D20.19 - Film, Sheeting, and Molded Products

ABSTRACT
This specification covers unpigmented, unsupported, sheet or tubular, medium-density polyethylene films intended for general uses and packaging applications. The film shall be made from homopolymer polyethylene, copolymer polyethylene commonly referred to as low-pressure polyethylene, or blends of homopolymers and copolymers that include ethylene/vinyl-acetate copolymers. The specimens shall be conditioned before testing in the standard laboratory temperature. Tests shall be conducted to determine the physical properties of the specimens which shall conform to the following physical requirements: secant modulus or stiffness; kinetic coefficient of friction; optical properties such as clarity, gloss, and haze; surface treatment level or wetting tension; impact resistance; tensile strength and elongation at break; heat sealability; and odor level.
SCOPE
1.1 This specification covers unpigmented, unsupported, sheet or tubular, medium-density polyethylene films (hereafter referred to as film or films) from resins having densities in the range from 926.0 to 938.0 kg/m3 (0.926 to 0.938 g/cm3), inclusive, as measured on molded plaques.  
1.2 This specification is applicable to homopolymer polyethylene but is not restricted to it.  
1.3 This specification is also applicable to films made from copolymer polyethylene commonly referred to in industry as low-pressure polyethylene.  
1.4 This specification is also applicable to films made from blends of homopolymers and copolymers, including ethylene/vinyl-acetate copolymers.  
1.5 This specification allows for the use of recycled polyethylene film or resin as feedstock, in whole or in part, as long as all the requirements of this specification are met and as long as any specific requirements as governed by the producer and end user are also met (see Note 1).  
Note 1: Guide D7209 contains terminology and definitions relating to recycled plastics.  
1.6 Special care must be exercised if this specification is applied to colored or pigmented films. This specification does not address specific problems associated with coloring, such as, quantity and quality of pigment dispersion, optical properties, and increase in density. These and other areas must be taken into account by mutual agreement between the supplier and the purchaser.  
1.7 The thickness of the films covered by this specification range from 25 to 100 μm (0.001 to 0.004 in.), inclusive. The maximum width of the sheet or lay-flat is 3.05 m (120 in.).  
1.8 This specification does not cover oriented heat-shrinkable films.  
1.9 This specification defines the levels of various physical properties from which specifications for specific films are to be described. The levels of physical properties required by a film for a given application are selected from Section 6 and the corresponding tables. However, Sections 7.2 – 7.5 relating to tolerances shall apply without change to all film falling within the scope indicated by the title and 1.1 – 1.4.  
1.10 This specification covers dimensional tolerances, classification, intrinsic quality requirements, and test methods. The dimensional tolerances include thickness, width, and length or yield. Classification defines types, classes, surfaces, and finishes. The intrinsic quality requirements include density, workmanship, impact strength, tensile strength, heat sealability, and odor, as well as the classification properties for stiffness, coefficient of friction, optical properties, and surface treatment. A sampling method is included.  
1.11 The values stated in SI units are to be regarded as standard. The values in parentheses are given for information only.  
1.12 The following precautionary caveat pertains only to the test methods portion, Section 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate s...

ABSTRACT
This specification covers the classification of polyethylene film and sheeting. Recycled polyethylene film or resin may be used as feedstock, and the film or sheeting may contain additives for surface property improvement, pigments, or stabilizers, or a combination of these, but they must conform to the requirements specified. Material covered in this specification shall be designated by a five-digit type number, with each numeral (from 0 to 5) indicating the cell limit within which the values of the density, impact strength, kinetic coefficient of friction, haze, and nominal thickness of the material falls under. The sheet or film shall be manufactured free, as commercially possible, of gels, streaks, pinholes, particles of foreign matter, and undispersed raw material, and without any other visible defects such as holes, tears, or blisters. The edges of the sheet or film shall be free of nicks and cuts. The surface of the sheet or film may also be treated by flame, corona discharge, or other means to improve the surface properties. Tests to determine the density, impact strength, kinetic coefficient of friction, haze, and nominal thickness of the material shall be performed and shall conform to the requirements specified.
SCOPE
1.1 This specification covers the classification of polyethylene film up to 0.254 mm (0.010 in.) in thickness, inclusive. The film can contain additives for the improvement of the surface properties, pigments, or stabilizers, or combinations thereof.
Note 1: Film is defined in Terminology D883 as an optional term for sheeting having a nominal thickness no greater than 0.254 mm (0.010 in.).  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.3 The following precautionary caveat pertains only to the test method portion, Section 8, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This specification allows for the use of recycled polyethylene film or resin as feedstock, in whole or in part, as long as all the requirements as governed by the producer and end user are also met.
Note 2: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification establishes the dimensional (length and width, thickness, and weight) requirements for biaxially oriented polyethylene terephthalate film and sheeting, both virgin and recycled. For this specification, polyethylene terephthalate film and sheeting shall be defined as the material derived from terephthalic acid and ethylene glycol and shall consist of at least 90 % polyethylene terephthalate homopolymer. The film or sheeting shall be furnished flat or in rolls in the dimensions specified. This specification does not apply to coated, coextruded, tinted, pigmented, or metallized film or sheeting.
SCOPE
1.1 This specification covers requirements for biaxially oriented polyethylene terephthalate film and sheeting in thicknesses from 1.5 μm (0.06 mil) to 355 μm (14.0 mil). For this specification, polyethylene terephthalate film and sheeting shall be defined as the material derived from terephthalic acid and ethylene glycol and shall consist of at least 90 % polyethylene terephthalate homopolymer. This specification does not apply to coated, coextruded, tinted, pigmented, or metallized film or sheeting.  
1.2 Polyethylene terephthalate materials, being thermoplastic, are reprocessable and recyclable.2 This specification allows for the use of those polyethylene terephthalate plastic materials, provided that any specific requirements as governed by the producer and end user are met.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
Note 1: There is no known ISO equivalent to this specification.
Note 2: Film is defined as sheeting having a thickness of ≤250 microns (0.010 in.).  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This practice is intended to assist task groups participating in a round-robin study with the preparation of test sets of film specimens from film samples in the form of rolls on a core.  
4.2 This practice assumes that the essential features of the round-robin protocol have already been established by following the guidance of Practice E691. In particular, it is assumed that the following are known: (1) the number of film samples to be used, (2) the number of participating laboratories, (3) the number of replicate test results to be generated by each laboratory for each sample, and (4) the number of test specimens required to yield one test result for each sample.  
4.3 In accordance with this practice, samples are partitioned into test sets so that real within-sample variability will not unduly distort the conclusions drawn from statistical analyses of the data generated in the round-robin study.
SCOPE
1.1 This practice covers the preparation of test sets of plastic film specimens for subsequent use in an interlaboratory round-robin study to evaluate the precision of a test method.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Column crush tests only provide information about the crush properties of blown thermoplastic containers when employed under conditions approximating those under which the tests are conducted.  
4.2 The column crush properties include the crushing yield load, deflection at crushing yield load, crushing load at failure, and apparent crushing stiffness. Blown thermoplastic containers made from materials that possess a low order of ductility can fail in crushing by brittle fracture. In such cases, the crushing yield load is equivalent to the crushing load at failure. Blown thermoplastic containers made of ductile materials do not always exhibit a crushing load at failure although they will normally provide a crushing yield load value.  
4.3 Column crush tests provide a standard method of obtaining data for research and development, applications, design, quality control, acceptance or rejection under specifications, and special purposes. The tests cannot be considered significant for engineering design in applications differing widely from the load - time scale of the standard test. Such applications require additional tests such as impact, creep, and fatigue.
SCOPE
1.1 This test method covers the determination of mechanical properties of blown thermoplastic containers, whether blown commercially or in the laboratory, loaded under columnar crush conditions at a constant rate of compressive deflection.
Note 1: Although this test method was developed specifically for blow-molded containers, the general procedure can also be applied to containers of suitable geometries produced by other means, for example, thermoforming, injection molding, etc.  
1.2 The values stated in SI units are to be regarded as the standard.  
Note 2: There is no known ISO equivalent to this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 When properly used, these procedures serve to isolate such factors as material, blow-molding conditions, post-treatment, and so forth, on the stress-crack resistance of the container.  
5.2 Environmental stress cracking of blow-molded containers is governed by many factors. Since variance of any of these factors can change the environmental stress-crack resistance of the container, the test results are representative only of a given test performed under defined conditions in the laboratory. The reproducibility of results between laboratories on containers made on more than one machine from more than one mold has not been established.  
5.3 Results can be used for estimating the shelf life of blow-molded containers in terms of their resistance to environmental stress cracking provided this is done against a rigorous background of practical field experience and reproducible test data.
SCOPE
1.1 Under certain conditions of stress, and in the presence of environments such as soaps, wetting agents, oils, or detergents, blow-molded polyethylene containers exhibit mechanical failure by cracking at stresses appreciably below those that would cause cracking in the absence of these environments.  
1.2 This test method measures the environmental stress crack resistance of blow-molded containers, which is the summation of the influence of container design, resin, blow-molding conditions, post treatment, or other factors that can affect this property. Three procedures are provided as follows:  
1.2.1 Procedure A, Stress-Crack Resistance of Containers to Potential Stress-cracking Liquids—This procedure is particularly useful for determining the effect of container design on stress-crack resistance or the stress-crack resistance of a proposed container that contains a liquid product.  
1.2.2 Procedure B, Stress-Crack Resistance of a Specific Container to Polyoxyethylated Nonylphenol (CAS 68412-54-4), a Stress-Cracking Agent—The conditions of test described in this procedure are designed for testing containers made from Class 3 polyethylene Specification D4976. Therefore, this procedure is recommended for containers made from Class 3 polyethylene only. This procedure is particularly useful for determining the effect of resin on the stress-crack resistance of the container.  
1.2.3 Procedure C, Controlled Elevated Pressure Stress-Crack Resistance of a Specific Container to Polyoxyethylated Nonylphenol (CAS 68412-54-4), a Stress-Cracking Agent—The internal pressure is controlled at a constant elevated level.
