prEN ISO 3884

Solid recovered fuels - Methods for the determination of the content of elements (Al, Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn) (ISO/DIS 3884:2024)

This International Standard specifies methods for the determination of major and minor element concentrations in solid recovered fuels after digestion by the use of different acid mixtures and by addition of a fluxing agent for SRF ash and is applicable for major and minor/trace elements: Major elements: Aluminium (Al), Calcium (Ca), Iron (Fe), Potassium (K), Magnesium (Mg), Sodium (Na), Phosphorus (P), Sulphur (S), Silicon (Si) and Titanium (Ti). Minor/trace elements: Arsenic (As), Barium (Ba), Beryllium (Be), Cadmium (Cd), Cobalt (Co), Chromium (Cr), Copper (Cu), Mercury (Hg), Molybdenum (Mo), Manganese (Mn), Nickel (Ni), Lead (Pb), Antimony (Sb), Selenium (Se), Tin (Sn), Thallium (Tl), Vanadium (V) and Zink (Zn).

Feste Sekundärbrennstoffe - Verfahren zur Bestimmung des Gehaltes an Elementen (Al, Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn) (ISO/DIS 3884:2024)

Combustibles solides de récupération - Méthodes pour la détermination de la teneur en éléments (Al, Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn) (ISO/DIS 3884:2024)

Trdna alternativna goriva - Metode za določevanje glavnih elementov (Al, Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn) (ISO/DIS 3884:2024)

General Information

• Status: Not Published
• Publication Date: 15-Jun-2025
• ICS: 75.160.10 - Solid fuels
• Technical Committee: CEN/TC 343 - Solid Recovered Fuels
• Drafting Committee: CEN/TC 343 - Solid Recovered Fuels
• Current Stage: 4599 - Dispatch of FV draft to CMC - Finalization for Vote
• Start Date: 10-Oct-2024
• Due Date: 24-Dec-2024
• Completion Date: 10-Oct-2024
• Ref Project: oSIST prEN ISO 3884:2024 - Solid recovered fuels – Methods for the determination of the content of elements (Al, Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn) (ISO/DIS 3884:2024)

Relations

• Revises: EN 15410:2011 - Solid recovered fuels - Methods for the determination of the content of major elements (Al, Ca, Fe, K, Mg, Na, P, Si, Ti)
• Effective Date: 18-Jan-2023
• Revises: EN 15411:2011 - Solid recovered fuels - Methods for the determination of the content of trace elements (As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Tl, V and Zn)
• Effective Date: 21-Dec-2022

Standards Content (Sample)

SLOVENSKI STANDARD
01-april-2024
Trdna alternativna goriva - Metode za določevanje glavnih elementov (Al, Ca, Fe,
K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl,
V, Zn) (ISO/DIS 3884:2024)
Solid recovered fuels – Methods for the determination of the content of elements (Al, Ca,
Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se, Sn,
Tl, V, Zn) (ISO/DIS 3884:2024)
Feste Sekundärbrennstoffe - Verfahren zur Bestimmung des Gehaltes an Elementen (Al,
Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni, Pb, Sb, Se,
Sn, Tl, V, Zn) (ISO/DIS 3884:2024)
Combustibles solides de récupération - Méthodes pour la détermination de la teneur en
éléments (Al, Ca, Fe, K, Mg, Na, P, S, Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Mn, Ni,
Pb, Sb, Se, Sn, Tl, V, Zn) (ISO/DIS 3884:2024)
Ta slovenski standard je istoveten z: prEN ISO 3884
ICS:
75.160.10 Trda goriva Solid fuels
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

