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ASTM D6352-04e1

(Test Method)

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography

SIGNIFICANCE AND USE
The boiling range distribution of medium and heavy petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining processes (for example, hydrocracking, hydrotreating, visbreaking, or deasphalting). The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.
This test method extends the scope of boiling range determination by gas chromatography to include medium and heavy petroleum distillate fractions beyond the scope of Test Method D 2887 (538°C).
Boiling range distributions obtained by this test method have not been analyzed for correlation to those obtained by low efficiency distillation, such as with Test Method D 86 or D 1160.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum distillate fractions. The test method is applicable to petroleum distillate fractions having an initial boiling point greater than 174°C (345°F) and a final boiling point of less than 700°C (1292°F) (C10 to C90) at atmospheric pressure as measured by this test method.
1.2 The test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight components (for example naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example alcohols, ethers, acids, or esters) or residue are not to be analyzed by this test method. See Test Methods D 3710, D 2887, or D 5307 for possible applicability to analysis of these types of materials.
1.3 The values stated in SI units are to be regarded as standard. The values stated in inch-pound units are for information only and may be included as parenthetical values.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2004
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0H - Chromatographic Distribution Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D6352-04 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
Effective Date
01-Jun-2004
Replaced By
ASTM D6352-04(2009) - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
Effective Date
15-Apr-2009
Referred By
ASTM D7798-20 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates with Final Boiling Points up to 538 °C by Ultra Fast Gas Chromatography (UF GC)
Effective Date
01-Jun-2004
Referred By
ASTM D7213-15(2019) - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 °C to 615 °C by Gas Chromatography
Effective Date
01-Jun-2004
Referred By
ASTM D7398-21 - Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography
Effective Date
01-Jun-2004
Referred By
ASTM D7500-15(2019) - Standard Test Method for Determination of Boiling Range Distribution of Distillates and Lubricating Base Oils—in Boiling Range from 100 °C to 735 °C by Gas Chromatography
Effective Date
01-Jun-2004
Referred By
ASTM D7169-23 - Standard Test Method for Boiling Point Distribution of Samples with Residues Such as Crude Oils and Atmospheric and Vacuum Residues by High Temperature Gas Chromatography
Effective Date
01-Jun-2004
Referred By
ASTM D6417-15(2019) - Standard Test Method for Estimation of Engine Oil Volatility by Capillary Gas Chromatography
Effective Date
01-Jun-2004
Referred By
ASTM F3337-19 - Standard Guide for Taking Property and Behavior Measurements on Weathered Fractions of Oil
Effective Date
01-Jun-2004
Referred By
ASTM D7807-20 - Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection
Effective Date
01-Jun-2004