Note 1: There are environmental concerns regarding the disposal of Polyoxyethylated Nonylphenol (Nonylphenoxy poly(ethyleneoxy) ethanol (CAS 68412-54-4), for example, Igepal CO-630). Users are advised to consult their supplier or local environmental office and follow the guidelines provided for the proper disposal of this chemical.  
1.3 These procedures are not designed to test the propensity for environmental stress cracking in the neck of containers, such as when the neck is subjected to a controlled strain by inserting a plug.  
1.4 The values stated in SI units are to be regarded as standard.  
Note 2: There is no known ISO equivalent to this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8 and Note 1.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers the thread configuration and dimensions for finishes for plastic bottles with screw-type closures. The bottle overflow and body dimensional tolerances are detailed. The test apparatus for determining bottle capacity consists of a balance, pipet, graduated cylinder, beaker, conditioned water, and stop watch. In addition, the test apparatus for determining finish and body dimensions includes micrometers, Vernier height gages or Vernier calipers, internal micrometers or telescoping gages, and commercial scale. The test methods discussed are for the determination of bottle capacity, body dimensions, and finish dimensions.
SCOPE
1.1 This specification covers the thread configuration and dimensions for finishes for plastic bottles with screw-type closures, having a maximum capacity of 18.9 L (5 gal) and a maximum bottle dimension of 305 mm (12 in.). Included are tolerances for bottle capacity and body dimensions.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 The following precautionary caveat pertains only to the test methods portion, Section 8 of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The purpose of this classification system is to provide a method of adequately identifying plastic films using a system that applies universally for plastic films. It further provides a means for specifying these films by the use of a simple line call-out designation.  
4.2 This classification system was developed to permit the addition of additional film products and property values.  
4.3 It is intended that the classification of plastic sheeting, >0.25 mm [0.010 in.] thickness, multi-layer structures, blends, and other variants will be addressed in related standards.
SCOPE
1.1 This standard provides a classification system for tabulating the properties of unfilled, single-layer plastic films.
Note 1: The classification system serves many of the needs of industries using plastic films. The standard is subject to revision as the need requires; therefore, the latest revision should always be used.
Note 2: Film is defined in Terminology D883 as an optional term for sheeting having a nominal thickness no greater than 0.25 mm [0.010 in.].  
1.2 The classification system and subsequent line call-out (specification) is intended to be a means of identifying plastic films used for applications including industrial, packaging, construction, and agriculture. It is not intended for the selection of materials to be used in films. This selection should be made by those having expertise in the plastics field after careful consideration of the end-use requirements, the environment to which the films will be exposed, the fabrication process to be employed, the inherent properties of the material not covered in this document, and the economic factors.  
1.3 This classification system is based on the premise that plastic films can be arranged into broad generic families based on materials with similar composition using basic film properties. A system is thus established which, together with values describing additional requirements, permits as complete a description as desired of the selected film.  
1.4 In all cases where the provisions of this classification system would conflict with the referenced ASTM specification for a particular film product, the latter shall take precedence.
Note 3: It is strongly recommended that this classification system be used for all new applications and specifications and that the specification of films using existing standards be expeditiously withdrawn or converted to this classification system.  
1.5 This classification system applies to commercial products and, as such, there is no control over the manufacturing parameters employed in producing the film. It shall be the responsibility of those developing the specification documents utilizing this classification system to identify the critical parameters and values to be used for the cell classifications and suffix requirements.  
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 4: There is no known ISO equivalent to this standard.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers polyethylene sheeting with a determined thickness intended for construction, industrial and agricultural applications. The sheeting shall be made from polyethylene or modified polyethylene, such as an ethylene copolymer consisting of a major portion of ethylene in combination with a minor portion of some other monomer, or a mixture of polyethylene with a lesser amount of other polymers. General requirements for the material are also observed according to their appearance, dimensions in size and tolerance and minimum net weight. The sheeting may be natural, color-tinted, translucent or opaque. The tests given are intended primarily for use as production tests in conjunction with manufacturing processes and inspection methods to insure conformity of sheeting with the requirements of this specification. These tests shall be done in order to determine the following properties: thickness, length and width, weight, impact resistance, tensile properties, reflectance, luminous transmittance, water vapor transmission, and heat sealability.
SCOPE
1.1 This specification covers polyethylene sheeting, 250 μm (0.010 in. or 10 mils) or less in thickness, intended for construction, industrial, and agricultural applications.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 The following precautionary statement pertains only to the test methods portion, Section 8 of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
Note 1: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Evaluation of the impact toughness of film is important in predicting the performance of a material in applications such as packaging, construction, and other uses. The test simulates the action encountered in applications where moderate-velocity blunt impacts occur in relatively small areas of film.  
5.2 The values obtained by this test method are highly dependent on the method and conditions of film fabrication as well as the type and grade of resin.  
5.3 Test methods employing different missile velocities, impinging surface diameters, or effective specimen diameters will most likely produce different results. Data obtained by this test method cannot necessarily be compared directly with those obtained by other test methods.  
5.4 The impact resistance of a film, while partly dependent on thickness, does not have a simple correlation with sample thickness. Hence, impact values expressed in joules [ft·lbf] normalized over a range of thickness will not necessarily be linear with thickness. Data from this test method are comparable only for specimens that vary by no more than ±15 % from the nominal or average thickness of the specimens tested.  
5.5 The test results obtained by this test method are greatly influenced by the quality of film under test. The influence of variability of data obtained by this procedure will, therefore, depend strongly on the sample quality, uniformity of film thickness, the presence of die marks, contaminants, etc.  
5.6 Several impact test methods are used for film. It is sometimes desirable to know the relationships among test results derived by different test methods. A study was conducted in which four films made from two resins (polypropylene and linear low-density polyethylene), with two film thicknesses for each resin, were impacted using Test Methods D1709 (Test Method A), Test Method D3420 (Procedures A and B), and Test Method D4272. The test results are shown in Appendix X2. Differences in results between Test Methods...
SCOPE
1.1 This test method describes the determination of the total energy impact of plastic films by measuring the kinetic energy lost by a free-falling dart that passes through the film.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm [0.010 in.].
Note 2: This test method and ISO 7765–2 address the same subject matter, but differ in technical content (and results cannot be directly compared between the two test methods). The ISO test method calls for a direct readout of energy by using a load cell as part of the impactor head, while Test Method D4272 calls for a constant weight impactor, then measuring the time of travel through a given distance to get energy values.
FIG. 1 Elements of an Instrumented Dart Drop System
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 These procedures provide a means to assess the drop impact resistance of the group or lot of blown containers from which the test specimens were selected.  
5.2 It is acceptable to use these procedures for routine inspection purposes.  
5.3 These procedures will evaluate the combined effect of construction, materials, and processing conditions on the impact resistance of the blown containers.  
5.4 Before proceeding with this test method, reference the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the materials specification shall take precedence over those mentioned in this test method. If there are no material specifications, then the default conditions apply.
SCOPE
1.1 This test method provides a means to assess the drop impact resistance of water-filled, blow-molded thermoplastic containers, which is a summation of the effects of material, manufacturing conditions, container design, and perhaps other factors.  
1.2 Two procedures are provided as follows:  
1.2.1 Procedure A, Static Drop Height Method—This procedure is particularly useful for quality control since it is quick.  
1.2.2 Procedure B, Bruceton Staircase Method—This procedure is used to determine the mean failure height and the standard deviation of the distribution.  
1.3 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are for information only.  
Note 1: There is no known ISO equivalent to this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is of value in ranking relative tearing resistance of various plastic films and thin sheeting of comparable thickness. Experience has shown the test to have its best reliability on relatively less extensible films and sheeting. Variable elongation and oblique tearing effects on the more extensible films preclude its use as a precise production-control tool for these types of plastics. This test method should be used for specification acceptance testing only after it has been demonstrated that the data for the particular material are acceptably reproducible. This test method should be used for service evaluation only after its usefulness for the particular application has been demonstrated with a number of different films.  
4.2 This test method has been widely used as one index of the tearing resistance of plastic film and thin sheeting used in packaging applications. While it is not always be possible to correlate film tearing data with its other mechanical or toughness properties, the apparatus of this test method provides a controlled means for tearing specimens at straining rates approximating some of those found in actual packaging service.  
4.3 Due to orientation during their manufacture, plastic films and sheeting frequently show marked anisotropy in their resistance to tearing. This is further complicated by the fact that some films elongate greatly during tearing, even at the relatively rapid rates of loading encountered in this test method. The degree of this elongation is dependent in turn on film orientation and the inherent mechanical properties of the polymer from which it is made. These factors make tear resistance of some films reproducible between sets of specimens to ±5 % of the mean value, while others potentially show no better reproducibility than ±50 %.  
4.4 Data obtained by this test method may supplement that from Test Method D1004, wherein the specimen is strained at a rate of 50 mm (2 in.) per minute. However, spec...
SCOPE
1.1 This test method2 covers the determination of the average force to propagate tearing through a specified length of plastic film or nonrigid sheeting after the tear has been started, using an Elmendorf-type tearing tester. Two specimens are cited, a rectangular type, and one with a constant radius testing length. The latter shall be the preferred or referee specimen.  
1.2 Because of (1) difficulties in selecting uniformly identical specimens, (2) the varying degree of orientation in some plastic films, and (3) the difficulty found in testing highly extensible or highly oriented materials, or both, the reproducibility of the test results may be variable and, in some cases, not good or misleading. Provisions are made in the test method to address oblique directional tearing which may be found with some materials.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 13.1.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.).
Note 2: This standard is equivalent to ISO 6383-2.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 When a drop of liquid rests on the surface of a solid, and a gas is in contact with both, the forces acting at the interfaces must balance. These forces can be represented by surface energies acting in the direction of the surfaces and it follows that:
   where:
  θ  =  angle of contact of the edge of the drop with the solid surface,   γGL  =  surface energy of the gas - liquid interface,   γGS  =  surface energy of the gas - solid interface, and   γSL  =  surface energy of the solid - liquid interface.    
5.1.1 The right side of the above equation (the difference between the surface energies of the gas - solid and solid - liquid interfaces) is defined as the wetting tension of the solid surface. It is not a fundamental property of the surface but depends on interaction between the solid and a particular environment.  
