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ASTM D5517-96

(Test Method)

Standard Test Method for Determining Extractability of Metals from Art Materials

Standard Test Method for Determining Extractability of Metals from Art Materials

SCOPE
1.1 This test method covers the extraction of metals from art materials using an extractant that simulates the acid potential of gastric juice. This test method is similar to the extraction method noted in Specification F963 but involves conducting extraction steps at body temperature instead of at room temperature. The extraction procedure specified in this test method is more rigorous than that noted in Specification F963.
1.2 This test method is adapted from the European Toy Safety Standard, EN 71-3:1988.
1.3 This test method differs from EN 71-3:1988 in that a solvent extraction step is not required for processing waxes or oil-based products. The rationale for this test method is discussed in Appendix X1.
1.4 This test method does not specify any specific acceptable metal level.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Nov-2000
ICS
97.195 - Items of art and handicrafts. Cultural property and heritage
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.57 - Artist Paints and Related Materials
Current Stage
Ref Project

Relations

Replaced By
ASTM D5517-00 - Standard Test Method for Determining Extractability of Metals from Art Materials
Effective Date
10-Nov-2000

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ASTM D5517-96 - Standard Test Method for Determining Extractability of Metals from Art MaterialsASTM D5517-96 - Standard Test Method for Determining Extractability of Metals from Art Materials
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ASTM D5517-96 - Standard Test Method for Determining Extractability of Metals from Art Materials
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Standards Content (Sample)


NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 5517 – 96
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Test Method for
Determining Extractability of Metals from Art Materials
This standard is issued under the fixed designation D 5517; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope “Soluble” Metal Content Part 1: Determination of Lead
Content—Flame Atomic Absorption Spectrometric
1.1 This test method covers the extraction of metals from art
Method and Dithiazone Spectrophotometric Method
materials using an extractant that simulates the acid potential of
Part 2: Determination of Antimony Content—Flame Atomic
gastric juice. This test method is similar to the extraction
Absorption Spectrophotometric Method and Rhodamine
method noted in Specification F 963 but involves conducting
B Spectrophotometric Method
extraction steps at body temperature instead of at room
Part 3: Determination of Barium Content—Flame Atomic
temperature. The extraction procedure specified in this test
Emission Spectrometric Method
method is more rigorous than that noted in Specification F 963.
Part 4: Determination of Cadmium Content—Flame Atomic
1.2 This test method is adapted from the European Toy
Absorption Spectrometric Method and Polarographic
Safety Standard, EN 71-3:1988.
Method
1.3 This test method differs from EN 71-3:1988 in that a
Part 5: Determination of Hexavalent Chromium Content of
solvent extraction step is not required for processing waxes or
the Pigment Portion of the Liquid Paint or the Paint in
oil-based products. The rationale for this test method is
Powder Form—Diphenylcarbazide Spectrophotometric
discussed in Appendix X1.
Method
1.4 This test method does not specify any specific accept-
Part 6: Determination of Total Chromium Content of the
able metal level.
Liquid Portion of Paint—Flame Atomic Absorption Spec-
1.5 This standard does not purport to address all of the
trometric Method
safety concerns, if any, associated with its use. It is the
2.3 USEPA Standards:
responsibility of the user of this standard to establish appro-
USEPA Test Method SW-846
priate safety and health practices and determine the applica-
6010 Test Method for antimony, arsenic, barium, beryllium,
bility of regulatory limitations prior to use.
cadmium, chromium, cobalt, copper, lead, manganese,
2. Referenced Documents
molybdenum, nickel, selenium, silver, thallium, vana-
dium, and zinc
2.1 ASTM Standards:
6020 Test Method for aluminum, antimony, arsenic, barium,
D 4236 Practice for Labeling Art Materials for Chronic
beryllium, cadmium, chromium, cobalt, copper, lead,
Health Hazards
manganese, nickel, silver, thallium, and zinc
E 180 Practice for Determining the Precision of Data of
7040 Test Method for antimony
ASTM Methods for Analysis and Testing of Industrial
7041 Test Method for antimony
Chemicals
7060 Test Method for arsenic
E 456 Terminology Relating to Quality and Statistics
7061 Test Method for arsenic
F 963 Consumer Safety Specification on Toy Safety
7080 Test Method for barium
2.2 International Standards:
7090 Test Method for beryllium
EN 71-3:1988 Safety of Toys
7091 Test Method for beryllium
ISO 3696 Water for Laboratory Use—Specifications
7130 Test Method for cadmium
ISO 3856 Paints and Varnishes—Determination of
7131 Test Method for cadmium
7190 Test Method for chromium
This test method is under the jurisdiction of ASTM Committee D-1 on Paint 7191 Test Method for chromium
and Related Coatings, Materials, and Applications and is the direct responsibility of
7200 Test Method for cobalt
Subcommittee D01.57 on Artist Paints and Related Materials.
7201 Test Method for cobalt
Current edition approved May 10, 1996. Published July 1996. Originally
7210 Test Method for copper
published as D 5517 – 94. Last previous edition D 5517 – 94.
Annual Book of ASTM Standards, Vol 06.02.
7420 Test Method for lead
Annual Book of ASTM Standards, Vol 15.05.
Annual Book of ASTM Standards, Vol 14.02.
Annual Book of ASTM Standards, Vol 15.07.
6 7
Available from the Comite European de Normalisation, Central Secretariat, Available from USEPA, Office of Solid Waste and Emergency Response,
Rue Brederode 2, B–100 Brussels. Washington, DC 20460.
D 5517
7421 Test Method for lead 1 L with Grade 3 purity water.
7460 Test Method for manganese 7.2 Hydrochloric Acid (0.14 N)—Add 5.10 g concentrated
7470 Test Method for mercury hydrochloric acid (HCl) to Grade 3 purity water and dilute to
7471 Test Method for mercury 1 L with Grade 3 purity water.
7480 Test Method for molybdenum 7.3 Hydrochloric Acid (2.0 N)—Add 72.9 g concentrated
7481 Test Method for molybdenum hydrochloric acid (HCl) to Grade 3 purity water and dilute to
7520 Test Method for nickel 1 L with Grade 3 purity water.
7550 Test Method for osmium 7.4 Hydrochloric Acid (6.0 N)—Add 218.8 g concentrated
7740 Test Method for selenium hydrochloric acid (HCl) to Grade 3 purity water and dilute to
7741 Test Method for selenium 1 L with Grade 3 purity water.
7760 Test Method for silver 7.5 Water, of at least Grade 3 purity in accordance with ISO
7840 Test Method for thallium 3696.
7841 Test Method for thallium
8. Preparation of Test Portions
7870 Test Method for tin
7910 Test Method for vanadium 8.1 A test portion is approximately 100 mg.
7911 Test Method for vanadium 8.2 Art materials that are in the form of a liquid, dust or
7950 Test Method for zinc comminuted solid or are metals are tested without further
preparation.
3. Terminology
8.3 Scraped coatings of art materials are prepared by com-
3.1 Definitions:
minuting the sample sufficiently to pass through a 0.5-mm
3.1.1 For formal definitions of statistical terms see Termi-
sieve.
nology E 456.
8.4 Films, textiles, and paper are prepared by cutting into
3.2 Definitions of Terms Specific to This Standard:
approximately 6 by 6-mm squares.
3.2.1 bioavailability—The extent that a substance can be
8.5 Solids are comminuted, ground or scraped to prepare a
inhaled or absorbed in a biologically active form.
sample sufficient to pass through a 0.5-mm sieve.
3.2.2 detection limit—Three times the standard deviation of
the blank value. 9. Procedure
3.2.3 base material—Material upon which coatings are
9.1 Mix th
...

