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ASTM D977-13e1

(Specification)

Standard Specification for Emulsified Asphalt

Standard Specification for Emulsified Asphalt

ABSTRACT
This specification covers the requirements for thirteen grades of emulsified asphalt for use in pavement construction in the manner designated. The emulsified asphalts shall be homogeneous after thorough mixing and shall be tested within 14 days of delivery. Asphalts separated by freezing shall no longer be tested. Materials shall be appropriately sampled and tested, and shall conform accordingly to the following physical requirements: viscosity; storage stability; demulsibility; coating ability and water resistance; cement mixing; residue by distillation; oil distillate; ductility; solubility in trichloroethylene; and behavior during sieve, penetration, and float tests.
SCOPE
1.1 This specification covers thirteen grades of emulsified asphalt for use in pavement construction in the manner designated.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

General Information

Status
Historical
Publication Date
31-May-2013
ICS
91.100.50 - Binders. Sealing materials
93.080.20 - Road construction materials
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.41 - Emulsified Asphalt Specifications
Current Stage
Ref Project

Relations

Replaces
ASTM D977-13 - Standard Specification for Emulsified Asphalt
Effective Date
01-Jun-2013
Replaced By
ASTM D977-17 - Standard Specification for Emulsified Asphalt
Effective Date
01-Jun-2017
Referred By
ASTM D244-09(2017) - Standard Test Methods and Practices for Emulsified Asphalts
Effective Date
01-Jun-2013
Referred By
ASTM D7497-21 - Standard Practice for Recovering Residue from Emulsified Asphalt Using Low-Temperature Evaporative Technique
Effective Date
01-Jun-2013
Referred By
ASTM D4215-21 - Standard Specification for Cold-Mixed, Cold-Laid Asphalt Paving Mixtures
Effective Date
01-Jun-2013
Referred By
ASTM D3910-21 - Standard Practices for Design, Testing, and Construction of Slurry Seal
Effective Date
01-Jun-2013
Referred By
ASTM D7404-19 - Standard Test Method for Determination of Emulsified Asphalt Residue by Moisture Balance Analyzer
Effective Date
01-Jun-2013
Referred By
ASTM D1369-19 - Standard Practice for Quantities of Materials for Asphalt-Aggregate Surface Treatments
Effective Date
01-Jun-2013
Referred By
ASTM D4223/D4223M-20 - Standard Practices for Preparation of Test Specimens of Asphalt-Stabilized Soils
Effective Date
01-Jun-2013
Referred By
ASTM D4057-22 - Standard Practice for Manual Sampling of Petroleum and Petroleum Products
Effective Date
01-Jun-2013
Referred By
ASTM D7196-23 - Standard Test Method for Raveling Test of Cold-Mixed Emulsified Asphalt Samples
Effective Date
01-Jun-2013
Referred By
ASTM D7226-13(2023) - Standard Test Method for Determining the Viscosity of Emulsified Asphalts Using a Rotational Paddle Viscometer
Effective Date
01-Jun-2013
Referred By
ASTM D3628-15(2021) - Standard Practice for Selection and Use of Emulsified Asphalts
Effective Date
01-Jun-2013
Referred By
ASTM D7496-18 - Standard Test Method for Viscosity of Emulsified Asphalt by Saybolt Furol Viscometer
Effective Date
01-Jun-2013
Referred By
ASTM D5360-15 - Standard Practice for Design and Construction of Bituminous Surface Treatments
Effective Date
01-Jun-2013