5.1.2 When the gas is air saturated with vapors of the liquid, γGL will be the surface tension of the liquid. If the angle of contact is 0° the liquid is said to just wet the surface of the solid, and in this particular case (since cos θ = 1) the wetting tension of the solid will be equal to the surface tension of the liquid.  
5.2 The ability of polyethylene and polypropylene films to retain inks, coatings, adhesives, etc., is primarily dependent upon the character of their surfaces, and can be improved by one of several surface-treating techniques. These same treating techniques have been found to increase the wetting tension of a polyethylene or a polypropylene film surface in contact with mixtures of formamide and ethyl Cellosolve in the presence of air. It is therefore possible to relate the wetting tension of a polyethylene or a polypropylene film surface to its ability to accept and retain inks, coatings, adhesives, etc. The measured wetting tension of a specific film surface can only be related to acceptable ink, coating, or adhesive retention through experience. Wetting tension in itself is not a completely acceptable measur...
SCOPE
1.1 This test method covers the measurement of the wetting tension of a polyethylene or polypropylene film surface in contact with drops of specific test solutions in the presence of air.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
Note 1: This test method and the specified reagents were specifically developed for polyethylene and polypropylene films. It is possible to utilize this test method and the specified reagents for films composed of other polymers, but this can affect the surface energies of the gas-liquid and solid-liquid interfaces, which will affect the contact angle and wetting tension. The applicability and significance for use of non-polyolefin materials must be established by the user.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 9.
Note 2: This test method is equivalent to ISO 8296.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The mechanical performance of welded thermoplastic structures is largely dependent on the quality of the welding operation. It is necessary for fabricators to determine that the proper welding procedures are being followed and that welders maintain their proficiency. Results from this practice are indicative of skill in proper welding procedures for different thermoplastic materials and the use of appropriate welding equipment. If the welded test specimens have short term weld factors that meet or exceed the minimums as set forth in this practice, it can be concluded that, with the same degree of skill and diligence by the welder, acceptable welds can be obtained in fabricated structures.
SCOPE
1.1 This practice covers the preparation and evaluation of joints between two pieces of weldable grades of thermoplastic materials, backed and unbacked, (such as those shown in Table 1) up to 2 in. (50 mm) in thickness.  
1.2 Since there are numerous new technologies and techniques constantly being developed for plastic welding, there are no profiles and procedures that can be considered as standard for all plastics at various thicknesses. This practice is not intended to define profiles and procedures; however, it is intended to establish methods to evaluate minimum short term weld factors to be achieved by the welder for the respective plastics.  
1.3 Weld procedures used for test pieces shall reflect procedures to be used in actual fabrication.  
1.4 Welding methods to be used include machine welding, extrusion welding, and hot gas welding.  
1.5 This practice can be utilized by relevant certification bodies to assess welder proficiency and qualification.  
1.6 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers nonrigid, unsupported vinyl chloride plastic film and sheeting in which the resin portion of the composition contains at least 90 % vinyl chloride. The remaining 10 % may include one or more monomers copolymerized with vinyl chloride, or consist of other resins mechanically blended together with poly(vinyl chloride) or copolymers thereof. The film and sheeting covered herein shall be 0.075 to 0.25 mm (3 to 10 mils) in thickness for film and greater than 0.25 mm in thickness for sheet, and shall include the stabilizers and plasticizers necessary to meet the requirements of this specification. The material may be transparent, translucent, or opaque, and may be plain, printed, embossed, or otherwise surface treated. This specification designates three general-purpose types of vinyl chloride film and sheeting - calendered, extruded, and cast. The materials shall be tested for its tensile strength and elongation at rapture, tear resistance, volatile loss, water extraction, low temperature impact, burning rate, shrinkage, and color fastness to rubbing.
SCOPE
1.1 This specification covers nonrigid, unsupported vinyl chloride plastic film and sheeting in which the resin portion of the composition contains at least 90 % vinyl chloride. The remaining 10 % can include one or more monomers copolymerized with vinyl chloride, or consist of other resins mechanically blended together with poly(vinyl chloride) or copolymers thereof.  
1.2 The vinyl chloride plastic film and sheeting covered herein shall be 0.075 to 0.25 mm (3 to 10 mils) in thickness for film and greater than 0.25 mm in thickness for sheeting. The film and sheeting shall include the stabilizers and plasticizers necessary to meet the requirements of this specification. This specification covers transparent, translucent, or opaque film and sheeting that is plain, printed, embossed, or otherwise surface treated.  
1.3 The values stated in SI units are to be regarded as the standard.  
1.4 The following safety hazards caveat pertains only to the test methods portion, Section 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is intended to be a rapid empirical test to determine the loss of the plasticizer or other extractable components from the plastic film when immersed in liquids commonly used in households.
SCOPE
1.1 This test method for resistance of plastic films to chemicals covers the measurement of the weight loss of film after immersion in chemicals.  
Note 1: There is no known ISO equivalent to this standard.
Note 2: Film is defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.), in accordance with Terminology D883.  
1.2 The values stated in SI units are to be regarded as standard. The values stated in other units are nominal values given for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Test Methods A and B are used to establish the weight of the dart when 50 % of the specimens fail under the conditions specified. Data obtained by one test method cannot be compared directly with the other test method nor with those obtained from tests employing different conditions of missile velocity, impinging surface diameter, effective specimen diameter, material construction and finish of the dart head, and film thickness. The values obtained by these test variables are highly dependent on the method of film fabrication.  
4.2 The results obtained by Test Methods A and B are greatly influenced by the quality of film under test. The confidence limits of data obtained by this procedure can, therefore, vary significantly, depending on the sample quality, uniformity of film gage, die marks, contaminants, etc.  
4.3 Test Methods A and B have been found useful for specification purposes.  
Note 4: With sufficient data, correlation between test results and field performance can usually be established.  
4.4 The impact resistance of plastic film, while partly dependent on thickness, has no simple correlation with sample thickness. Hence, impact values cannot be normalized over a range of thickness without producing misleading data as to the actual impact resistance of the material. Data from these test methods are comparable only for specimens that vary by no more than ±25 % from the nominal or average thickness of the specimens tested.  
4.5 Several impact test methods are used for film. It is sometimes desirable to know the relationships among test results derived by different test methods. A study was conducted in which four films made from two resins (polypropylene and linear low-density polyethylene), with two film thicknesses for each resin, were impacted using Test Methods D1709 (Method A), D3420 (Procedures A and B), and D4272. The test results are shown in the Appendix. Differences in results between Test Methods D1709 and D4272 are not unusual since...
SCOPE
1.1 These test methods cover the determination of the energy that causes plastic film to fail under specified conditions of impact of a free-falling dart. This energy is expressed in terms of the weight (mass) of the missile falling from a specified height which would result in 50 % failure of specimens tested.  
1.2 Two test methods are described:  
1.2.1 Test Method A employs a dart with a 38.10 ± 0.13-mm (1.500 ± 0.005-in.) diameter hemispherical head dropped from a height of 0.66 ± 0.01 m (26.0 ± 0.4 in.). This test method can be used for films whose impact resistances require masses of about 50 g to about 6 kg to fracture them.  
1.2.2 Test Method B employs a dart with a 50.80 ± 0.13-mm (2.000 ± 0.005-in.) diameter hemispherical head dropped from a height of 1.52 ± 0.03 m (60.0 + 0.25, −1.70 in.). Its range of applicability is from about 0.3 kg to about 6 kg.  
1.3 Two testing techniques are described:  
1.3.1 The standard technique is the staircase method. By this technique, the missile weight employed during the test is decreased or increased by uniform increments after the testing of each specimen, depending upon the result (fail or not fail) observed for the specimen.  
1.3.2 The alternative technique provides for testing specimens in successive groups of ten. One missile weight is employed for each group and the missile weight is varied in uniform increments from group to group.  
1.3.3 The staircase technique and the alternative technique give equivalent results both as to the values of impact failure weight which are obtained and as to the precisions with which they are determined.  
1.4 The values stated in SI units are to be regarded as standard. The values stated in parentheses are for information only.
Note 1: Tests on materials that do not break, for any reason, are not considered to be valid. It has been noted that certain materials may stretch so far as to bottom out at the base of certain ...

ABSTRACT
This specification covers uniaxially, biaxially, or balanced oriented polypropylene (OPP) films in a specified thickness range. Films can contain colorants, stabilizers, or other additives, and can be coated for the improvement of performance properties such as heat sealability, gas permeability, and so forth. Films can also be annealed (heat-set) to reduce the unrestrained linear shrinkage and shrink tension on exposure to heat. The base polymer shall be a Group 1 or 2 polypropylene (PP), or a blend of such with one or more other polymers, provided the PP fraction is the main component. Films shall adhere to physical requirements as defined for appearance, blocking, thickness, package yield, width, length, and requirements for those intended for the packaging of food, drugs, and cosmetics. For characterization purposes, this specification provides a cell classification based on six performance parameters characterized by a code designation (1 to 6), as follows: (1) coefficient of friction; (2) unrestrained linear thermal shrinkage; (3) wetting tension; (4) heat-sealability; (5) gloss; (6) haze.
SCOPE
1.1 This specification covers oriented polypropylene (OPP) film in the thickness range from 10 to 75 μm (0.4 to 3.0 mils).  
1.2 The film can contain colorants, stabilizers, or other additives, and can be coated for the improvement of performance properties (heat sealability, gas permeability, and so forth).  
1.3 The film can be annealed (heat-set) to reduce the unrestrained linear shrinkage and shrink tension on exposure to heat.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.5 The following safety hazards caveat pertains only to the test methods portion, Section 7, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Blocking develops in film processing and storage when layers of smooth film are in intimate contact with nearly complete exclusion of air. Temperature, or pressure, or both, can induce or change the degree of adhesion of the surfaces.  
5.2 The procedure of this test method closely simulates the operation of separating film in some end-use applications.
SCOPE
1.1 This test method yields quantitative information regarding the degree of blocking (unwanted adhesion) existing between layers of plastic film. It is not intended to measure susceptibility to blocking.  
