CEN/TS 16172:2013

Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS)

This Technical Specification specifies the determination of trace elements in aqua regia or nitric acid digest solutions of sludge, treated biowaste and soil, using atomic absorption spectrometry with electrothermal atomisation in a graphite furnace. The method is applicable for the determination of the following elements:
Arsenic (As), cadmium (Cd), cobalt (Co), lead (Pb), antimony (Sb), thallium (Tl), vanadium (V).
This method may be applied to other elements. The lower working range is approximately 0,1 mg/kg to 0,01 mg/kg, depending on the element to be determined.

Schlamm, behandelter Bioabfall und Boden - Bestimmung von Elementen mittels Graphitrohrofen-Atomabsorptionsspektrometrie (GF-AAS)

Diese Technische Spezifikation legt ein Verfahren zur Bestimmung von Spurenelementen in Königswasser- und Salpetersäure-Aufschlusslösungen von Schlamm, behandeltem Bioabfall und Boden unter Anwendung von Atomabsorptionsspektrometrie mit elektrothermischer Atomisierung in einem Graphitrohrofen fest. Das Verfahren ist anwendbar auf die Bestimmung geringer Konzentrationen der folgenden Elemente:
Antimon (Sb), Arsen (As), Blei (Pb), Cadmium (Cd), Kobalt (Co), Thallium (Tl), Vanadium (V).
Dieses Verfahren darf für die Bestimmung anderer Elemente angewendet werden. Die untere Nachweisgrenze ist etwa 0,1 mg/kg bis 0,01 mg/kg je nach zu bestimmendem Element.

Boues, bio-déchets traités et sols - Détermination des éléments par spectrométrie d'absorption atomique avec four en graphite (GF-AAS)

La présente Spécification technique spécifie la détermination des éléments en traces solubles dans des solutions de digestion d’eau régale ou d’acide nitrique de boues, de bio-déchets traités et de sols, en utilisant la spectrométrie d’absorption atomique avec atomisation électrothermique dans un four graphite. La méthode est applicable pour la détermination des éléments suivants :
Arsenic (As), cadmium (Cd), cobalt (Co), plomb (Pb), antimoine (Sb), thallium (Tl), vanadium (V).
La présente méthode peut être appliquée à d’autres éléments. La plus faible gamme de mesure est d’environ 0,1 mg/kg à 0,01 mg/kg, en fonction de l’élément à doser.

Blato, obdelani biološki odpadki in tla - Določevanje elementov z metodo atomske absorpcijske spektrometrije z grafitno pečjo (GF-AAS)

Ta tehnična specifikacija opredeljuje določevanje elementov v sledeh v zlatotopki ali izvlečku dušikove kisline blata, obdelanih bioloških odpadkov in tal z metodo atomske absorpcijske spektrometrije z grafitno pečjo. Metoda se uporablja za določevanje naslednjih elementov: arzen (As), kadmij (Cd), kobalt (Co), svinec (Pb), antimon (Sb), talij (Tl), vanadij (V). Ta metoda se lahko uporablja tudi za določevanje drugih elementov. Spodnji delovni obseg znaša približno od 0,1 mg/kg do 0,01 mg/kg, odvisno od elementa za določevanje.

General Information

• Status: Withdrawn
• Publication Date: 29-Jan-2013
• Withdrawal Date: 03-Oct-2017
• ICS: 13.030.01 - Wastes in general
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: CEN/TC 444 - Environmental characterization
• Drafting Committee: CEN/TC 444/WG 3 - Inorganic analysis
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 04-Oct-2017
• Directive: 86/278/EEC - Protection of the environment, and in particular of the soil, when sewage sludge is used in agriculture
• Mandate: M/330 - Mandate given to CEN for the development of horizontal standards in the fields of sludge, biowaste and soil.
• Ref Project: SIST-TS CEN/TS 16172:2013 - Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS)

Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 16172:2013
01-julij-2013
%ODWRREGHODQLELRORãNLRGSDGNLLQWOD'RORþHYDQMHHOHPHQWRY]PHWRGRDWRPVNH
DEVRUSFLMVNHVSHNWURPHWULMH]JUDILWQRSHþMR*)$$6
Sludge, treated biowaste and soil - Determination of elements using graphite furnace
atomic absorption spectrometry (GF-AAS)
Schlamm, behandelter Bioabfall und Boden - Bestimmung von Elementen mittels
Graphitofen-Atomabsorptionsspektrometrie (GF-AAS)
Boue, biodéchets traités et sols - Détermination des éléments par spectrométrie
d'absorption atomic avec four en graphite (GF-AAS)
Ta slovenski standard je istoveten z: CEN/TS 16172:2013
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
13.080.10 .HPLMVNH]QDþLOQRVWLWDO Chemical characteristics of
soils
SIST-TS CEN/TS 16172:2013 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST-TS CEN/TS 16172:2013

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SIST-TS CEN/TS 16172:2013


TECHNICAL SPECIFICATION
CEN/TS 16172

SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION
January 2013
ICS 13.080.10; 13.030.01
English Version
Sludge, treated biowaste and soil - Determination of elements
using graphite furnace atomic absorption spectrometry (GF-
AAS)
Boues, bio-déchets traités et sols - Détermination des Schlamm, behandelter Bioabfall und Boden - Bestimmung
éléments par spectrométrie d'absorption atomique avec von Elementen mittels Graphitrohrofen-
four en graphite (GF-AAS) Atomabsorptionsspektrometrie (GF-AAS)
This Technical Specification (CEN/TS) was approved by CEN on 16 June 2012 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their
comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available
promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS)
until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United
Kingdom.





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© 2013 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 16172:2013: E
worldwide for CEN national Members.

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SIST-TS CEN/TS 16172:2013
CEN/TS 16172:2013 (E)
Contents Page
Foreword .3
Introduction .4
1 Scope .5
2 Normative references .5
3 Principle .5
4 Interferences and sources of error .6
5 Reagents .6
6 Apparatus .8
7 Procedure .9
7.1 Graphite furnace programme .9
7.2 Test solution .9
7.3 Test blank solution .
...