ASTM C641-17

Standard Test Method for Iron Staining Materials in Lightweight Concrete Aggregates

SIGNIFICANCE AND USE
4.1 This test method evaluates the potential degree of staining attributable to the presence of iron compounds in a lightweight aggregate sample primarily by means of a visual classification method. Such compounds may or may not produce stains on the surface of the concrete in which the aggregate is incorporated.
SCOPE
1.1 This test method covers the testing of lightweight concrete aggregates to evaluate the potential degree of staining from iron compounds.  
1.2 The values stated in SI units are to be regarded as the standard. The inch-pound values given in parentheses are provided for information only.  
1.3 This standard does not purport to address the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

• Status: Historical
• Publication Date: 14-Jun-2017
• ICS: 91.100.30 - Concrete and concrete products
• Technical Committee: C09 - Concrete and Concrete Aggregates
• Drafting Committee: C09.21 - Lightweight Aggregates and Concrete

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C641 − 17
Standard Test Method for
1
Iron Staining Materials in Lightweight Concrete Aggregates
This standard is issued under the fixed designation C641; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* C702/C702M Practice for Reducing Samples of Aggregate
to Testing Size
1.1 This test method covers the testing of lightweight
D75/D75M Practice for Sampling Aggregates
concrete aggregates to evaluate the potential degree of staining
E11 Specification for Woven Wire Test Sieve Cloth and Test
from iron compounds.
Sieves
1.2 The values stated in SI units are to be regarded as the
E832 Specification for Laboratory Filter Papers
standard. The inch-pound values given in parentheses are
provided for information only.
3. Terminology
1.3 This standard does not purport to address the safety
3.1 Definitions:
problems associated with its use. It is the responsibility of the
3.1.1 For definitions of terms used in this test method, refer
user of this standard to establish appropriate safety and health
to Terminology C125.
practices and determine the applicability of regulatory limita-
tions prior to use.
4. Significance and Use
1.4 This international standard was developed in accor-
4.1 This test method evaluates the potential degree of
dance with internationally recognized principles on standard-
staining attributable to the presence of iron compounds in a
ization established in the Decision on Principles for the
lightweight aggregate sample primarily by means of a visual
Development of International Standards, Guides and Recom-
classification method. Such compounds may or may not
mendations issued by the World Trade Organization Technical
produce stains on the surface of the concrete in which the
Barriers to Trade (TBT) Committee.
aggregate is incorporated.
2. Referenced Documents
5. Apparatus
2
2.1 ASTM Standards:
5.1 Balance—A balance or scale accurate to within 0.1 % of
C125 Terminology Relating to Concrete and Concrete Ag-
the test load at any point within the range of use.
gregates
3
C330/C330M Specification for Lightweight Aggregates for
5.2 Sieves—9.5-mm ( ⁄8-in.) and 600-µm (No. 30) sieves
Structural Concrete
conforming to Specification E11.
C331/C331M Specification for Lightweight Aggregates for
5.3 Filter Paper—shall comply with Specification E832
Concrete Masonry Units
class E2 with a minimum diameter of 240 mm.
5.4 Cheesecloth Wrapping—Two thicknesses, reagent grade
1
This test method is under the jurisdiction of ASTM Committee C09 on
cheesecloth, approximately 457 mm (18 in.) square is sufficient
Concrete and Concrete Aggregatesand is the direct responsibility of Subcommittee
for wrapping each sample.
C09.21 on Lightweight Aggregates and Concrete.
Current edition approved June 15, 2017. Published July 2017. Originally
5.5 Steam Bath—Any suitable apparatus that will meet the
approved in 1969. Last previous edition approved in 2009 as C641 – 09. DOI:
requirement of the test procedure. Water in the steam bath, and
10.1520/C0641-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
makeup water, shall be iron-free water or distilled water.
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on NOTE 1—An oven top glassware sterilizer made of nonferrous materials