1.2 By this procedure, the film-to-film adhesion, expressed as a blocking load in grams, will cause two layers of film with an area of contact of 100 cm2 to separate. The test method is limited to a maximum load of 200 g.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method is similar to ISO 11502 Method B, but is not technically equivalent.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This guide is intended to provide recommendations and suggested good practices to determine precise dimensions when necessary for the calculation of properties expressed in physical units. It is not intended to replace practical thickness measurements based on commercial portable tools, nor is it implied that thickness measurements made by the procedures will agree exactly.
SCOPE
1.1 This guide covers the determination of the thickness of plastic films where the thickness is used directly in determining the results of tests for various properties. Use this practice except as otherwise required in material specifications or in applicable test standards.
Note 1: Film is defined in Terminology D883 as an optional term for sheeting having a nominal thickness no greater than 0.25 mm (0.010 in.).
Note 2: Alternative methods are acceptable if they meet the requirements of measurement precision as noted in this guide.
Note 3: This guide is not intended to address the sampling techniques or the measurement of film thickness for the commercial classification of commercial products or for quality control purposes.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 4: This standard and ISO 4593 address the same subject matter but differ in technical content.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Defects in film are not acceptable to the end-user as there is a reduction in the fitness-for-use in many applications. This document is intended to be a practice to assist users in the inspection, quantification and observation of defects.  
4.2 This practice is applicable in a laboratory environment, continuous inspection as a quality control or as a research tool. It is also appropriate for use in any commercial process used to produce film including extrusion, calendaring, etc.  
4.3 This practice is also suitable for use as an evaluation or screening tool for materials intended to be used in other processes where defects of this nature are critical, such as fiber spinning non-woven, etc.  
4.4 Results achieved by different equipment, even from the same vendor in the same laboratory, are often not directly comparable as a bias exists that cannot be fully addressed through consistent operating conditions. Results frequently shift when analyzer components are upgraded. Additionally, results are often not directly comparable between different product types. All results are to be considered as relative values rather than absolute.  
4.4.1 Therefore, it is not recommended to provide absolute results as part of a sales contract between the buyer and seller. For sales contracts, it is recommended to establish product grade designations based on the historical relationship of the absolute results reported, and fitness-for-use or based on a reference material agreed by both parties. This is attained by the collection of data over a time-period to establish acceptable control limits.  
4.4.2 The defect size range of interest is usually different between resin supplier and converters. Total defect counts are not one to one comparable between small laboratory extrusion lines and commercial extrusion lines. Therefore, an individual correlation is the aim to get accepted results for fitness-for-use.
Note 2: This was tested on Brabender, Collin, Goettfert, and OCS s...
SCOPE
1.1 This practice intends to provide standardized approaches and criteria for the observation and reporting of defects in various types of plastic film, by means of an optical scanning system. Scope includes the in situ inspection of defects in films fabricated for specific applications after preparation of a suitable film from plastic resin.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This test method compares closures for ESCR. Suitable variables are: closure materials, closure designs, processes, applied torque, and stress-crack agents.  
5.2 Results can be used for estimating shelf life of closures in terms of ESCR. This requires that the user has calibrated failure time in this test to failure time in the field for actual packaging systems.
SCOPE
1.1 This test method determines the susceptibility of threaded plastic closures to failure due to environmental stress cracking (ESC).  
1.2 In use, threaded plastic closures can contact agents that appreciably reduce the stress at which cracks form. Examples of such agents are: soaps, detergents, oils, and liquid bleaches.  
1.3 Major factors that influence environmental stress crack resistance (ESCR) of threaded plastic closures include the closure material(s), closure design, molded-in stress, and applied stress.  
1.4 This procedure can be applied to all closures, but is particularly applicable to closures made from plastics based on polypropylene (PP) or polystyrene (PS).  
1.5 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8 and 6.2.
Note 1: There is no known ISO equivalent to this standard.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers flat-bottom, upright, cylindrical tanks molded in one-piece seamless construction by rotational molding. The tanks are molded from polyethylene for above ground, vertical installation and are capable of containing aggressive chemicals at atmospheric pressure. This specification does not cover the design of vessels intended for use at pressures other than atmospheric pressure. Furthermore, this specification does not cover the design of portable tanks and is not for vessels intended for use with liquids heated above their flash points in continuous service. Special design considerations not covered in this specification shall be given to vessels subject to superimposed mechanical forces, such as seismic forces, wind load or agitation; to vessels subject to service above specified temperature; and vessels subject to specified superimposed pressure of water. Low-temperature impact test shall be performed on rotational-molded polyethylene tanks. The test method is used on tanks molded from both the crosslinked and non-crosslinked polyethylenes. Dart drop impact test shall be performed to determine the quality of the tank. O-xylene-insoluble fraction or gel test shall be performed on crosslinked polyethylene. Visual inspection and water test shall also be performed on the samples.
SCOPE
1.1 This specification covers flat-bottom, upright, cylindrical tanks molded in one-piece seamless construction by rotational molding. The tanks are molded from polyethylene for above ground, vertical installation and are capable of containing aggressive chemicals at atmospheric pressure. Included are requirements for materials, properties, design, construction, dimensions, tolerances, workmanship and appearance. Tank capacities are from 1900 L (500 gal) up.  
1.2 This specification covers the design of stationery vessels for use at atmospheric pressure intended for use with liquids heated below their flash points and continuous service temperatures below 66°C (150°F) for Type I tanks and below 60°C (140°F) for Type II tanks.  
1.2.1 NFPA Standards 30 and NFPA 31 shall be consulted for installations that are subject to the requirements of these standards.  
1.3 For service requirements beyond the scope of this specification (1.2), such as externally imposed mechanical forces, internal pressure or vacuum, higher temperature service, etc., other relevant sources of standards, for example, local and state building codes, NFPA, ASME, ARM, etc., shall be consulted.  
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
Note 1: ISO 13341:2005+A1:2011 and ISO 13575:2012 are similar, but not equivalent to this standard.  
1.5 The following precautionary caveat pertains only to the test methods portion, Section 11, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 The puncture-propagation of tear test measures the resistance of a material to snagging, or more precisely, to dynamic puncture and propagation of that puncture resulting in a tear. Failures due to snagging occur in a variety of end uses, including industrial bags, liners, and tarpaulins. The units reported in this test method are Newtons (tear resistance).  
4.2 Experience has shown that for many materials puncture does not contribute significantly to the force value determined, due to the sharpness of the propagating probe used. However, comparing the results of prepunctured test specimens with normal nonpunctured specimens will give an indication of the extent of any puncture resistance in the reported result.  
4.3 For many materials, there may be a specification that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the current ASTM materials standards.
SCOPE
1.1 This test method covers the determination of the dynamic tear resistance of plastic film and thin sheeting subjected to end-use snagging-type hazards.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.).
Note 2: There is no known ISO equivalent to this standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Like other techniques to measure toughness, this test method provides a means to determine parameters of a material at strain rates closer to some end-use applications than provided by low-speed uniaxial tensile tests. Dynamic tensile behavior of a film is important, particularly when the film is used as a packaging material. The same uncertainties about correlations with thickness that apply to other impact tests also apply to this test (see section 3.4 of Test Methods D1709). Hence, no provision for rationalizing to unit thickness is provided. Also, no provision is made for testing at non-ambient temperatures.  
5.2 This test method includes two procedures, similar except with regard to sample size: Procedure A for 60-mm diameter and Procedure B for 89-mm diameter (commonly called the “Spencer”). The data have not been shown relatable to each other.  
5.3 Several impact test methods are used for film. It is sometimes desirable to know the relationships among test results derived by different methods. A study was conducted in which four films made from two resins (polypropylene and linear low-density polyethylene), with two film thicknesses for each resin, were impacted using Test Methods D1709 (Method A), Test Method D3420 (Procedures A and B), and Test Method D4272. The test results are shown in Appendix X1. Differences in results between Test Methods D1709 and D4272 are expected since Test Methods D1709 represents failure initiated energy while Test Method D4272 is initiation plus completion energy. Some films have shown consistency when the initiation energy was the same as the total energy. This statement and the test data also appear in the significance and appendixes sections of Test Methods of D1709 and D4272.
SCOPE
1.1 This test method covers the determination of resistance of film to impact-puncture penetration. Knowledge of how the impact energy is absorbed by the specimen while it is deforming under the impact loading, and the behavior of the specimen after yielding, is not provided by this test. No provision is made for nonambient temperatures in this test method.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.  
Note 1: There is no known ISO equivalent to this standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Tear resistance of plastic film or sheeting is a complex function of its ultimate resistance to rupture. The specimen geometry and speed of testing in this test method are controlled to produce tearing in a small area of stress concentration at rates far below those usually encountered in service. Experience has shown the test to have its best reliability for materials which do not have brittle failure or do not elongate greater than two hundred percent during testing.  
5.2 The data from this test method furnish comparative information for ranking the tearing resistance of plastic specimens of similar composition. Actual use performance in tearing of some plastics may not necessarily correlate with data from this test method.  
5.3 The resistance to tear of plastic film and sheeting, while partly dependent upon thickness, has no simple correlation with specimen thickness. Hence, tearing forces measured in newtons (or pounds-force) cannot be normalized over a wide range of specimen thickness without producing misleading data as to the actual tearing resistance of the material. Data from this test method are comparable only from specimens, which vary by no more than ±10 % from the nominal or average thickness of all specimens tested. Therefore, the tearing resistance is expressed in maximum newtons (or pounds-force) of force to tear the specimen.  
5.4 The tear resistance of plastic film may be a specification that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the ASTM materials standards that currently exist.
SCOPE
1.1 This test method2 covers the determination of the tear resistance of flexible plastic film and sheeting at very low rates of loading, 51 mm (2 in.)/min. and is designed to measure the force to initiate tearing. The specimen geometry of this test method produces a stress concentration in a small area of the specimen. The maximum stress, usually found near the onset of tearing, is recorded as the tear resistance in newtons (or pounds-force). The method is not applicable for film or sheeting material where brittle failures occur during testing or where maximum extension is greater than 101.6 mm (4 in.).  
1.1.1 Although resistance to tear can be expressed in newtons per microns, (pounds-force per mil) of specimen thickness, this is only advisable where correlation for the particular material being tested has been established. In most cases, comparison between films of dissimilar thickness is not valid.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.).  
