Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2018)

This document specifies general requirements for sampling, preservation, handling, transport and storage of all water samples including those for biological analyses.
It is not applicable to water samples intended for microbiological analyses as specified in ISO 19458, ecotoxicological assays, biological assays and passive sampling as specified in the scope of ISO 5667‑23.
This document is particularly appropriate when spot or composite samples cannot be analysed on site and have to be transported to a laboratory for analysis.

Wasserbeschaffenheit - Probenahme - Teil 3: Konservierung und Handhabung von Wasserproben (ISO 5667-3:2018)

Dieses Dokument legt allgemeine Anforderungen für die Probenahme, Konservierung, Handhabung, den Transport und die Lagerung aller Wasserproben einschließlich derer für biologische Untersuchungen fest.
Es ist nicht anwendbar für Wasserproben zur mikrobiologischen Untersuchung nach ISO 19458, für ökotoxikologische Tests, für biologische Tests sowie zur passiven Probenahme nach ISO 5667 23.
Dieses Dokument ist besonders für jene Proben (Einzel  oder Mischproben) geeignet, die nicht unmittelbar vor Ort untersucht werden können und hierfür in das Labor gebracht werden müssen.

Qualité de l'eau - Échantillonnage - Partie 3: Conservation et manipulation des échantillons d'eau (ISO 5667-3:2018)

Le présent document spécifie les exigences générales relatives à l'échantillonnage, la conservation, la manipulation, le transport et le stockage de tous les échantillons d'eau, y compris ceux destinés à des analyses biologiques.
Elle ne s'applique pas aux échantillons d'eau destinés à des analyses microbiologiques telles que spécifiées dans l'ISO 19458, des essais écotoxicologiques, des essais biologiques et ni à l'échantillonnage passif tel que spécifié dans le domaine d'application de l'ISO 5667‑23.
Le présent document s'applique en particulier chaque fois qu'un échantillon ponctuel ou composite ne peut être analysé sur site et doit être transporté vers un laboratoire pour analyse.

Kakovost vode - Vzorčenje - 3. del: Konzerviranje in ravnanje z vzorci vode (ISO 5667-3:2018)

Ta dokument določa splošne zahteve za vzorčenje, konzerviranje, ravnanje, prevoz in skladiščenje vseh vzorcev vode, tudi tistih za biološke analize.
Ne uporablja se za vzorce vode za mikrobiološke analize iz standarda ISO 19458 ter za ekotoksikološke preskuse, biološke preskuse in pasivno vzorčenje iz standarda ISO 5667-23.
Ta dokument je zlasti primeren, če naključnih ali sestavljenih vzorcev ni mogoče analizirati na mestu samem in jih je treba prenesti v laboratorij za analizo.

General Information

Status
Withdrawn
Publication Date
12-Jun-2018
Withdrawal Date
09-Apr-2024
Technical Committee
Drafting Committee
Current Stage

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SLOVENSKI STANDARD
01-september-2018
1DGRPHãþD
SIST EN ISO 5667-3:2013
.DNRYRVWYRGH9]RUþHQMHGHO.RQ]HUYLUDQMHLQUDYQDQMH]Y]RUFLYRGH ,62

Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667
-3:2018)
Wasserbeschaffenheit - Probenahme - Teil 3: Konservierung und Handhabung von
Wasserproben (ISO 5667-3:2018)
Qualité de l'eau - Échantillonnage - Partie 3: Conservation et manipulation des
échantillons d'eau (ISO 5667-3:2018)
Ta slovenski standard je istoveten z: EN ISO 5667-3:2018
ICS:
13.060.45 Preiskava vode na splošno Examination of water in
general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 5667-3
EUROPEAN STANDARD
NORME EUROPÉENNE
June 2018
EUROPÄISCHE NORM
ICS 13.060.45 Supersedes EN ISO 5667-3:2012
English Version
Water quality - Sampling - Part 3: Preservation and
handling of water samples (ISO 5667-3:2018)
Qualité de l'eau - Échantillonnage - Partie 3: Wasserbeschaffenheit - Probenahme - Teil 3:
Conservation et manipulation des échantillons d'eau Konservierung und Handhabung von Wasserproben
(ISO 5667-3:2018) (ISO 5667-3:2018)
This European Standard was approved by CEN on 9 June 2018.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 5667-3:2018 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 5667-3:2018) has been prepared by Technical Committee ISO/TC 147 "Water
quality" in collaboration with Technical Committee CEN/TC 230 “Water analysis” the secretariat of
which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by December 2018, and conflicting national standards
shall be withdrawn at the latest by December 2018.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 5667-3:2012.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 5667-3:2018 has been approved by CEN as EN ISO 5667-3:2018 without any
modification.
INTERNATIONAL ISO
STANDARD 5667-3
Fifth edition
2018-05
Water quality — Sampling —
Part 3:
Preservation and handling of water
samples
Qualité de l'eau — Échantillonnage —
Partie 3: Conservation et manipulation des échantillons d'eau
Reference number
ISO 5667-3:2018(E)
©
ISO 2018
ISO 5667-3:2018(E)
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Fax: +41 22 749 09 47
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved

ISO 5667-3:2018(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Sampling and chain of custody . 2
5 Reagents and materials . 2
6 Containers . 5
6.1 Container selection and preparation . 5
6.2 Filtration on site . 5
6.3 Filling the container . 5
7 Sample handling and preservation . 5
7.1 Sample handling and preservation for physical and chemical examination . 5
7.2 Sample handling and preservation for biological examination . 6
7.3 Sample handling and preservation for radiochemical analysis . 7
8 Sample transport . 7
9 Identification of samples . 8
10 Sample reception . 8
11 Sample storage . 8
Annex A (informative) Techniques for sample preservation .10
Annex B (informative) Container preparation .44
Annex C (informative) Protocol as used in Dutch validation studies .45
Bibliography .47
ISO 5667-3:2018(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO’s adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following
URL: www .iso .org/iso/foreword .html.
This document was prepared by Technical Committee ISO/TC 147, Water quality, Subcommittee SC 6,
Sampling (general methods).
This fifth edition cancels and replaces the fourth edition (ISO 5667-3:2012), of which it constitutes a
minor revision. The changes compared to the previous edition are as follows:
— updated references in Table A.1;
— clarification in the Introduction concerning use of the preservation times and conditions set out in
Table A.1.
A list of all parts in the ISO 5667 series can be found on the ISO website.
iv © ISO 2018 – All rights reserved

ISO 5667-3:2018(E)
Introduction
This document is intended to be used in conjunction with ISO 5667-1, which deals with the design of
sampling programmes and sampling techniques.
Where possible this document has been brought into line with current standards. Where new research
or validation results have provided new insights, the latest knowledge has been used.
Guidance on validation protocols can be found in ISO 17034.
ISO 5667-3 provides in Table A.1 validated preservation times and/or conditions as well as descriptions
of best practice. Table A.1 also refers, for each analyte, to those ISO standards available at the date of
publication of this ISO 5667-3. This is however not an exhaustive list. Other methods may be used when
they have been validated. However, it is strongly recommended that where a method validation is not
available, the preservation times for the analyte as listed in Table A.1 for ISO test methods be followed.
The preservation and storage conditions and maximum storage times per analyte as listed in Table A.1
should be regarded as default conditions to be applied in the absence of any other information.
However, if validation of preservation techniques and holding times has been carried out, relative
to specific circumstances and matrices, by a laboratory, then, provided that it can produce evidence
of this validation where they differ from those set out in Table A.1 of this standard, these validated
preservation and storage conditions and maximum storage times are deemed acceptable for use by the
validating laboratories.
Attention is drawn to the proposed development of a new part in the ISO 5667 series, which further
elaborates on ISO 566
...

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