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5.1 This acid extraction method is intended to indicate the solubility of metals from art materials in a weak acid medium. This test method may be useful as one indicator of the amount of metal that is readily available for absorption. It is not meant as a replacement for in vivo tests of absorption of a metal.6 Other relevant information, when available, should be included in the overall toxicological assessment of metal-containing art materials, such as physico-chemical properties, toxicokinetics (absorption, distribution, metabolism and excretion), and mechanisms of toxicity of the metal(s) of interest.  
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SCOPE
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4.1 This specification establishes quality requirements and provides a basis for common understanding among producers, distributors, and users.  
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SCOPE
1.1 This specification establishes requirements for composition, performance, and labeling of artists' pastels.  
1.2 This specification includes requirements for identification and lightfastness.  
1.3 Pastel specimens are exposed to both natural daylight through window glass and window glass-filtered simulated daylight radiation to determine the lightfastness category for each pastel.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1023-10(2023)(Practice)
Standard Practice for Labeling Ceramic Art Materials for Chronic Adverse Health Hazards

ABSTRACT
This practice describes a procedure for developing precautionary labels for ceramic art materials and provides hazard and precautionary statements concerning chronic adverse health hazards known to be associated with a product or product component(s), when the component(s) is present in a physical form, volume, or concentration that in the opinion of a toxicologist has the potential to produce a chronic adverse health effect(s). Precautionary labels covered by this practice are intended for adult usage and does not assure completely the safe use of an art product. This practice does not specify test methods for determining whether a substance or product presents chronic adverse health hazards and does not apply to products appropriately labeled for known chronic adverse health hazards according to chemical substances labeling standards and practices, such as another national consensus standard, existing labeling statutes, regulations, or guidelines. Requirements for the conformance to this practice are given. Determination of labeling and labeling practices such as, signal word, list of potential chronic hazards, name of chronic hazard components, safe handling, instructions, list of sensitizing components, combined statements, information sources, and supplement information are detailed.
SCOPE
1.1 This practice describes a procedure for developing precautionary labels for ceramic art materials and provides hazard and precautionary statements based upon knowledge that exists in the scientific and medical communities. This practice concerns those chronic adverse health hazards known to be associated with a product or product component(s), when the component(s) is present in a physical form, volume, or concentration that in the opinion of a toxicologist has the potential to produce a chronic adverse health effect(s).  
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1.4 This practice does not specify test methods for determining whether a substance or product presents chronic adverse health hazards.  
1.5 This practice does not apply to products appropriately labeled for known chronic adverse health hazards according to chemical substances labeling standards and practices, such as another national consensus standard, existing labeling statutes, regulations, or guidelines.  
1.6 Since knowledge about chronic adverse health hazards is incomplete and warning cannot cover all uses of any product, it is not possible for precautionary labeling to assure completely safe use of an art product.  
1.7 Manufacturers or repackagers may wish to determine individually or collectively precautionary labeling for ceramic art materials in accordance with this practice. Compliance may be certified by a certifying organization. Guidelines for a certifying organization are given in Appendix X1.  
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.9 This international standard was developed in accordance with international...

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ASTM D4302-14(2021)(Specification)
Standard Specification for Artists’ Oil, Resin-Oil, and Alkyd Paints

ABSTRACT
This specification establishes requirements for composition, physical properties, performance, and labeling of artists' oil, resin-oil, and alkyd paints. This specification covers pigments, vehicles, and additives. Requirements are included for pigment identification, lightfastness, consistency, and drying time. The different labelling requirements for artists' oil paints, resin-oil, and alkyd paints are presented in details. The quality assurance method for artists' oil paints and artists' resin-oil paints are presented in details. The quality assurance methods for artists' alkyd paints are presented. The lightfastness of the paints shall be tested to meet the requirements prescribed. Lightfastness categories shall be assign to meet the requirements prescribed.
SIGNIFICANCE AND USE
4.1 This specification establishes quality requirements and provides a basis for common understanding among producers, distributors, and users.  
4.2 It is not intended that all paints meeting the requirements be identical nor of uniform excellence in all respects. Variations in manufacture, not covered by this specification, may cause some artists to prefer one brand over another, either of which may be acceptable under this specification.
SCOPE
1.1 This specification establishes requirements for composition, physical properties, performance, and labeling of artists’ oil, resin-oil, and alkyd paints.  
1.2 This specification covers pigments, vehicles, and additives. Requirements are included for pigment identification, lightfastness, consistency, and drying time.  
1.3 Table 1 lists some pigments meeting the lightfastness requirements in this specification. In order to identify other pigments that meet these requirements, instructions are given for test specimen preparation. Test methods for determining relative lightfastness are referenced.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.5 This pertains only to the test method found in Section 8. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
    10 pages
    English language
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