1.2 Constant-Rate-of-Grip Separation Test—This test method employs a constant rate of separation of the grips holding the test specimen.  
1.2.1 Specimen extension shall be measured in this test method by grip separation.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 2: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 As a result of the manufacturing process, internal stresses may be locked into the film which can be released by heating. The temperature at which shrinkage will occur is related to the processing techniques employed to manufacture the film and may also be related to a phase transition in the base resin. The magnitude of the shrinkage will vary with the temperature of the film.  
4.2 Shrinkage of a particular material produced by a particular process may be characterized by this test method by making measurements at several temperatures through the shrinkage range of the material.  
4.3 Following a characterization in a particular case, it is usually sufficient thereafter to measure shrinkage at only one selected temperature for purposes of process or quality control, or both.
SCOPE
1.1 This test method covers determination of the degree of unrestrained linear thermal shrinkage at given specimen temperatures of plastic film and sheeting of 0.76 mm (0.030 in.) thickness or less. This test method does not cover shrinkage from loss of solvent in some materials.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This standard and ISO 11501 address the same subject matter, but differ in technical content.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is particularly applicable to nonrigid thermoplastic sheeting or film made by the calender or extrusion process. The test gives an indication of lot-to-lot uniformity in regards to the degree of internal strains introduced during processing.  
4.2 The heating medium in this test method is air and does not necessarily yield the same results as Test Method D2732, which uses a liquid medium.  
4.3 Before proceeding with this test method, review the specifications of the material being tested, if available. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the relevant ASTM material specification shall take precedence over those mentioned in this test method. If there are no relevant ASTM material specifications, then the default conditions apply. Table 1 of Classification System D4000 lists the ASTM material standards that currently exist.
SCOPE
1.1 This test method covers the measurement of changes in linear dimensions of nonrigid thermoplastic sheeting or film that result from exposure of the material to specified conditions of elevated temperature and time.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method and ISO 11501 address the same matter, but differ in technical content (and results cannot be directly compared between the two methods).  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is designed to provide load versus deformation response of plastic films under essentially multi-axial deformation conditions at impact velocities. This test method further provides a measure of the rate sensitivity of the plastic films to impact.  
4.2 Multi-axial impact response, while partly dependent on thickness, does not necessarily have a linear correlation with specimen thickness. Therefore, results should be compared only for specimens of essentially the same thickness, unless specific responses versus thickness formulae have been established for the plastic films being tested.  
4.3 For many plastic films, it is possible that a specification exists that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the ASTM materials standards that currently exist.  
4.4 The values obtained by this test method are highly dependent on the method and conditions of film fabrication as well as the type and grade of resin. Results can vary significantly, depending upon sample quality, uniformity of film gage, die marks, contaminants, and so forth.
SCOPE
1.1 This test method covers the determination of puncture properties of plastic films, over a range of test velocities.  
1.1.1 ASTM Terminology Standard D883 has defined film as having a thickness not greater than 0.25 mm. Plastic materials having a thickness above this limit are not to be excluded from use unless shown to be rigid (see 3.2.1). Test Method D3763 is the recommended method for instrumented puncture testing of rigid plastics.  
1.2 Test data obtained by this test method is relevant and appropriate for use in engineering design.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method does not closely conform to ISO 7765-2. The only similarity between the two tests is that they are both instrumented impact tests. The differences in striker, fixture, specimen geometries and in test velocity can produce significantly different test results.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Puncture resistance is very important in end-use performance of stretch wrap film used in consumer and industrial product applications. Puncture resistance is a measure of the energy-absorbing ability of a stretch wrap film in resisting a protrusion. The test method is designed to provide the user with a means of measuring the stretch wrap film's puncture resistance performance under essentially biaxial deformation conditions. A biaxial stress is representative of the type of stress encountered by stretch wrap products in many end-use applications.  
4.2 Although this test method cannot be expected to duplicate all field experiences, since the rate of speed, weight, and configuration of such destructive forces vary widely, a generally reliable comparison of samples may be made from the data obtained.
SCOPE
1.1 This test method determines the resistance of a stretch wrap film to the penetration of a probe at a standard low rate, a single test velocity. Performed at standard conditions, the test method imparts a biaxial stress that is representative of the type of stress encountered in many product end-use applications. The maximum force, force at break, penetration distance, and energy to break are determined.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This test method is of value in rating the tear-propagation resistance of various plastic films and thin sheeting of comparable thickness. For highly extensible film or sheeting the deformation energy of the specimen legs is significantly greater than the tearing energy. The tear-propagation resistance in slightly extensible or non-extensible film or sheeting is distinguished from the tear-propagation resistance in highly extensible film or sheeting by the load-time or load-displacement data, (Fig. 1 and Fig. 2). The tear-propagation force for slightly extensible or non-extensible material is determined from the average tear force versus the initial and peak force for a highly extensible material.
FIG. 1 Load-Time Chart for Low-Extensible Film  
FIG. 2 Load-Time Chart for Highly Extensible Film  
5.2 This test method shall be used for specification acceptance testing only after it has been demonstrated that the data for the particular material are acceptably reproducible.  
5.3 The data obtained by this test method furnish information for ranking the tear-propagation resistance of plastic films and sheeting of similar composition. Actual use performance may not necessarily correlate with data from this test method. Sets of data from specimens of dissimilar thickness are usually not comparable.  
5.4 Before proceeding with this test method, reference should be made to the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the relevant ASTM material specification shall take precedence over those mentioned in this test method. If there are no relevant ASTM material specifications, then the default conditions apply. Table 1 of Classification Systems D4000 lists the ASTM materials standards that currently exist.
SCOPE
1.1 This test method covers the determination of the force necessary to propagate a tear in plastic film and thin sheeting (thickness of 1 mm (0.04 in.) or less) by a single-tear method. The method is not applicable for film or sheeting material where brittle failures occur during testing.  
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.).  
1.2 Constant-Rate-of-Grip Separation Test—This test method employs a constant rate of separation of the grips holding the test specimen.  
1.2.1 Specimen extension may be measured in this test method by grip separation.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 2: This standard is similar to ISO 6383-1, but is not considered technically equivalent. The specimen size for ISO 6383-1 is larger, and the method specifies different test speeds.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 Tensile properties determined by this test method are of value for the identification and characterization of materials for control and specification purposes. Tensile properties can vary with specimen thickness, method of preparation, speed of testing, type of grips used, and manner of measuring extension. Consequently, where precise comparative results are desired, these factors must be carefully controlled. This test method shall be used for referee purposes, unless otherwise indicated in particular material specifications. For many materials, there can be a specification that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 in Classification D4000 lists the ASTM materials standards that currently exist.  
5.2 Tensile properties can be utilized to provide data for research and development and engineering design as well as quality control and specification. However, data from such tests cannot be considered significant for applications differing widely from the force-time scale of the test employed.  
5.3 The tensile modulus of elasticity is an index of the stiffness of thin plastic sheeting. The reproducibility of test results is good when precise control is maintained over all test conditions. When different materials are being compared for stiffness, specimens of identical dimensions must be employed.  
5.4 The tensile energy to break (TEB) is the total energy absorbed per unit volume of the specimen up to the point of rupture. In some texts this property has been referred to as toughness. It is used to evaluate materials that are subjected to heavy abuse or that can stall web transport equipment in the event of a machine malfunction in end-use applications. However, the rate of strain, specimen parameters, and especially flaws can cause large variations in the resul...
SCOPE
1.1 This test method covers the determination of tensile properties of plastics in the form of thin sheeting and films (less than 1.0 mm (0.04 in.) in thickness).  
Note 1: Film is defined in Terminology D883 as an optional term for sheeting having a nominal thickness no greater than 0.25 mm (0.010 in.).
Note 2: Tensile properties of plastics 1.0 mm (0.04 in.) or greater in thickness shall be determined according to Test Method D638.  
1.2 This test method can be used to test all plastics within the thickness range described and the capacity of the machine employed.  
1.3 Specimen extension can be measured by grip separation, extension indicators, or displacement of gage marks.  
1.4 The procedure for determining the tensile modulus of elasticity is included at one strain rate.  
Note 3: The modulus determination is generally based on the use of grip separation as a measure of extension; however, the desirability of using extensometers, as described in 6.2, is recognized and provision for the use of such instrumentation is incorporated in the procedure.  
1.5 Test data obtained by this test method is relevant and appropriate for use in engineering design.  
1.6 The values stated in SI units are to be regarded as the standard. The values in parentheses are provided for information only.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 4: This test method is similar to ISO 527-3, but is not considered technically equivalent. ISO 527-3 allows for additional specimen configurations, specifies different test speeds, and requires an extensometer or gage marks on the specimen.  
1.8 This international standard was developed in accordance with internationally r...

SIGNIFICANCE AND USE
4.1 The purpose of this classification system is to provide a method of adequately identifying polyethylene terephthlate films and sheeting and to provide a means for specifying these films and sheeting by the use of a simple line call-out designation.
SCOPE
1.1 This standard provides a classification system for tabulating the properties for biaxially oriented polyethylene terephthalate film and sheeting in thicknesses from 1.5 μm to 355 μm. For this classification system, polyethylene terephthalate film and sheeting shall be defined as the material derived from terephthalic acid and ethylene glycol and shall consist of at least 90 % polyethylene terephthalate homopolymer with a typical melting temperature range of 225 °C to 250 °C. This specification does not apply to coated, coextruded, tinted, pigmented, or metallized film or sheeting. This classification (in accordance with D8065/D8065M) is intended to eventually replace Specification D5047 (ref. Note 3).
Note 1: Film is defined in Terminology D883 as an optional term for sheeting having a nominal thickness no greater than 250 µm.
Note 2: In order to conform to the original scope of Specification D5047, this classification also includes sheeting up to and including thicknesses of 355 µm.
Note 3: It is strongly recommended that this classification system be used for all new applications and specifications and that the specification of films referencing Specification D5047 be expeditiously withdrawn or converted to this classification system.  
1.2 Polyethylene terephthalate materials, being thermoplastic, are reprocessable and recyclable. This specification allows for the use of those polyethylene terephthalate plastic materials, provided that any specific requirements as governed by the producer and end user are met.  
