Standard Test Method for Unrestrained Linear Thermal Shrinkage of Plastic Film<brk/> and Sheeting

SIGNIFICANCE AND USE
4.1 As a result of the manufacturing process, internal stresses may be locked into the film which can be released by heating. The temperature at which shrinkage will occur is related to the processing techniques employed to manufacture the film and may also be related to a phase transition in the base resin. The magnitude of the shrinkage will vary with the temperature of the film.  
4.2 Shrinkage of a particular material produced by a particular process may be characterized by this test method by making measurements at several temperatures through the shrinkage range of the material.  
4.3 Following a characterization in a particular case, it is usually sufficient thereafter to measure shrinkage at only one selected temperature for purposes of process or quality control, or both.
SCOPE
1.1 This test method covers determination of the degree of unrestrained linear thermal shrinkage at given specimen temperatures of plastic film and sheeting of 0.76 mm (0.030 in.) thickness or less. This test method does not cover shrinkage from loss of solvent in some materials.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This standard and ISO 11501 address the same subject matter, but differ in technical content.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Mar-2020
Technical Committee
D20 - Plastics

Relations

Effective Date
01-Apr-2020
Effective Date
01-Feb-2024
Effective Date
01-Nov-2023
Effective Date
01-Apr-2020
Effective Date
01-Jan-2020
Effective Date
01-Aug-2019
Effective Date
15-Apr-2019
Effective Date
01-Feb-2019
Effective Date
01-Dec-2018
Effective Date
01-Nov-2018
Effective Date
15-Aug-2017
Effective Date
01-Mar-2014
Effective Date
15-Nov-2012
Effective Date
15-May-2011
Effective Date
01-May-2011

Overview

ASTM D2732-14(2020): Standard Test Method for Unrestrained Linear Thermal Shrinkage of Plastic Film and Sheeting provides a systematic approach for determining the degree of linear thermal shrinkage of plastic film and sheeting under unrestrained conditions. This standard is essential for manufacturers, quality assurance professionals, and researchers working with plastic materials, as it helps assess the dimensional stability of plastics when exposed to heat during processing, storage, or end use.

By measuring thermal shrinkage in materials up to 0.76 mm (0.030 in.) thick, this standard enables identification of internal stresses introduced during manufacturing, as well as the effects of different processing techniques on the base resin of plastic films and sheeting.

Key Topics

  • Purpose: Evaluates unrestrained linear thermal shrinkage in plastic film and sheeting, focusing on dimensional stability under specified temperature conditions.
  • Applicability: Targets plastic films and sheeting no thicker than 0.76 mm, excluding shrinkage due to solvent loss.
  • Measurement: Determines shrinkage by comparing original and post-heating linear dimensions, expressed as a percentage.
  • Temperature Sensitivity: Allows for shrinkage testing across various temperatures to characterize specific materials and production methods.
  • Quality Control: Once characterized, shrinkage measurements at a single temperature can support ongoing process and quality control.
  • Test Apparatus: Utilizes a constant-temperature liquid bath, precise thermometers, and free shrink holders to ensure accurate, reproducible measurements.

Applications

ASTM D2732-14(2020) is widely applied in industries and research settings where the thermal properties of plastic films and sheeting are critical. Practical uses include:

  • Quality Control: Used by manufacturers to monitor production consistency and ensure plastic films meet dimensional stability requirements during heat exposure.
  • Material Characterization: Assists research and development teams in comparing new resins and processing techniques for films used in packaging, labels, and technical films.
  • Process Optimization: Enables identification of processing parameters that influence internal stresses and shrinkage, supporting improved production efficiency and product performance.
  • Regulatory Compliance: Helps organizations comply with international practices and quality standards in the plastic film and sheeting industry.

This method is relevant for producers of shrink films, food packaging films, industrial sheeting, and any application where film deformation from heat must be controlled or predicted.