the ASTM website. is satisfactory.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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C641 − 17
6. Reagents aggregate and prepare by sieving material to pass the 9.5-mm
3
( ⁄8-in.) sieve and is retained on the 600-µm (No. 30) sieve.
6.1 Purity of Reagents—Reagent grade chemicals shall be
used in all tests. Unless otherwise indicated, it is intended that
8. Procedure
all reagents shall conform to the specifications of the Commit-
8.1 Select two portions each weighing 100 g from the
tee on Analytical Reagents of the American Chemical Society,
aggregate sample prepared for test.
3
where such specifications are available.
8.2 Crimp the edges of two filter papers to form cup-shaped
6.2 Purity of Water—Unless otherwise indicated, references
receptacles approximately 130 mm (5 in.) in diameter and 60
to water shall be understood to mean distilled water or water of
1
mm (2 ⁄2 in.) in depth. Place one of the 100-g portions in each
equal pu
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C641 − 09 C641 − 17
Standard Test Method for
1
Iron Staining Materials in Lightweight Concrete Aggregates
This standard is issued under the fixed designation C641; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope*
1.1 This test method covers the testing of lightweight concrete aggregates to evaluate the potential degree of staining from iron
compounds.
1.2 The values stated in SI units are to be regarded as the standard. The inch-pound values given in parentheses are provided
for information only.
1.3 This standard does not purport to address the safety problems associated with its use. It is the responsibility of the user of
this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior
to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C125 Terminology Relating to Concrete and Concrete Aggregates
C330C330/C330M Specification for Lightweight Aggregates for Structural Concrete
C331C331/C331M Specification for Lightweight Aggregates for Concrete Masonry Units
C702C702/C702M Practice for Reducing Samples of Aggregate to Testing Size
D75D75/D75M Practice for Sampling Aggregates
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E832 Specification for Laboratory Filter Papers
3. Terminology
3.1 Definitions:
3.1.1 For definitions of terms used in this test method, refer to Terminology C125.
4. Significance and Use
4.1 This test method evaluates the potential degree of staining attributable to the presence of iron compounds in a lightweight
aggregate sample primarily by means of a visual classification method. Such compounds may or may not produce stains on the
surface of the concrete in which the aggregate is incorporated.
5. Apparatus
5.1 Balance—A balance or scale accurate to within 0.1 % of the test load at any point within the range of use.
3
5.2 Sieves—9.5-mm ( ⁄8-in.) and 600-μm (No. 30) sieves conforming to Specification E11.
5.3 Filter Paper—shall comply with Specification E832 class E2 with a minimum diameter of 250240 mm.
1
This test method is under the jurisdiction of ASTM Committee C09 on Concrete and Concrete Aggregatesand is the direct responsibility of Subcommittee C09.21 on
Lightweight Aggregates and Concrete.
Current edition approved Oct. 1, 2009June 15, 2017. Published November 2009July 2017. Originally approved in 1969. Last previous edition approved in 20072009 as
C 641 – 07.C641 – 09. DOI: 10.1520/C0641-09.10.1520/C0641-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C641 − 17
5.4 Cheesecloth Wrapping—Two thicknesses, reagent grade cheesecloth, approximately 457 mm (18 in.) square is sufficient for
wrapping each sample.
5.5 Steam Bath—Any suitable apparatus that will meet the requirement of the test procedure. Water in the steam bath, and
makeup water, shall be iron-free water or distilled water.
NOTE 1—An oven top glassware sterilizer made of nonferrous materials is satisfactory.
6. Reagents
6.1 Purity of Reagents—Reagent grade chemicals shall be used in all tests. Unless otherwise indicated, it is intended that all
reagents shall conform to the specifications of the Committee on Analytical Reagents of the American Chemical Society, where
3
such specifications are available.
6.2 Purity of Water—Unless otherwise indicated, references to water shall be understood to mean distilled water or water of
equal purity.
6.3 Concentration of Reagents:
6.3.1 Concentrated Acid and Ammonium
...