1.3 In all cases where the provisions of this classification system would conflict with a currently referenced ASTM specification for a particular film product, the latter shall take precedence (see Note 3).  
1.4 This classification system applies to commercial products and, as such, there is no control over the manufacturing parameters employed in producing the film. It shall be the responsibility of those developing the specification documents utilizing this classification system to identify the critical parameters and values to be used for the cell classifications and suffix requirements.  
1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 4: There is no known ISO equivalent to this standard.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 As a result of the manufacturing process, internal stresses are locked into the film and these can be released by heating.
Note 3: For any given type of film or sheeting, the temperatures at which shrinkage will begin are related to processing techniques employed to manufacture the film and also may be related to a phase transition in the base resin.  
5.2 Shrink tension affects the appearance and performance of a film in a shrink-packaging application. It is also used to determine the degree and direction of orientation. The orientation exerts a great influence upon important physical characteristics such as tensile strength, stiffness, tear resistance, and impact strength.  
5.3 Data from Procedure A are most useful for determining the degree and direction of orientation, orientation release stress, and the maximum force that the film can exert at a given temperature.  
5.4 Since, in actual applications, film is seldom, if ever, totally restrained, data from Procedure B are useful in estimating the force an item to be packaged will actually receive and in predicting the appearance of packaged items.  
5.5 The characterization of shrink tension as a function of temperature, and the resultant determination of orientation release stress and its corresponding temperature, is usually carried out only for a particular material of specified thickness for a defined fabrication process. For product development purposes, quality control and determination of conformity be made to the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the relevant ASTM material specification shall take precedence over those mentioned in this test method. If there are no relevant ASTM material specifications, then the default conditions apply. Table 1 of Classification Systems D4000 lists the ASTM material specifications that currently exist.
SCOPE
1.1 This test method covers the determination of the shrink tension and related characteristics, that is, shrink force and orientation release stress, of heat-shrinkable plastic film and sheeting of less than 1.0 mm (0.04 in.) thickness. Two procedures are described that permit the measurement of shrink forces at predetermined temperatures. They are as follows:  
1.1.1 Procedure A is designed to measure the maximum force exerted by a specimen that is totally restrained from shrinking as it is heated rapidly to a specific temperature.  
1.1.2 Procedure B is designed to measure the maximum force exerted by a specimen that is permitted to shrink a predetermined amount prior to restraint while being heated rapidly to a specific temperature.  
1.2 Orientation release stress can be determined from the data obtained using Procedure A.  
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 µm (0.010 in.).
Note 2: There is no known ISO equivalent to this test method.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 Many test methods including Test Methods D882, D2838, F88, F1921/F1921M, and F2029 require the use of narrow strips of varying length. The quality of the sample preparation directly affects test results. This practice describes three techniques for preparing samples with straight, clean, parallel edges with no visible imperfections.  
Note 2: After cutting, each specimen should be examined visually to insure the edges are undamaged (free of nicks). On a periodic basis specimen edge quality should be evaluated by microscopic examination. To determine when cutting blades need to be replaced or sharpened, a control chart of tensile strength and percent elongation at break (see Test Method D882) of a uniform material may be maintained. Tensile strength and percent elongation at break will decrease as the quality of specimen cutting decreases.
SCOPE
1.1 This practice covers equipment and techniques for cutting film and sheeting specimens for testing.2 The specimens are nick-free, non-stretched and can be rapidly prepared.  
1.2 The values given in SI units are to be considered standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 This test method provides precise dimensions necessary for the calculation of properties expressed in physical units.  
5.2 This test method provides a means to characterize the variability of the material thickness in the transverse and machine directions for quality control purposes, production process support and analysis, incoming product inspection and for defining variability for buying/selling film.  
5.3 This test method provides a method for instrument calibration utilizing traceable standards available from the National Institute of Standards and Technology (NIST).  
5.4 It is not intended to replace other thickness measurements based on commercial portable tools, nor is it implied that thickness measurements made by different procedures will exactly agree.
SCOPE
1.1 This test method covers the determination of the thickness of plastic film, ranging in thickness from 2.5 to 250 µm, with a non-contact thickness gauge that uses capacitance-based technology. It includes a method to generate a series of thickness data points that can be used to characterize the variability patterns of film for both transverse or machine direction (profiling).
Note 1: Thicker specimens, typically 250 µm to 2500 µm thick, can utilize this test method if the apparatus is designed to measure and handle materials of this thickness range, and the apparatus complies with the requirements as defined in this standard.  
1.2 This test method provides a method for buyers and sellers of film to communicate the thickness and pattern of thickness variability of the product they are buying/selling.  
1.3 This test method does not apply to textured or porous films or films that are conductive or coated with a conductive substance.
Note 2: Films that contain excessive levels of anti-static additive can be conductive and need to be tested to verify that they do not cause a negative reading on the instrument.  
1.4 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
Note 3: There is no known ISO equivalent to this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 The ability of polymer films to retain inks, coatings, adhesives, etc. is primarily dependent on the character of their surfaces and can be improved by one of several surface-treating techniques. The electrical discharge treatment, such as corona treatment, has been found to increase the wetting tension of a polymer film. The stronger the treatment, the more actively the surface reacts with different polar interfaces. It is therefore possible to relate the contact angle of a polymer film surface to its ability to accept and retain inks, coatings, adhesives, etc., if the ink, coating, or adhesive contains the polar functionalities. Contact angle in itself is not a completely acceptable measure of ink, coating, or adhesive adhesion.  
5.2 The wetting tension of a polymer film belongs to a group of physical parameters for which no standard of accuracy exists. The wetting tension of a polymer cannot be measured directly because solids do not change shape measurably in reaction to surface energy. Many indirect methods have been proposed.5 Different test methods tend to produce different results on identical samples. Practical determination of a solid's surface energy uses this interaction of the solid with test liquids.  
5.3 Although the level of surface treatment of polymer films has been traditionally defined in the industry in terms of dynes/cm (mN/m), these values are derived from a subjective interpretation of the observed test liquid behavior.  
5.4 The following ranges of water contact angle values can be used as a guide for defining the level of surface treatment of polyolefins and many other polymer films with initial low surface energies:    
Marginal or no treatment  
>90°  
Low treatment  
85 to 90°  
Medium treatment  
78 to 84°  
High treatment  
71 to 77°  
Very high treatment  
5.4.1 The suitability of the test for specification acceptance, manufacturing control, and end use of polymer films will have to be established through c...
SCOPE
1.1 This test method covers measurement of the contact angle of water droplets on corona-treated polymer film surfaces.  
Note 1: This standard is identical to ISO 15989.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers the requirements for extruded (cast or blown) and compression-molded sheeting made from low-, medium-, and high-density polyethylenes and copolymers in specified thicknesses. Depending on the functional requirements, sheeting conforming to this specification is used in applications such as chemical tank linings, spacers in electrical equipment, thermoforming into such items as trays, pallets, and shipping containers, and as machine-shop stock. This specification allows for reprocessable and recyclable polyethylene plastic materials, provided that any specific requirements as governed by the producer and end user are met. The three types of polyethylene sheeting covered here are: Type I, natural or colored for general purpose; Type II, natural or colored for dielectrics; and Type III, black for weather-resistant applications. Sampled specimens shall be tested for their conformance with physical requirements as follows: dimension (length, width, diameter, and cores); form; tensile strength at yield and nominal strain at break; shrinkage; warpage and twist; and color, appearance, and workmanship.
SCOPE
1.1 This specification covers requirements for extruded (cast or blown) and compression-molded sheeting made from low-, medium- and high-density polyethylenes and copolymers in thickness of 0.25 mm (0.010 in.) and greater. Depending on the functional requirements, sheeting conforming to this specification is used in applications such as chemical tank linings, spacers in electrical equipment, thermoforming into such items as trays, pallets, and shipping containers, and as machine-shop stock.  
1.2 Polyethylene materials, being thermoplastics, are reprocessable and recyclable (see Guides D5033 and D7209). This specification allows for the use of those polyethylene plastic materials, provided that any specific requirements as governed by the producer and end user are met.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4 The following precautionary caveat pertains only to the test methods portion, Section 11, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
Note 1: There is no known ISO equivalent to this standard.

ABSTRACT
This specification covers unpigmented, unsupported, low-density polyethylene films (hereafter referred to as film or films) for general use and packaging applications. It is applicable to films made from polyethylene copolymers, and also applicable to films made from blends of homopolymers and copolymers, including ethylene/vinylacetate copolymers. The low-density polyethylene film shall be classified by Types 1, 2, and 3; Surfaces 1, 2, and 3; Classes 1, 2, 3, and 4; and Finishes 1, 2, 3, and 4. The film shall be made from an ethylene homopolymer, ethylene copolymers, or blends of homopolymers or copolymers, or homopolymer and copolymer, so that it meets the density and other film requirements specified. Tests shall be performed to conform to the specified properties of the material in accordance with the following test methods: conditioning; test conditions; thickness; yield; flatness; density; coefficient of friction; clarity; haze; wetting tension; impact resistance; tensile properties; heat sealability; and odor.
SCOPE
1.1 This specification covers unpigmented, unsupported, low-density polyethylene and linear low-density polyethylene films (hereafter referred to as film or films) with densities ranging from 0.910-0.925 g/cm3 per Specification D4976.  
Note 1: The density of a film will not necessarily be equal to the density of a molded plaque from the same resin.
Note 2: Blends of ethylene/vinyl acetate (EVA) with low-density polyethylene may have densities up to 0.929 g/cm3.  
1.2 This specification is applicable to homopolymer polyethylene, but is not restricted to it. It is applicable to films made from polyethylene copolymers, and also applicable to films made from blends of homopolymers and copolymers, including ethylene/vinyl acetate copolymers.  
1.3 The thickness of the films covered by this specification is 101.6 μm or less (0.004 in. or less), inclusive. The maximum width of the sheet or layflat is 3.30 m (130 in.).  
1.4 This specification does not cover oriented heat-shrinkable films.  
1.5 This specification allows for the use of recycled polyethylene film or resin as feedstock, in whole or in part, as long as all of the requirements of this specification are met and as long as any specific requirements as governed by the producer and end user are also met. (See Note 3.)  
