.
5
ASTM-API Committee on Static Petroleum Measurement. Annual Book of ASTM Standards, Vol 05.03.
6
Current edition approved June 10, 1999. Published August 1999. Originally Annual Book of ASTM Standards, Vol 14.02.
7
published as D 95–21. Last previous edition D 95–83 (1990). Published as Manual of Petroleum Measurement Standards.Available from the
2
Annual Book of ASTM Standards, Vol 04.03. American Petroleum Institute (API), 1220 L St., NW, Washington, DC 20005.
Copyright ©ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA19428-2959, United States.
1

---------------------- Page: 1 ----------------------
e1
D95–99
Fuel Oils by the Centrifuge Method (Laboratory Proce- 5.1.3.2 Iso-octane, of 95% purity or better. (Warning—
dure) (ASTM Test Method D 1796) Extremely flammable. Harmful if inhaled. Vapors may cause
fire.)
3. Summary of Test Method
5.2 Solvent Blank—The water content of the solvent shall
3.1 The material to be tested is heated under reflux with a be determined by distilling an equivalent amount of the same
water-immiscible solvent, which co-distills with the water in solventusedforthetestsampleinthedistillationapparatusand
the sample. Condensed solvent and water are continuously testing as outlined in Section 9. The blank shall be determined
separated in a trap, the water settli
...

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