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ASTM D977-13e1 - Standard Specification for Emulsified AsphaltASTM D977-13e1 - Standard Specification for Emulsified Asphalt
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ASTM D977-13e1 - Standard Specification for Emulsified Asphalt
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation:D977 −13
Standard Specification for
1
Emulsified Asphalt
This standard is issued under the fixed designation D977; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1
ε NOTE—Editorially corrected 5.1.1 in January 2014.
1. Scope D7496 Test Method for Viscosity of Emulsified Asphalt by
Saybolt Furol Viscometer
1.1 This specification covers thirteen grades of emulsified
D7553 Test Method for Solubility of Asphalt Materials in
asphalt for use in pavement construction in the manner
N-Propyl Bromide
designated.
1.2 The values stated in SI units are to be regarded as
3. Requirements
standard. No other units of measurement are included in this
3.1 The emulsified asphalt shall be tested within 14 days of
standard.
delivery. The emulsified asphalt shall be homogeneous after
thorough mixing provided separation has not been caused by
2. Referenced Documents
freezing. Emulsified asphalts separated by freezing shall not be
2
2.1 ASTM Standards:
tested.
D5 Test Method for Penetration of Bituminous Materials
3.2 Emulsified asphalt shall conform to the requirements
D113 Test Method for Ductility of Bituminous Materials
prescribed in Table 1 or Table 2. If no table is specified, default
D139 Test Method for Float Test for Bituminous Materials
is Table 1.
D140 Practice for Sampling Bituminous Materials
D244 Test Methods and Practices for Emulsified Asphalts
4. Sampling
D2042 Test Method for Solubility of Asphalt Materials in
4.1 Samples of emulsified asphalt shall be taken in accor-
Trichloroethylene
dance with Practice D140.
D3910 Practices for Design, Testing, and Construction of
Slurry Seal
4.2 Samples shall be stored in clean, airtight sealed contain-
D6930 Test Method for Settlement and Storage Stability of ers as specified in Practice D140 at a temperature of not less
Emulsified Asphalts
than 4°C until tested.
D6933 Test Method for Oversized Particles in Emulsified
5. Test Methods
Asphalts (Sieve Test)
D6935 Test Method for Determining Cement Mixing of
5.1 The properties of the emulsified asphalts given in Table
Emulsified Asphalt
1 or Table 2 shall be determined in accordance with the
D6936 Test Method for Determining Demulsibility of Emul-
following ASTM test methods:
sified Asphalt
5.1.1 Viscosity—Test Method D7496 for Table 1 or Test
D6997 Test Method for Distillation of Emulsified Asphalt
Method D7226 for Table 2.
D7226 Test Method for Determining the Viscosity of Emul-
5.1.2 Storage Stability—Test Method D6930.
sified Asphalts Using a Rotational Paddle Viscometer
5.1.3 Demulsibility—Test Method D6936.
5.1.4 Coating Ability and Water Resistance—Test Methods
D244.
1
This specification is under the jurisdiction of ASTM Committee D04 on Road
5.1.5 Cement Mixing—Test Method D6935.
and Paving Materials and is the direct responsibility of Subcommittee D04.41 on
5.1.6 Sieve Test—Test Method D6933.
Emulsified Asphalt Specifications.
5.1.7 Distillation—Test Method D6997.
CurrenteditionapprovedJune1,2013.PublishedJuly2013.Originallyapproved
5.1.8 Tests on Residue from Distillation—Test Methods
in 1948. Last previous edition approved in 2012 as D977-12b. DOI: 10.1520/
D0977-13E01.
D244.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
5.1.8.1 Penetration—Test Method D5
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
5.1.8.2 Ductility—Test Method D113
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. 5.1.8.3 Solubility—Test Method D2042 or D7553
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
´1
D977−13
2
TABLE 1 Requirements for Emulsified Asphalt
NOTE 1—QS-1h emulsified asphalt shall meet the requirements outlined in Practice D3910 .
NOTE 2—QS-1h is used for Quick Set Slurry Seal systems.
Rapid-Setting Medium-Setting
Type RS-1 RS-2 HFRS-2 MS-1 MS-2 MS-2h
Grade min max min max min max min max min max min max
Tests on emulsions:
Viscosity, Saybolt Furol at 25°C SFS 20 100 . . . . 20 100 100 . 100 .
Viscosity, Saybolt Furol at 50°C SFS . . 75 400 75 400 . . . . . .
A
Storage stability test, 24-h, % . 1 . 1 . 1 . 1 . 1 . 1
Demulsibility, 35 ml, 0.02 N CaCl , % 60 . 60 . 60 . . . . . . .
2
Coating ability and water resistance:
Coating, dry aggregate . . . good good good
Coating, after spraying . . . fair fair fair
Coating, wet aggregate . . . fair fa
...

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5.1 Values of density are used for converting volumes to units of mass and for correcting measured volumes at the measured temperature to a standard temperature using Practice D4311/D4311M.
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1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table notes, 11.1) in the range from 6 to 100 000 mm2/s [cSt].  
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.  
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1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
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ASTM D1461-17(2022)(Test Method)
Standard Test Method for Moisture or Volatile Distillates in Asphalt Mixtures

SIGNIFICANCE AND USE
3.1 This test method is used for determining either the amount of moisture or the amount of volatile petroleum distillates in asphalt mixtures.  
3.2 Applicable standards are those in which measurements or calibrations are made, samples are procured, or products are selected.3
SCOPE
1.1 This test method covers the determination, by direct measurement, of moisture or volatile fractions of the asphalt in asphalt mixtures.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D3289-17(2022)(Test Method)
Standard Test Method for Density of Semi-Solid and Solid Asphalt Materials (Nickel Crucible Method)

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5.1 Values of density are used for converting volumes to units of mass, and for correcting measured volumes from the temperature of measurement to a standard temperature using Practice D4311/D4311M.
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1.1 This test method covers the determination of the density of semi-solid and solid asphalt materials by weighing in air and in water.
Note 1: An alternate method for determining the density of semi-solid and solid asphalt materials is Test Method D70/D70M. For materials which are too fluid for use of this method, use Test Method D3142/D3142M.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 Warning— Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury or its vapor may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website—www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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