Note 3: Guide D7209 describes terminology and definitions related to recycled plastics.  
1.6 This specification defines the levels of the various physical properties from which specifications for specific films may be described. The levels of physical properties required by a film for a given application are selected from Section 6. However, Sections 2 – 5 relating to tolerances shall apply without change to all film falling within the scope indicated by the title and 1.1 – 1.4.  
1.7 This specification covers dimensional tolerances, classifications, intrinsic quality requirements, and test methods. The dimensional tolerances include thickness, width, and length or yield. Classification defines types, classes, surfaces, and finishes. The intrinsic quality requirements include density, workmanship, tensile strength, heat sealability, and odor, as well as the classification properties for impact strength, coefficient of friction, optical properties, and surface treatment. A sampling method is included.  
1.8 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.9 The following precautionary caveat pertains only to the test methods portion, Section 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 4: There is no known ISO equivalent to this standard.

ABSTRACT
This specification covers the classification of polyethylene film and sheeting. Recycled polyethylene film or resin may be used as feedstock, and the film or sheeting may contain additives for surface property improvement, pigments, or stabilizers, or a combination of these, but they must conform to the requirements specified. Material covered in this specification shall be designated by a five-digit type number, with each numeral (from 0 to 5) indicating the cell limit within which the values of the density, impact strength, kinetic coefficient of friction, haze, and nominal thickness of the material falls under. The sheet or film shall be manufactured free, as commercially possible, of gels, streaks, pinholes, particles of foreign matter, and undispersed raw material, and without any other visible defects such as holes, tears, or blisters. The edges of the sheet or film shall be free of nicks and cuts. The surface of the sheet or film may also be treated by flame, corona discharge, or other means to improve the surface properties. Tests to determine the density, impact strength, kinetic coefficient of friction, haze, and nominal thickness of the material shall be performed and shall conform to the requirements specified.
SCOPE
1.1 This specification covers the classification of polyethylene film and sheeting up to 0.3 mm (0.012 in.) in thickness, inclusive. The film or sheeting can contain additives for the improvement of the surface properties, pigments, or stabilizers, or combinations thereof.
Note 1: Film is defined in Terminology D883 as an optional term for sheeting having a nominal thickness no greater than 0.254 mm (0.010 in.).  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.3 The following precautionary caveat pertains only to the test method portion, Section 8, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This specification allows for the use of recycled polyethylene film or resin as feedstock, in whole or in part, as long as all the requirements as governed by the producer and end user are also met (see Note 2).  
Note 2: Guide D7209 describes terminology and definitions related to recycled plastics.
Note 3: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is intended to be a rapid empirical test to determine the loss of the plasticizer or other extractable components from the plastic film when immersed in liquids commonly used in households.
SCOPE
1.1 This test method for resistance of plastic films to chemicals covers the measurement of the weight loss of film after immersion in chemicals.  
Note 1: There is no known ISO equivalent to this standard.
Note 2: Film is defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.), in accordance with Terminology D883.  
1.2 The values stated in SI units are to be regarded as standard. The values stated in other units are nominal values given for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Defects in film are not acceptable to the end-user as there is a reduction in the fitness-for-use in many applications. This document is intended to be a practice to assist users in the inspection, quantification and observation of defects.  
4.2 This practice is applicable in a laboratory environment, continuous inspection as a quality control or as a research tool. It is also appropriate for use in any commercial process used to produce film including extrusion, calendaring, etc.  
4.3 This practice is also suitable for use as an evaluation or screening tool for materials intended to be used in other processes where defects of this nature are critical, such as fiber spinning non-woven, etc.  
4.4 Results achieved by different equipment’s even from the same vendor in different laboratories are not directly comparable and may result in a bias that cannot be fully addressed through consistent operating conditions, and results may shift as analyzer components are upgraded for a given analyzer. Additionally, results may not be directly comparable between different product types. All results should be considered as relative values rather than absolute.  
4.4.1 Therefore, it is not recommended to provide absolute results as part of a sales contract between the buyer and seller. For sales contracts, it is recommended to establish product grade designations based on the historical relationship of the absolute results reported, and fitness-for-use or based on a reference material agreed by both parties. This is attained by the collection of data over a time-period to establish acceptable control limits.  
4.4.2 The defect size range of interest is usually different between resin supplier and converters. Total defect counts are not one to one comparable between small laboratory extrusion lines and commercial extrusion lines. Therefore, an individual correlation is the aim to get accepted results for fitness-for-use.
Note 2: This was tested on Brabender, Collin, Go...
SCOPE
1.1 This practice intends to provide standardized approaches and criteria for the observation and reporting of defects in various types of plastic film, by means of an optical scanning system. Scope includes the in situ inspection of defects in films fabricated for specific applications as well as preparation of a suitable film sample to characterize defects within plastic granules followed by inspection of the film sample.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is of value in ranking relative tearing resistance of various plastic films and thin sheeting of comparable thickness. Experience has shown the test to have its best reliability on relatively less extensible films and sheeting. Variable elongation and oblique tearing effects on the more extensible films preclude its use as a precise production-control tool for these types of plastics. This test method should be used for specification acceptance testing only after it has been demonstrated that the data for the particular material are acceptably reproducible. This test method should be used for service evaluation only after its usefulness for the particular application has been demonstrated with a number of different films.  
4.2 This test method has been widely used as one index of the tearing resistance of plastic film and thin sheeting used in packaging applications. While it is not always be possible to correlate film tearing data with its other mechanical or toughness properties, the apparatus of this test method provides a controlled means for tearing specimens at straining rates approximating some of those found in actual packaging service.  
4.3 Due to orientation during their manufacture, plastic films and sheeting frequently show marked anisotropy in their resistance to tearing. This is further complicated by the fact that some films elongate greatly during tearing, even at the relatively rapid rates of loading encountered in this test method. The degree of this elongation is dependent in turn on film orientation and the inherent mechanical properties of the polymer from which it is made. These factors make tear resistance of some films reproducible between sets of specimens to ±5 % of the mean value, while others potentially show no better reproducibility than ±50 %.  
4.4 Data obtained by this test method may supplement that from Test Method D1004, wherein the specimen is strained at a rate of 50 mm (2 in.) per minute. However, spec...
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1.1 This test method2 covers the determination of the average force to propagate tearing through a specified length of plastic film or nonrigid sheeting after the tear has been started, using an Elmendorf-type tearing tester. Two specimens are cited, a rectangular type, and one with a constant radius testing length. The latter shall be the preferred or referee specimen.  
1.2 Because of (1) difficulties in selecting uniformly identical specimens, (2) the varying degree of orientation in some plastic films, and (3) the difficulty found in testing highly extensible or highly oriented materials, or both, the reproducibility of the test results may be variable and, in some cases, not good or misleading. Provisions are made in the test method to address oblique directional tearing which may be found with some materials.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 13.1.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.).
Note 2: This standard is equivalent to ISO 6383-2.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers nonrigid, unsupported vinyl chloride plastic film and sheeting in which the resin portion of the composition contains at least 90 % vinyl chloride. The remaining 10 % may include one or more monomers copolymerized with vinyl chloride, or consist of other resins mechanically blended together with poly(vinyl chloride) or copolymers thereof. The film and sheeting covered herein shall be 0.075 to 0.25 mm (3 to 10 mils) in thickness for film and greater than 0.25 mm in thickness for sheet, and shall include the stabilizers and plasticizers necessary to meet the requirements of this specification. The material may be transparent, translucent, or opaque, and may be plain, printed, embossed, or otherwise surface treated. This specification designates three general-purpose types of vinyl chloride film and sheeting - calendered, extruded, and cast. The materials shall be tested for its tensile strength and elongation at rapture, tear resistance, volatile loss, water extraction, low temperature impact, burning rate, shrinkage, and color fastness to rubbing.
SCOPE
1.1 This specification covers nonrigid, unsupported vinyl chloride plastic film and sheeting in which the resin portion of the composition contains at least 90 % vinyl chloride. The remaining 10 % can include one or more monomers copolymerized with vinyl chloride, or consist of other resins mechanically blended together with poly(vinyl chloride) or copolymers thereof.  
1.2 The vinyl chloride plastic film and sheeting covered herein shall be 0.075 to 0.25 mm (3 to 10 mils) in thickness for film and greater than 0.25 mm in thickness for sheeting. The film and sheeting shall include the stabilizers and plasticizers necessary to meet the requirements of this specification. This specification covers transparent, translucent, or opaque film and sheeting that is plain, printed, embossed, or otherwise surface treated.  
1.3 The values stated in SI units are to be regarded as the standard.  
1.4 The following safety hazards caveat pertains only to the test methods portion, Section 10, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is designed to provide load versus deformation response of plastic films under essentially multi-axial deformation conditions at impact velocities. This test method further provides a measure of the rate sensitivity of the plastic films to impact.  
4.2 Multi-axial impact response, while partly dependent on thickness, does not necessarily have a linear correlation with specimen thickness. Therefore, results should be compared only for specimens of essentially the same thickness, unless specific responses versus thickness formulae have been established for the plastic films being tested.  
4.3 For many plastic films, it is possible that a specification exists that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the ASTM materials standards that currently exist.  
4.4 The values obtained by this test method are highly dependent on the method and conditions of film fabrication as well as the type and grade of resin. Results can vary significantly, depending upon sample quality, uniformity of film gage, die marks, contaminants, and so forth.
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1.1 This test method covers the determination of puncture properties of plastic films, over a range of test velocities.  
1.1.1 ASTM Terminology Standard D883 has defined film as having a thickness not greater than 0.25 mm. Plastic materials having a thickness above this limit are not to be excluded from use unless shown to be rigid (see 3.2.1). Test Method D3763 is the recommended method for instrumented puncture testing of rigid plastics.  
1.2 Test data obtained by this test method is relevant and appropriate for use in engineering design.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method does not closely conform to ISO 7765-2. The only similarity between the two tests is that they are both instrumented impact tests. The differences in striker, fixture, specimen geometries and in test velocity can produce significantly different test results.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method is designed to provide load versus deformation response of plastic films under essentially multi-axial deformation conditions at impact velocities. This test method further provides a measure of the rate sensitivity of the plastic films to impact.  