DRAFT
International
Standard
ISO/DIS 3884
ISO/TC 300
Solid recovered fuels — Methods for
Secretariat: SFS
the determination of the content of
Voting begins on:
elements (Al, Ca, Fe, K, Mg, Na, P, S,
2024-02-12
Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg,
Voting terminates on:
Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn)
2024-05-06
ICS: 75.160.10
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENTS AND APPROVAL. IT
IS THEREFORE SUBJECT TO CHANGE
AND MAY NOT BE REFERRED TO AS AN
INTERNATIONAL STANDARD UNTIL
PUBLISHED AS SUCH.
This document is circulated as received from the committee secretariat.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
ISO/CEN PARALLEL PROCESSING
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
NATIONAL REGULATIONS.
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION.
Reference number
ISO/DIS 3884:2024(en)
DRAFT
ISO/DIS 3884:2024(en)
International
Standard
ISO/DIS 3884
ISO/TC 300
Solid recovered fuels — Methods for
Secretariat: SFS
the determination of the content of
Voting begins on:
elements (Al, Ca, Fe, K, Mg, Na, P, S,
Si, Ti, As, Ba, Be, Cd, Co, Cr, Cu, Hg,
Voting terminates on:
Mo, Mn, Ni, Pb, Sb, Se, Sn, Tl, V, Zn)
ICS: 75.160.10
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENTS AND APPROVAL. IT
IS THEREFORE SUBJECT TO CHANGE
AND MAY NOT BE REFERRED TO AS AN
INTERNATIONAL STANDARD UNTIL
PUBLISHED AS SUCH.
This document is circulated as received from the committee secretariat.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
© ISO 2024
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
STANDARDS MAY ON OCCASION HAVE TO
ISO/CEN PARALLEL PROCESSING
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
BE CONSIDERED IN THE LIGHT OF THEIR
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
or ISO’s member body in the country of the requester.
NATIONAL REGULATIONS.
ISO copyright office
RECIPIENTS OF THIS DRAFT ARE INVITED
CP 401 • Ch. de Blandonnet 8
TO SUBMIT, WITH THEIR COMMENTS,
CH-1214 Vernier, Geneva
NOTIFICATION OF ANY RELEVANT PATENT
Phone: [phone]
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION.
Email: [e-mail]
Website: www.iso.org
Published in Switzerland Reference number
ISO/DIS 3884:2023(en)
ii
ISO/DIS 3884:2023(en)
Contents Page
Foreword .v
Introduction .vi
1 Scope . 1
2 Normative references . 2
3 Terms and definitions . 2
4 Symbols and abbreviations . 2
5 Safety remarks . 4
6 Principle . 5
7 Reagents . 5
8 Apparatus . 5
9 Interferences and sources of errors . 7
9.1 General information.7
9.2 Closed vessel system for microwave digestion .7
10 Preparation of the test sample. 7
11 Procedure . 8
11.1 General .8
11.2 Blank test .8
11.3 Method A (general method for SRF and major elements in ashed SRF) - Microwave
assisted digestion with hydrochloric, nitric and hydrofluoric acid mixture (6 ml HCl;
2 ml HNO ; 2 ml HF) .8
11.4 Method AT (method for SRF and major elements in ashed SRF) - Microwave assisted
digestion with hydrochloric, nitric and tetrafluoroboric acid mixture (6 ml HCl; 2 ml
HNO ; 4 ml HBF ) .10
3 4
11.5 Method B (e.g. plastic based SRF and others if method A cannot be applied) - Microwave
assisted digestion with hydrochloric, nitric and hydrofluoric acid mixture (0,5 ml HCl;
6 ml HNO ; 1 ml HF) .11
11.6 Method BT (e.g. plastic based SRF and others) - Microwave assisted digestion with
hydrochloric, nitric and tetrafluoroboric acid mixture (0,5 ml HCl; 6 ml HNO ; 2 ml
HBF ) .11
11.7 Method C (e.g. wood based SRFs) - Microwave assisted digestion with nitric acid,
hydrogen peroxide and hydrofluoric acid mixture (2,5 ml H O ; 5 ml HNO ; 0,4 ml HF) . 12
2 2 3
11.8 Method CT (e.g. wood based SRFs) - Microwave assisted digestion with nitric acid,
hydrogen peroxide and tetrafluoroboric acid mixture (2,5 ml H O ; 5 ml HNO ; 0,8 ml
2 2 3
HBF ) . 13
11.9 Method D (major elements in SRF ash) – digestion of ashed SRF with fluxing agent
lithium metaborate (fused bead) . 13
12 Analysis . . 14
12.1 Preparation of the solution for analysis .14
12.2 Analytical step .14
12.3 XRF analysis on ashed samples – sample preparation (major elements only) .14
13 Calculations .15
14 Quality control .15
15 Performance characteristics .15
16 Test report .15
Annex A (informative) Calibration of the power adjustment . 17
Annex B (informative) Validation and performance data (SRF22ERI) .18

iii
ISO/DIS 3884:2023(en)
Annex C (informative) Performance data (QUOVADIS) .63
Annex D (informative) Results of ruggedness testing (QUOVADIS) . 76
Bibliography .80

iv
ISO/DIS 3884:2023(en)
Foreword
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