EN ISO 17881-2:2016

Textiles - Determination of certain flame retardants - Part 2: Phosphorus flame retardants (ISO 17881-2:2016)

ISO 17881-2:2016 specifies a test method for determining some phosphorous flame retardants in textiles by high performance liquid chromatography ? tandem mass spectrometry (HPLC-MS/MS).
The method is applicable to all kinds of textile products.
NOTE          For tris (1-aziridinyl) phosphineoxide (TEPA), only unbonded TEPA is extractable.

Textilien - Bestimmung einiger Flammschutzmittel - Teil 2: Phosphororganische Flammschutzmittel (ISO 17881-2:2016)

Dieser Teil der ISO 17881 legt ein Prüfverfahren zur Bestimmung einiger phosphororganischer Flammschutzmittel in Textilien durch Hochleistungsflüssigkeitschromatographie - Tandem-Massenspektrometrie (en: high performance liquid chromatography – tandem mass spectrometry, HPLC-MS/MS) fest.
Das Verfahren gilt für alle Arten textiler Erzeugnisse.
ANMERKUNG   Tris(1-aziridinyl)phosphinoxid (TEPA) ist nur als ungebundenes TEPA extrahierbar.

Textiles - Détermination de certains retardateurs de flamme - Partie 2: Retardateurs de flamme phosphorés (ISO 17881-2:2016)

ISO 17881-2:2016 spécifie une méthode d'essai pour la détermination d'un certain nombre de retardateurs de flamme phosphorés dans les textiles, par chromatographie liquide haute performance ? spectrométrie de masse en tandem (CLHP-SM/SM).
Cette méthode s'applique à tous les types de produits textiles.
NOTE          Pour l'oxyde de tris(1-aziridinyl)phosphine (TEPA), seul le TEPA non lié peut être extrait.

Tekstilije - Določevanje nekaterih zaviralcev gorenja - 2. del: Fosforjevi zaviralci gorenja (ISO 17881-2:2016)

Ta del standarda ISO 17881 določa preskusno metodo za določanje nekaterih fosforjevih zaviralcev gorenja s tekočinsko kromatografijo visoke zmogljivosti – tandemsko masno spektrometrijo (GC-MS). Metoda se uporablja za vse vrste tekstilnih izdelkov.
OPOMBA Za tris (1-aziridinil) fosfinoksid (TEPA) je mogoče izločiti samo TEPA brez vezave.

General Information

• Status: Published
• Publication Date: 23-Feb-2016
• Withdrawal Date: 30-Aug-2016
• ICS: 59.080.01 - Textiles in general
• Technical Committee: CEN/TC 248 - Textiles and textile products
• Drafting Committee: CEN/TC 248/WG 26 - Methods of test for phthalates
• Current Stage: 6060 - Definitive text made available (DAV) - Publishing
• Start Date: 24-Feb-2016
• Completion Date: 24-Feb-2016
• Ref Project: SIST EN ISO 17881-2:2016 - Textiles - Determination of certain flame retardants - Part 2: Phosphorus flame retardants (ISO 17881-2:2016)

Standards Content (Sample)

SLOVENSKI STANDARD
01-maj-2016
7HNVWLOLMH'RORþHYDQMHQHNDWHULK]DYLUDOFHYJRUHQMDGHO)RVIRUMHYL]DYLUDOFL
JRUHQMD,62
Textiles - Determination of certain flame retardants - Part 2: Phosphorus flame retardants
(ISO 17881-2:2016)
Textilien - Bestimmung einiger Flammschutzmittel - Teil 2: Phosphororganische-
Flammschutzmittel (ISO 17881-2:2016)
Textiles - Détermination de certains retardateurs de flamme - Partie 2: Retardateurs de
flamme phosphorés (ISO 17881-2:2016)
Ta slovenski standard je istoveten z: EN ISO 17881-2:2016
ICS:
13.220.40 Sposobnost vžiga in Ignitability and burning
obnašanje materialov in behaviour of materials and
proizvodov pri gorenju products
59.080.01 Tekstilije na splošno Textiles in general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 17881-2
EUROPEAN STANDARD
NORME EUROPÉENNE
February 2016
EUROPÄISCHE NORM
ICS 59.080.01
English Version
Textiles - Determination of certain flame retardants - Part
2: Phosphorus flame retardants (ISO 17881-2:2016)
Textiles - Détermination de certains retardateurs de Textilien - Bestimmung einiger Flammschutzmittel -
flamme - Partie 2: Retardateurs de flamme phosphorés Teil 2: Phosphororganische Flammschutzmittel (ISO
(ISO 17881-2:2016) 17881-2:2016)
This European Standard was approved by CEN on 11 December 2015.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 17881-2:2016 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
European foreword
This document (EN ISO 17881-2:2016) has been prepared by Technical Committee ISO/TC 38
“Textiles” in collaboration with Technical Committee CEN/TC 248 “Textiles and textile products” the
secretariat of which is held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by August 2016, and conflicting national standards shall
be withdrawn at the latest by August 2016.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent
rights.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 17881-2:2016 has been approved by CEN as EN ISO 17881-2:2016 without any
modification.
INTERNATIONAL ISO
STANDARD 17881-2
First edition
2016-02-01
Textiles — Determination of certain
flame retardants —
Part 2:
Phosphorus flame retardants
Textiles — Détermination de certains retardateurs de flamme —
Partie 2: Retardateurs de flamme phosphorés
Reference number
ISO 17881-2:2016(E)
©
ISO 2016
ISO 17881-2:2016(E)
© ISO 2016, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
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ii © ISO 2016 – All rights reserved

ISO 17881-2:2016(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Principle . 1
3 Reagents . 1
4 Apparatus . 1
5 Procedure. 2
5.1 Preparation of standard solutions . 2
5.1.1 Stock standard solution . 2
5.1.2 Working solution . 2
5.2 Preparation of test specimen . 2
5.3 Ultrasonic wave extraction . 2
5.4 Flame retardants determination . 2
6 Calculation . 3
7 Test report . 3
Annex A (informative) Test parameters by HPLC-MS/MS . 4
Annex B (informative) Round Robin test . 6
ISO 17881-2:2016(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
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ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents s
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