Related Standards

Several standards and practices are referenced in or complement ASTM D2732-14(2020):

  • ASTM D618: Practice for Conditioning Plastics for Testing
  • ASTM D883: Terminology Relating to Plastics
  • ASTM D1204: Test Method for Linear Dimensional Changes of Nonrigid Thermoplastic Sheeting or Film at Elevated Temperature
  • ASTM E2251: Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
  • ISO 11501: Determination of Dimensional Change on Heating (similar in scope but differs technically)

Adherence to ASTM D2732-14(2020) supports alignment with international quality and trade requirements, reinforcing product reliability and market acceptance in sectors reliant on plastic film and sheeting.

Relevant keywords: unrestrained linear thermal shrinkage, plastic film, plastic sheeting, ASTM D2732, dimensional stability, quality control, thermal testing, manufacturing standards, plastic materials testing, shrinkage testing.

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Frequently Asked Questions

ASTM D2732-14(2020) is a standard published by ASTM International. Its full title is "Standard Test Method for Unrestrained Linear Thermal Shrinkage of Plastic Film<brk/> and Sheeting". This standard covers: SIGNIFICANCE AND USE 4.1 As a result of the manufacturing process, internal stresses may be locked into the film which can be released by heating. The temperature at which shrinkage will occur is related to the processing techniques employed to manufacture the film and may also be related to a phase transition in the base resin. The magnitude of the shrinkage will vary with the temperature of the film. 4.2 Shrinkage of a particular material produced by a particular process may be characterized by this test method by making measurements at several temperatures through the shrinkage range of the material. 4.3 Following a characterization in a particular case, it is usually sufficient thereafter to measure shrinkage at only one selected temperature for purposes of process or quality control, or both. SCOPE 1.1 This test method covers determination of the degree of unrestrained linear thermal shrinkage at given specimen temperatures of plastic film and sheeting of 0.76 mm (0.030 in.) thickness or less. This test method does not cover shrinkage from loss of solvent in some materials. 1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Note 1: This standard and ISO 11501 address the same subject matter, but differ in technical content. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE 4.1 As a result of the manufacturing process, internal stresses may be locked into the film which can be released by heating. The temperature at which shrinkage will occur is related to the processing techniques employed to manufacture the film and may also be related to a phase transition in the base resin. The magnitude of the shrinkage will vary with the temperature of the film. 4.2 Shrinkage of a particular material produced by a particular process may be characterized by this test method by making measurements at several temperatures through the shrinkage range of the material. 4.3 Following a characterization in a particular case, it is usually sufficient thereafter to measure shrinkage at only one selected temperature for purposes of process or quality control, or both. SCOPE 1.1 This test method covers determination of the degree of unrestrained linear thermal shrinkage at given specimen temperatures of plastic film and sheeting of 0.76 mm (0.030 in.) thickness or less. This test method does not cover shrinkage from loss of solvent in some materials. 1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Note 1: This standard and ISO 11501 address the same subject matter, but differ in technical content. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D2732-14(2020) is classified under the following ICS (International Classification for Standards) categories: 83.140.10 - Films and sheets. The ICS classification helps identify the subject area and facilitates finding related standards.

ASTM D2732-14(2020) has the following relationships with other standards: It is inter standard links to ASTM D2732-14, ASTM D883-24, ASTM D883-23, ASTM D1204-14(2020), ASTM D883-20, ASTM D883-19c, ASTM D883-19a, ASTM D883-19, ASTM D883-18a, ASTM D883-18, ASTM D883-17, ASTM D1204-14, ASTM D883-12e1, ASTM D883-11, ASTM E2251-11. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.