4.2 Multi-axial impact response, while partly dependent on thickness, does not necessarily have a linear correlation with specimen thickness. Therefore, results should be compared only for specimens of essentially the same thickness, unless specific responses versus thickness formulae have been established for the plastic films being tested.  
4.3 For many plastic films, it is possible that a specification exists that requires the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 of Classification System D4000 lists the ASTM materials standards that currently exist.  
4.4 The values obtained by this test method are highly dependent on the method and conditions of film fabrication as well as the type and grade of resin. Results can vary significantly, depending upon sample quality, uniformity of film gage, die marks, contaminants, and so forth.
SCOPE
1.1 This test method covers the determination of puncture properties of plastic films, over a range of test velocities.  
1.1.1 ASTM Terminology Standard D883 has defined film as having a thickness not greater than 0.25 mm. Plastic materials having a thickness above this limit are not to be excluded from use unless shown to be rigid (see 3.2.1). Test Method D3763 is the recommended method for instrumented puncture testing of rigid plastics.  
1.2 Test data obtained by this test method is relevant and appropriate for use in engineering design.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method does not closely conform to ISO 7765-2. The only similarity between the two tests is that they are both instrumented impact tests. The differences in striker, fixture, specimen geometries and in test velocity can produce significantly different test results.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 As a result of the manufacturing process, internal stresses are locked into the film and these can be released by heating. For any given type of film or sheeting, the temperatures at which shrinkage will begin are related to processing techniques employed to manufacture the film and also may be related to a phase transition in the base resin.  
5.2 Shrink tension affects the appearance and performance of a film in a shrink-packaging application. It may also be used to determine the degree and direction of orientation. The orientation exerts a great influence upon important physical characteristics such as tensile strength, stiffness, tear resistance, and impact strength.  
5.3 Data from Procedure A are most useful for determining the degree and direction of orientation, orientation release stress, and the maximum force that the film can exert at a given temperature.  
5.4 Since, in actual applications, film is seldom, if ever, totally restrained, data from Procedure B are useful in estimating the force an item to be packaged will actually receive and in predicting the appearance of packaged items.  
5.5 The characterization of shrink tension as a function of temperature, and the resultant determination of orientation release stress and its corresponding temperature, is usually carried out only for a particular material of specified thickness for a defined fabrication process. For product development purposes, quality control and determination of conformity to specification limits, the measurement of shrink tension at only one or two specified temperatures is normally sufficient.  
5.6 Before proceeding with this test method, reference shall be made to the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or combination thereof, covered in the relevant ASTM material specification shall take precedence over those mentioned in this test method. If there are no relevant ASTM material spec...
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1.1 This test method covers the determination of the shrink tension and related characteristics, that is, shrink force and orientation release stress, of heat-shrinkable plastic film and sheeting of less than 1.0 mm (0.04 in.) thickness. Two procedures are described that permit the measurement of shrink forces at predetermined temperatures. They are as follows:  
1.1.1 Procedure A is designed to measure the maximum force exerted by a specimen that is totally restrained from shrinking as it is heated rapidly to a specific temperature.  
1.1.2 Procedure B is designed to measure the maximum force exerted by a specimen that is permitted to shrink a predetermined amount prior to restraint while being heated rapidly to a specific temperature.  
1.2 Orientation release stress can be determined from the data obtained using Procedure A.  
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Note 1: Film has been arbitrarily defined as sheeting having nominal thickness not greater than 0.25 mm (0.010 in.).
Note 2: There is no known ISO equivalent to this test method.
WITHDRAWN RATIONALE
This test method covers the determination of the shrink tension and related characteristics, that is, shrink force and orientation release stress, of heat-shrinkable plastic film and sheeting of less than 1.0 mm (0.04 in.) thickness. Two procedures are described that permit the measurement of shrink forces at predetermined temperatures. They are as follows:
Formerly under the jurisdiction of Committee D20 on Plastics, this test method was withdrawn in January 2018 in accordance with...

SIGNIFICANCE AND USE
4.1 When a drop of liquid rests on the surface of a solid, and a gas is in contact with both, the forces acting at the interfaces must balance. These forces can be represented by surface energies acting in the direction of the surfaces and it follows that:
   where:
  θ  =  angle of contact of the edge of the drop with the solid surface,   γGL  =  surface energy of the gas - liquid interface,   γGS  =  surface energy of the gas - solid interface, and   γSL  =  surface energy of the solid - liquid interface.    
4.1.1 The right side of the above equation (the difference between the surface energies of the gas - solid and solid - liquid interfaces) is defined as the wetting tension of the solid surface. It is not a fundamental property of the surface but depends on interaction between the solid and a particular environment.  
4.1.2 When the gas is air saturated with vapors of the liquid, γGL  will be the surface tension of the liquid. If the angle of contact is 0° the liquid is said to just wet the surface of the solid, and in this particular case (since cos θ = 1) the wetting tension of the solid will be equal to the surface tension of the liquid.  
4.2 The ability of polyethylene and polypropylene films to retain inks, coatings, adhesives, etc., is primarily dependent upon the character of their surfaces, and can be improved by one of several surface-treating techniques. These same treating techniques have been found to increase the wetting tension of a polyethylene or a polypropylene film surface in contact with mixtures of formamide and ethyl Cellosolve in the presence of air. It is therefore possible to relate the wetting tension of a polyethylene or a polypropylene film surface to its ability to accept and retain inks, coatings, adhesives, etc. The measured wetting tension of a specific film surface can only be related to acceptable ink, coating, or adhesive retention through experience. Wetting tension in itself is not a completely acceptable measu...
SCOPE
1.1 This test method covers the measurement of the wetting tension of a polyethylene or polypropylene film surface in contact with drops of specific test solutions in the presence of air.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
Note 1: This test method and the specified reagents were specifically developed for polyethylene and polypropylene films. It is possible to utilize this test method and the specified reagents for films composed of other polymers, but this can affect the surface energies of the gas-liquid and solid-liquid interfaces, which will affect the contact angle and wetting tension. The applicability and significance for use of non-polyolefin materials must be established by the user.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 8.
Note 2: This test method is equivalent to ISO 8296.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 When properly used, these procedures serve to isolate such factors as material, blow-molding conditions, post-treatment, and so forth, on the stress-crack resistance of the container.  
5.2 Environmental stress cracking of blow-molded containers is governed by many factors. Since variance of any of these factors can change the environmental stress-crack resistance of the container, the test results are representative only of a given test performed under defined conditions in the laboratory. The reproducibility of results between laboratories on containers made on more than one machine from more than one mold has not been established.  
5.3 Results can be used for estimating the shelf life of blow-molded containers in terms of their resistance to environmental stress cracking provided this is done against a rigorous background of practical field experience and reproducible test data.
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1.1 Under certain conditions of stress, and in the presence of environments such as soaps, wetting agents, oils, or detergents, blow-molded polyethylene containers exhibit mechanical failure by cracking at stresses appreciably below those that would cause cracking in the absence of these environments.  
1.2 This test method measures the environmental stress crack resistance of blow-molded containers, which is the summation of the influence of container design, resin, blow-molding conditions, post treatment, or other factors that can affect this property. Three procedures are provided as follows:  
1.2.1 Procedure A, Stress-Crack Resistance of Containers to Potential Stress-cracking Liquids—This procedure is particularly useful for determining the effect of container design on stress-crack resistance or the stress-crack resistance of a proposed container that contains a liquid product.  
1.2.2 Procedure B, Stress-Crack Resistance of a Specific Container to Polyoxyethylated Nonylphenol (CAS 68412-54-4), a Stress-Cracking Agent—The conditions of test described in this procedure are designed for testing containers made from Class 3 polyethylene Specification D4976. Therefore, this procedure is recommended for containers made from Class 3 polyethylene only. This procedure is particularly useful for determining the effect of resin on the stress-crack resistance of the container.  
1.2.3 Procedure C, Controlled Elevated Pressure Stress-Crack Resistance of a Specific Container to Polyoxyethylated Nonylphenol (CAS 68412-54-4), a Stress-Cracking Agent—The internal pressure is controlled at a constant elevated level.
Note 1: There are environmental concerns regarding the disposal of Polyoxyethylated Nonylphenol (Nonylphenoxy poly(ethyleneoxy) ethanol (CAS 68412-54-4), for example, Igepal CO-630). Users are advised to consult their supplier or local environmental office and follow the guidelines provided for the proper disposal of this chemical.  
1.3 These procedures are not designed to test the propensity for environmental stress cracking in the neck of containers, such as when the neck is subjected to a controlled strain by inserting a plug.  
1.4 The values stated in SI units are to be regarded as standard.  
Note 2: There is no known ISO equivalent to this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8 and Note 1.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification establishes the dimensional (length and width, thickness, and weight) requirements for biaxially oriented polyethylene terephthalate film and sheeting, both virgin and recycled. For this specification, polyethylene terephthalate film and sheeting shall be defined as the material derived from terephthalic acid and ethylene glycol and shall consist of at least 90 % polyethylene terephthalate homopolymer. The film or sheeting shall be furnished flat or in rolls in the dimensions specified. This specification does not apply to coated, coextruded, tinted, pigmented, or metallized film or sheeting.
SCOPE
1.1 This specification covers requirements for biaxially oriented polyethylene terephthalate film and sheeting in thicknesses from 1.5 μm (0.06 mil) to 355 μm (14.0 mil). For this specification, polyethylene terephthalate film and sheeting shall be defined as the material derived from terephthalic acid and ethylene glycol and shall consist of at least 90 % polyethylene terephthalate homopolymer. This specification does not apply to coated, coextruded, tinted, pigmented, or metallized film or sheeting.  
1.2 Polyethylene terephthalate materials, being thermoplastic, are reprocessable and recyclable.2 This specification allows for the use of those polyethylene terephthalate plastic materials, provided that any specific requirements as governed by the producer and end user are met.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
Note 1: There is no known ISO equivalent to this specification.
Note 2: Film is defined as sheeting having a thickness of ≤250 microns (0.010 in.).