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ASTM D6352-04e1 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas ChromatographyASTM D6352-04e1 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
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ASTM D6352-04e1 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
e1
Designation: D 6352 – 04
Standard Test Method for
Boiling Range Distribution of Petroleum Distillates in
1
Boiling Range from 174 to 700°C by Gas Chromatography
This standard is issued under the fixed designation D 6352; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1
e NOTE—Variable definitions were added to 10.15.1.3 and 10.15.1.4 editorially in August 2004.
1. Scope* D 1160 Test Method for Distillation of Petroleum Products
at Reduced Pressure
1.1 This test method covers the determination of the boiling
D 2887 Test Method for Boiling Range Distribution of
range distribution of petroleum distillate fractions. The test
Petroleum Fractions by Gas Chromatography
method is applicable to petroleum distillate fractions having an
D 2892 Test Method for Distillation of Crude Petroleum
initial boiling point greater than 174°C (345°F) and a final
(15-Theoretical Plate Column)
boiling point of less than 700°C (1292°F) (C10 to C90) at
D 3710 Test Method for Boiling Range Distribution of
atmospheric pressure as measured by this test method.
Gasoline and Gasoline Fractions by Gas Chromatography
1.2 The test method is not applicable for the analysis of
D 4626 Practice for Calculation of Gas Chromatographic
petroleum or petroleum products containing low molecular
Response Factors
weight components (for example naphthas, reformates, gaso-
D 5307 Test Method for Determination of Boiling Range
lines, crude oils). Materials containing heterogeneous compo-
Distribution of Crude Petroleum by Gas Chromatography
nents (for example alcohols, ethers, acids, or esters) or residue
E 355 Practice for Gas Chromatography Terms and Rela-
are not to be analyzed by this test method. See Test Methods
tionships
D 3710, D 2887, or D 5307 for possible applicability to analy-
E 594 Practice for Testing Flame Ionization Detectors Used
sis of these types of materials.
in Gas or Supercritical Fluid Chromatography
1.3 The values stated in SI units are to be regarded as
E 1510 Practice for Installing Fused Silica Open Tubular
standard. The values stated in inch-pound units are for infor-
Capillary Columns in Gas Chromatographs
mation only and may be included as parenthetical values.
1.4 This standard does not purport to address all of the
3. Terminology
safety concerns, if any, associated with its use. It is the
3.1 Definitions—This test method makes reference to many
responsibility of the user of this standard to establish appro-
common gas chromatographic procedures, terms, and relation-
priate safety and health practices and determine the applica-
ships. For definitions of these terms used in this test method,
bility of regulatory limitations prior to use.
refer to Practices E 355, E 594, and E 1510.
2. Referenced Documents 3.2 Definitions of Terms Specific to This Standard:
2 3.2.1 area slice—the area resulting from the integration of
2.1 ASTM Standards:
the chromatographic detector signal within a specified reten-
D 86 Test Method for Distillation of Petroleum Products at
tiontimeinterval.Inareaslicemode(see6.4.2),peakdetection
Atmospheric Pressure
parameters are bypassed and the detector signal integral is
recorded as area slices of consecutive, fixed duration time
intervals.
1
This test method is under the jurisdiction of ASTM Committee D02 on
3.2.2 corrected area slice—an area slice corrected for base-
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
line offset by subtraction of the exactly corresponding area
D02.04 on Hydrocarbon Analysis.
slice in a previously recorded blank (non-sample) analysis.
CurrenteditionapprovedJune1,2004.PublishedJuly2004.Originallyapproved
in 1998. Last previous edition approved in 2003 as D 6352–03.
3.2.3 cumulative corrected area—the accumulated sum of
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
correctedareaslicesfromthebeginningoftheanalysisthrough
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
a given retention time, ignoring any non-sample area (for
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. example, solvent).
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
e1
D6352–04
3.2.4 final boiling point (FBP)—the temperature (corre- method can be used for product specification testing with the
spondingtotheretentiontime)atwhichacumulativecorrect
...

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5.1 The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining process, This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
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5.1 The bromine number is useful as a measure of aliphatic unsaturation in petroleum samples. When used in conjunction with the calculation procedure described in Annex A2, it can be used to estimate the percentage of olefins in petroleum distillates boiling up to approximately 315 °C (600 °F).  
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SCOPE
1.1 This test method covers the determination of solvent extractables in petroleum waxes.  
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1.3 The values stated in inch-pound units or in SI units and which are not in parentheses are to be regarded as the standard. The values given in parentheses are for information only.  
Note 2: Oil tubes and apparatus used in this test method have traditionally been marked in inches, (the tube is required to be etched with 1/8 in. divisions.) The Saybolt Color Numbers are aligned with inch, 1/2 in., 1/4 in., and 1/8 in. changes in the depth of oil. These fractional inch changes do not readily correspond to SI equivalents and in view of the preponderance of apparatus already in use and marked in inches, the inch/pound unit is regarded as the standard. However the test method does use SI units of length when the length is not directly related to divisions on the oil tube and Saybolt Color Numbers. The test method uses SI units for temperature.  
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Standard Practice for Calculating Viscosity of a Blend of Petroleum Products

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5.1 Predicting the viscosity of a blend of components is a common problem. Both the Wright Blending Method and the ASTM Blending Method, described in this practice, may be used to solve this problem.  
5.2 The inverse problem, predicating the required blend fractions of components to meet a specified viscosity at a given temperature may also be solved using either the Inverse Wright Blending Method or the Inverse ASTM Blending Method.  
5.3 The Wright Blending Methods are generally preferred since they have a firmer basis in theory, and are more accurate. The Wright Blending Methods require component viscosities to be known at two temperatures. The ASTM Blending Methods are mathematically simpler and may be used when viscosities are known at a single temperature.  
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5.5 The calculations described in this practice have been computerized as a spreadsheet and are available as an adjunct.3
SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
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ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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  • Standard
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    English language
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