ASTM D2732-14(2020) is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D2732 − 14 (Reapproved 2020)
Standard Test Method for
Unrestrained Linear Thermal Shrinkage of Plastic Film
and Sheeting
This standard is issued under the fixed designation D2732; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope E2251 Specification for Liquid-in-Glass ASTM Thermom-
eters with Low-Hazard Precision Liquids
1.1 This test method covers determination of the degree of
2.2 ISO Standard:
unrestrained linear thermal shrinkage at given specimen tem-
ISO 11501 Determination of Dimensional Change on Heat-
peratures of plastic film and sheeting of 0.76 mm (0.030 in.)
ing
thickness or less. This test method does not cover shrinkage
from loss of solvent in some materials.
3. Terminology
1.2 The values stated in SI units are to be regarded as
3.1 Definitions:
standard. The values given in parentheses are mathematical
3.1.1 unrestrained linear thermal shrinkage (free shrink or
conversions to inch-pound units that are provided for informa-
shrinkage)—the irreversible and rapid reduction in linear
tion only and are not considered standard.
dimension in a specified direction occurring in film subjected
1.3 This standard does not purport to address all of the to elevated temperatures under conditions where nil or negli-
safety concerns, if any, associated with its use. It is the gible restraint to inhibit shrinkage is present. It is normally
responsibility of the user of this standard to establish appro- expressed as a percentage of the original dimension.
priate safety, health, and environmental practices and deter-
4. Significance and Use
mine the applicability of regulatory limitations prior to use.
4.1 As a result of the manufacturing process, internal
NOTE 1—This standard and ISO 11501 address the same subject matter,
stresses may be locked into the film which can be released by
but differ in technical content.
heating. The temperature at which shrinkage will occur is
1.4 This international standard was developed in accor-
related to the processing techniques employed to manufacture
dance with internationally recognized principles on standard-
thefilmandmayalsoberelatedtoaphasetransitioninthebase
ization established in the Decision on Principles for the
resin. The magnitude of the shrinkage will vary with the
Development of International Standards, Guides and Recom-
temperature of the film.
mendations issued by the World Trade Organization Technical
4.2 Shrinkage of a particular material produced by a par-
Barriers to Trade (TBT) Committee.
ticular process may be characterized by this test method by
2. Referenced Documents
making measurements at several temperatures through the
shrinkage range of the material.
2.1 ASTM Standards:
D618 Practice for Conditioning Plastics for Testing
4.3 Following a characterization in a particular case, it is
D883 Terminology Relating to Plastics
usually sufficient thereafter to measure shrinkage at only one
D1204 Test Method for Linear Dimensional Changes of
selected temperature for purposes of process or quality control,
Nonrigid Thermoplastic Sheeting or Film at Elevated
or both.
Temperature
5. Apparatus
This test method is under the jurisdiction ofASTM Committee D20 on Plastics
5.1 Constant-Temperature Liquid Bath, capable of control-
and is the direct responsibility of Subcommittee D20.19 on Film, Sheeting, and
ling accurately to 60.5°C.
Molded Products.
5.1.1 The liquid for the bath should not plasticize or react
Current edition approved April 1, 2020. Published April 2020. Originally
with the specimens. Poly(ethylene glycol), glycerin, and water
approved in 1968. Last previous edition approved in 2014 as D2732 – 14. DOI:
10.1520/D2732-14R20.
have been found to have wide applicability.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
the ASTM website. 4th Floor, New York, NY 10036, http://www.ansi.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D2732 − 14 (2020)
5.2 Thermometer—ASTM Thermometer S5C-11 conform- 6.2 Aminimum of two specimens is necessary for each test
ing to the requirements as prescribed in Specification E2251. temperature.
5.3 Square Metal Stamp, 100 by 100 mm, with engraved
7. Conditioning
arrow indicating machine direction of film and stamp pad and
7.1 Conditioning—Condition the test specimens in accor-
ink. (The ink should not be soluble in the bath liquid.)
dance with Procedure A of Practice D618 unless otherwise
NOTE 2—Ametal die or template (100 by 100 mm) can be used instead
specified by agreement or the relevant ASTM material speci-
of the square metal stamp.
fication.Incasesofdisagreement,thetolerancesshallbe 61°C
5.4 Free Shrink Holder—A holder designed for test of a
(61.8°F) and 65 % relative humidity
single specimen, such as that shown in Fig. 1 and Fig. 2.
7.2 Test Conditions—Set the liq
...

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