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ASTM D2694-05(2019)

(Specification)

Standard Specification for Diethylene Glycol,

Standard Specification for Diethylene Glycol<sup>,</sup>

ABSTRACT
This specification covers diethylene glycol for use in the preparation of surface coatings. Diethylene glycol shall be tested for apparent specific gravity, color, distillation range, water content, acidity, ethylene glycol content, triethylene glycol content, and iron content, and shall conform to the requirements of the specification.
SCOPE
1.1 This specification covers diethylene glycol for use in the preparation of surface coatings.  
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit of Practice E29.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 For specific hazard information and guidance, consult the supplier's Material Safety Data Sheet.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Mar-2019
ICS
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.35 - Solvents, Plasticizers, and Chemical Intermediates
Current Stage
Ref Project

Relations

Replaces
ASTM D2694-05(2011) - Standard Specification for Diethylene Glycol
Effective Date
01-Apr-2019
Refers
ASTM E202-12 - Standard Test Methods for Analysis of Ethylene Glycols and Propylene Glycols
Effective Date
01-Apr-2012
Refers
ASTM D5386-10 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
01-Jan-2010
Refers
ASTM E29-08 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-Oct-2008
Refers
ASTM E29-06b - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
15-Nov-2006
Refers
ASTM E29-06a - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
15-Sep-2006
Refers
ASTM E29-06 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-May-2006
Refers
ASTM D5386-05 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
15-Oct-2005
Refers
ASTM D1209-05e1 - Standard Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
Effective Date
15-May-2005
Refers
ASTM D1209-05 - Standard Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
Effective Date
15-May-2005
Refers
ASTM E29-04 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-Dec-2004
Refers
ASTM D5386-04 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
01-Jan-2004
Refers
ASTM E29-02e1 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
10-May-2002
Refers
ASTM D1209-00 - Standard Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
Effective Date
10-May-2000
Refers
ASTM D5386-93b(2000)e1 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
10-Feb-2000

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ASTM D2694-05(2019) - Standard Specification for Diethylene Glycol<sup>,</sup>ASTM D2694-05(2019) - Standard Specification for Diethylene Glycol<sup>,</sup>
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ASTM D2694-05(2019) - Standard Specification for Diethylene Glycol<sup>,</sup>
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Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D2694 −05 (Reapproved 2019)
Standard Specification for
1,2
Diethylene Glycol
This standard is issued under the fixed designation D2694; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D5386 Test Method for Color of Liquids Using Tristimulus
Colorimetry
1.1 This specification covers diethylene glycol for use in the
E29 Practice for Using Significant Digits in Test Data to
preparation of surface coatings.
Determine Conformance with Specifications
1.2 The following applies to all specified limits in this
E202 Test Methods for Analysis of Ethylene Glycols and
standard: for purposes of determining conformance with this
Propylene Glycols
standard, an observed value or a calculated value shall be
E300 Practice for Sampling Industrial Chemicals
rounded off “to the nearest unit” in the last right-hand digit
2.2 U.S. Federal Specification:
used in expressing the specification limit of Practice E29.
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging
1.3 The values stated in SI units are to be regarded as
of
standard. No other units of measurement are included in this
standard.
3. Properties
1.4 For specific hazard information and guidance, consult
3.1 Diethylene glycol shall conform to the following re-
the supplier’s Material Safety Data Sheet.
quirements:
1.5 This standard does not purport to address all of the Apparent specific gravity
20/20 °C 1.1170 to 1.1200
safety concerns, if any, associated with its use. It is the
or
responsibility of the user of this standard to establish appro-
25/25 °C 1.1147 to 1.1177
A
priate safety, health, and environmental practices and deter-
Color, Pt-Co units, max 15
Distillation range, 760 mm Hg
mine the applicability of regulatory limitations prior to use.
Initial boiling point, °C, min 240
1.6 This international standard was developed in accor-
Dry point, °C, max 250
dance with internationally recognized principles on standard- Water, wt %, max 0.2
Acidity as acetic acid, wt %, max 0.01
ization established in the Decision on Principles for the
Ethylene glycol, wt %, max 0.5
Development of International Standards, Guides and Recom-
Triethylene glycol, wt %, max 1.0
mendations issued by the World Trade Organization Technical Iron, ppm, max 1.0
Barriers to Trade (TBT) Committee.
A
Instrumental Pt-Co color determined by Test Method D5386 has been shown to
have no statistically significant difference from Pt-Co color determined by Test
2. Referenced Documents
Method D1209. However, it is not known whether diethylene glycol was part of the
3 sample set included in the interlaboratory study.
2.1 ASTM Standards:
D1209 Test Method for Color of Clear Liquids (Platinum-
4. Sampling
Cobalt Scale)
4.1 The mate
...

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1.1 This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).
Note 1: Water-borne paints are internally standardized and diluted with water followed by addition of solid sodium chloride.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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